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Figure 2
Reconstructed precession images of the hk0 plane of (a) a single crystal of Al-stabilized LLZO directly after synthesis with some selected Bragg reflections indexed and (b) a single crystal after hydro­thermal alteration at 150 °C for 28 d. Note the presence of sharp superstructure reflections, which obey Ia[\overline{3}]d symmetry. In part (b), the yellow encircled Bragg reflections are the same as in part (a), while the blue encircled reflections in the rectangular box correspond (from left to right) to the [\overline {57}]0, [\overline {37}]0, [\overline {17}]0,… Bragg reflections.

Journal logoSTRUCTURAL
CHEMISTRY
ISSN: 2053-2296
Volume 78| Part 1| January 2022| Pages 1-6
https://doi.org/10.1107/S2053229621012250
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