Figure 2
I/σ(I) versus resolution for 364 reflections from the scaled natrolite data sets that should be systematically absent in the space group Fdd2 under the kinematic approximation. The points are coloured according to which of the three crystals they come from. A few reflections from each crystal show significant violation of their expected absence. On the right, images from the dials.image_viewer of the three spots with highest I/σ(I) are shown, clearly indicating that these violations are present in the data and are not an artefact of data processing. |