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Figure 3
PXRD patterns of NCL·MeOH[link] and NCL hydrate samples synthesized by reflux. (a) Pawley fit to the NCL·MeOH[link] pattern obtained on the product still wet with methanol. (b) Pawley fit to the PXRD pattern of NCL·MeOH[link] collected after storing in air overnight (blue tick marks = NCL·MeOH and black tick marks = hydrate). (c) Pawley fit of the PXRD pattern of NCL monohydrate HA (black tick marks), with a small amount of monohydrate HB (blue tick marks).

Journal logoSTRUCTURAL
CHEMISTRY
ISSN: 2053-2296
Volume 70| Part 8| July 2014| Pages 758-763
doi:10.1107/S2053229614015496
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