Figure 4
Scatter plots for the Bijvoet differences in the two twin components, prepared by the PLATON software (Spek, 2009). For preparing the plots, only non-overlapping reflections unaffected by the twinning were used. Only reflections with Δobs > 0.25σ(Δobs) are drawn. Reflections confirming the correct absolute structure are drawn in black and relections with the wrong sign are shown in red. Left: first twin component; 291 reflections are black and 74 are red. Right: second twin component; 66 reflections are black and 260 are red. |