The role of absorption in 3D electron diffraction dynamical structure refinement

Colmey, B.; Doherty, T.A.S.; Malik, S.A.; Midgley, P.A.

doi:10.1107/S2053273326009459

Figure 3
Thickness dependence of residual error R₁ (%) between simulated $[I_{{\rm abs}}]$ and $[I_{{\rm no\,abs}}]$ . (a) Integrated intensities (dark blue) compared with per-tilt intensities (light blue) for CsPbBr₃ at

; light-blue points are R₁ averages across $[\pm 1.5^{\circ}]$ tilt series with error bars showing standard deviation around the mean. Best-fit slopes were determined, yielding 0.048 and 0.058 % nm⁻¹ for the integrated intensities and per-tilt values, respectively. (b) Integrated intensity R₁ curves for CsPbBr₃, α-quartz and borane, each shown with three representative orientations (best-fit slopes and [uvw] indices given in Table S3).

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ISSN: 2053-2733

Volume 82| Part 6| November 2026|

https://doi.org/10.1107/S2053273326009459

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