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Figure 9
Variation in (a) the unit-cell volume (•) and (b) the a (□) and c (filled □) axis lengths over the temperature range 300→200 K for form I. Error bars (where visible) are drawn at ±(3 × s.u.). The clear discontinuities in the axis lengths correspond to the phase transformation from the `high-temperature' TFDIB framework to the `low-temperature' framework.

Journal logoSTRUCTURAL
CHEMISTRY
ISSN: 2053-2296
Volume 76| Part 5| May 2020| Pages 524-529
https://doi.org/10.1107/S2053229620005690
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