A new method for in situ structural investigations of nano-sized amorphous and crystalline materials using mixed-flow reactors

Hoeher, A.; Mergelsberg, S.; Borkiewicz, O.J.; Dove, P.M.; Michel, F.M.

doi:10.1107/S2053273319008623

Acta Crystallographica Section A
Acta Crystallographica
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Figure 5
Comparison of the PDF data collected for ACP and brushite, and different considered backgrounds: CaCl₂, Na₂HPO₄ and deionized water. The first two peaks in the ACP and brushite data represent mainly the P–O and Ca–O distances, with some O–O contributions. The PDF profiles for CaCl₂·H₂O and Na₂HPO₄ have similar locations for these initial peaks, but ACP and brushite also contain structure that is not inherited from the reactant solutions. The water PDF does not have a peak in the same location as peaks in ACP and brushite, ensuring that no signal from the sample is accidentally subtracted.

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ISSN: 2053-2733

Volume 75| Part 5| September 2019| Pages 758-765

https://doi.org/10.1107/S2053273319008623

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