Figure 4
Relative variation in the unit-cell parameters of thiophosgene at different temperatures. Symbols denote values resulting from Rietveld refinements (error bars are substantially smaller than the symbols); the solid lines are obtained from the fitting of a Debye-type model to the unit-cell parameters, as described in the text. The absolute values of the unit-cell parameters are tabulated in Table S1 and plotted in Figs. S1, S2 and S3. |