Synthesis, decom­position studies and crystal structure of a three-dimensional CuCN network structure with protonated N-methyl­ethano­lamine as the guest cation

Koenigsmann, C.; Rachid, L.N.; Sheedy, C.M.; Corfield, P.W.R.

doi:10.1107/S2053229620004477

Acta Crystallographica Section C
Acta Crystallographica
Section C STRUCTURAL CHEMISTRY

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Figure 7
(a) Thermogravimetric analysis data for [meoenH]Cu₂(CN)₃. The temperature was ramped at 4 °C min⁻¹ to 400 °C (left), producing the first mass loss of 36%. The temperature was held at 400 °C for 120 min to produce the second mass loss of 52% of the initial mass in an isothermal step (right). (b) PXRD data collected after TGA of samples heated to 280 and 400 °C. The PXRD pattern for our synthesized CuCN and a standard pattern for CuO (COD 90144580) are also shown.

STRUCTURAL
CHEMISTRY

ISSN: 2053-2296

Volume 76| Part 5| May 2020| Pages 405-411

https://doi.org/10.1107/S2053229620004477

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