Psilocybin: crystal structure solutions enable phase analysis of prior art and recently patented examples

Sherwood, A.M.; Kargbo, R.B.; Kaylo, K.W.; Cozzi, N.V.; Meisenheimer, P.; Kaduk, J.A.

doi:10.1107/S2053229621013164

Acta Crystallographica Section C
Acta Crystallographica
Section C STRUCTURAL CHEMISTRY

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Figure 24
(a) The Rietveld plot for the refinement of psilocybin Sample 22 (Hydrate A, heated 25 h at 40 °C). The blue crosses represent the observed data points and the green line is the calculated pattern. The cyan curve is the normalized error plot. (b) The Rietveld plot for the refinement of psilocybin Sample 23 (Hydrate A, heated 25 h at 45 °C). The blue crosses represent the observed data points and the green line is the calculated pattern. The cyan curve is the normalized error plot. (c) The Rietveld plot for the refinement of psilocybin Sample 24 (Hydrate A, heated 25 h at 55 °C). The blue crosses represent the observed data points and the green line is the calculated pattern. The cyan curve is the normalized error plot.

STRUCTURAL
CHEMISTRY

ISSN: 2053-2296

Volume 78| Part 1| January 2022| Pages 36-55

https://doi.org/10.1107/S2053229621013164

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