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Figure 4
(a) Crystal packing of 4 viewed along a (top) and along b (bottom). The view along a shows four columns; the view along b shows two columns in side profile. Columns comprise TBC6 and DMSO; chlorobenzene molecules occupy intercolumnar sites. Hydrogen bonds are shown as green dashed lines. Top and side views of a column for all structures are provided in Table S3. (b) TBC6–TBC6 motifs IV and V within a single column. H atoms are omitted for clarity; hydrogen bonds are shown as orange dashed lines. A, B and C denote symmetry-related TBC6 molecules. |
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