Figure 1
The final Rietveld refinement for (3), form II, showing the experimental powder diffraction pattern (crosses, red in the electronic version of the paper), the calculated powder pattern (solid line, green) and the difference between the experimental and calculated powder patterns (lower line). Tick marks indicate the reflection positions. The hump is due to the borosilicate capillary. The high-angle area of the Rietveld refinement is magnified by a factor of 10. |