Figure 1
The hk1 plane of reciprocal space of (NH4)Mg(HSO4)(SO4)(H2O)2 [100 K data in parts (a)/(b)] and of (NH4)MgH(SO4)2(H2O)2 [296 K data in part (c)] reconstructed from CCD data. (a) The small cell with matching reflections is marked with orange circles; no superstructure reflections are visible. (b) The actual supercell with matching reflections is marked with green circles. (c) The actual small cell is marked with orange circles without superstructure reflections. |