A coordinatively flexible hexa­dentate ligand gives structurally isomeric complexes M2(L)X3 (M = Cu, Zn; X = Br, Cl)

Wegeberg, C.; McKee, V.; McKenzie, C.J.

doi:10.1107/S2053229615023773

Acta Crystallographica Section C
Acta Crystallographica
Section C STRUCTURAL CHEMISTRY

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Figure 1
The ESI mass spectra (acetonitrile, positive mode, 10⁻⁶ M) of (a) Zn₂Br₃(tpena) and (b) Cu₂Br₃(tpena). The ion at m/z 317.080 in part (b) is due to the loss of a CH₂Py arm and CO₂ from [Cu(tpena–CO₂–CH₂Py)]⁺ (see Fig. 2

for proposed structure).

STRUCTURAL
CHEMISTRY

ISSN: 2053-2296

Volume 72| Part 1| January 2016| Pages 68-74

doi:10.1107/S2053229615023773

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