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Figure 2
NMR tube prepared for crystallization by (left) layering heptane onto a yellow THF solution, (middle) layering a yellow THF solution onto di­chloro­methane counter-solvent and (right) layering solution/counter-solvent in a lab-built constriction tube made from a Pasteur pipet.

Journal logoSTRUCTURAL
CHEMISTRY
ISSN: 2053-2296
Volume 80| Part 8| August 2024|
https://doi.org/10.1107/S2053229624006624
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