view article

Figure 1
The asymmetric unit of (1), showing displacement ellipsoids at the 50% probability level. The N—H⋯Cl hydrogen bonds are indicated by double-dashed lines. The Cu⋯Cu separations (bronze double-dashed lines, Å) are as follows: Cu1⋯Cu2 = 2.7454 (13), Cu3⋯Cu4 = 2.7350 (14), Cu5⋯Cu6 = 2.7551 (15), Cu1⋯Cu7 = 3.0169 (9), Cu2⋯Cu8 = 3.0174 (12), Cu3⋯Cu8 = 3.2142 (13), Cu4⋯Cu9 = 2.8145 (12), Cu5⋯Cu9 = 3.1067 (12) and Cu6⋯Cu10 = 2.845 (10). The Cu⋯Cu⋯Cu angles (°) are as follows: Cu7⋯Cu1⋯Cu2 = 142.08 (3), Cu1⋯Cu2⋯Cu8 = 147.34 (4), Cu2⋯Cu8⋯Cu3 = 175.11 (4), Cu8⋯Cu3⋯Cu4 = 136.27 (4), Cu3⋯Cu4⋯Cu9 = 149.88 (5), Cu4⋯Cu9⋯Cu5 = 174.23 (4), Cu9⋯Cu5⋯Cu6 = 135.11 (4), Cu5⋯Cu6⋯Cu10 = 143.90 (4), Cu1⋯Cu7⋯Cu1i = 180 and Cu6⋯Cu10⋯Cu6ii = 180 [symmetry codes: (i) −x + 1, −y, −z; (ii) −x, −y, −z + 2].

Journal logoSTRUCTURAL
CHEMISTRY
ISSN: 2053-2296
Follow Acta Cryst. C
Sign up for e-alerts
Follow Acta Cryst. on Twitter
Follow us on facebook
Sign up for RSS feeds