Four related benzazepine derivatives in a reaction pathway leading to a benzazepine carboxylic acid: hydrogen-bonded assembly in zero, one, two and three dimensions

Guerrero, S.A.; Sanabría, C.M.; Palma, A.; Cobo, J.; Glidewell, C.

doi:10.1107/S2053229614006007

Acta Crystallographica Section C
Acta Crystallographica
Section C STRUCTURAL CHEMISTRY

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Figure 12
Part of the crystal structure of compound (XII), showing the formation of a C(8)C(9)[R₂²(10)] chain of rings running parallel to [001]. The original atomic coordinates (Coda et al., 1986

) were used, modified by translations to assemble the asymmetric unit into a single molecule. H atoms bonded to O atoms are in positions calculated by assuming O—H distances of 0.85 Å and linear O—H⋯O hydrogen bonds. For the sake of clarity, the unit-cell outline has been omitted. Atoms marked with an asterisk (*) or a hash (#) are at the symmetry positions (−x + $[{3\over 2}]$ , −y, z − $[{1\over 2}]$ ) and (−x + $[{3\over 2}]$ , −y, z + $[{1\over 2}]$ ), respectively.

STRUCTURAL
CHEMISTRY

ISSN: 2053-2296

Volume 70| Part 4| March 2014| Pages 408-415

doi:10.1107/S2053229614006007

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