A new method for in situ structural investigations of nano-sized amorphous and crystalline materials using mixed-flow reactors

Hoeher, A.; Mergelsberg, S.; Borkiewicz, O.J.; Dove, P.M.; Michel, F.M.

doi:10.1107/S2053273319008623

Acta Crystallographica Section A
Acta Crystallographica
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Figure 9
In situ PDF data from ACC and ACP synthesized in the MFR. There are distinct differences between the phases, most notably in the position of the first peak at 1.6 Å for the P–O distances in ACP and at 1.3 Å for the C–O distances in ACC.

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ISSN: 2053-2733

Volume 75| Part 5| September 2019| Pages 758-765

https://doi.org/10.1107/S2053273319008623

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