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Figure 6
(a)/(b) The 51V NMR spectra of the crystallization solution of VMo7 and (c)/(d)/(e) solutions obtained upon dissolution of crystallized VMo7 at different pH values. Conditions: (a) 175 mM MoVI, 25 mM VV, pH = 3.1, 24 h after the synthesis; (b) same conditions as (a) after another 24 h; (c)/(d)/(e) 10 mM VV solution prepared from VMo7 by dissolving it in 0.5 mM NaCl at pH values of (c) 4.0, (d) 5.2 and (e) 6.0. The pH was adjusted by the addition of a dilute KOH solution.

Journal logoSTRUCTURAL
CHEMISTRY
ISSN: 2053-2296
Volume 75| Part 7| July 2019| Pages 872-876
https://doi.org/10.1107/S205322961900620X
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