Effect of pressure on the crystal structure of salicylaldoxime-I, and the structure of salicylaldoxime-II at 5.93 GPa

Wood, P.A.; Forgan, R.S.; Henderson, D.; Parsons, S.; Pidcock, E.; Tasker, P.A.; Warren, J.E.

doi:10.1107/S0108768106031752

Acta Crystallographica Section B
Acta Crystallographica
Section B STRUCTURAL SCIENCE, CRYSTAL ENGINEERING AND MATERIALS

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Figure 7
Space-filling plots showing the contraction of voids which occur in salicylaldoxime phase I with the application of pressure. The top and bottom rows correspond to the salicylaldoxime-I structure at ambient pressure and at 5.28 GPa, respectively. (a) and (b) show the structure with the a* direction vertical; there are large voids between the molecules, which almost disappear completely with increasing pressure. (c) and (d) show the void between molecules related by the n-glide; this gap also closes up considerably with the application of pressure.

STRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS

ISSN: 2052-5206

Volume 62| Part 6| November 2006| Pages 1099-1111

doi:10.1107/S0108768106031752

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