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Figure 10
The measured GISAXS intensities (three left-hand columns) and Monte Carlo simulations (right-most column) for (a)–(d) sample 1, (e)–(h) sample 2 and (i)–(l) sample 3. The measurements are performed for different mean orientation angles ψ of the side facets of the NWs with respect to the X-ray beam, namely from 0° to 90° in steps of 5°. For clarity, these measurements are presented in three different panels (from 0° to 30°, from 30° to 60° and from 60° to 90°). The intensities are plotted as I(qx)qx4 versus qx to highlight deviations from Porod's law. The curves calculated at ψ = 0° for each sample are repeated as blue curves in the left-most column, for direct comparison of the calculated and measured curves.

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ISSN: 2053-2733
Volume 77| Part 1| January 2021| Pages 42-53
https://doi.org/10.1107/S205327332001548X
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