Figure 1
Local coordination of Sb and S atoms showing the Sb4S4 hetero-ring and an [SbS4]5− unit connected through a shared S3 atom (bottom), and one of the two disordered and diprotonated cyclam molecules (top), showing the atom-labelling scheme and displacement ellipsoids at the 50% probability level. H atoms have been omitted for clarity. [Symmetry codes: (i) −x + 2, y + , −z + ; (ii) −x + 2, −y + 2, −z + 1; (iii) −x + 2, −y + 1, −z + 1; (iv) −x + 1, −y + 2, −z; (v) x, −y + , z − .] |