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Figure 4
Rietveld refinement on the PXRD pattern of FA3Sb2I9 single crystals made by CDCG. Input unit-cell information was taken from the structure resolved from SCXRD data. Yobs (red) is the collected diffraction pattern, Ycalc (blue) is the calculated pattern from TOPAS-Academic and Yobs − Ycalc (yellow) is the residual plot. Reflections that are ≥5% of the highest intensity reflection are indexed.

Journal logoSTRUCTURAL
CHEMISTRY
ISSN: 2053-2296
Volume 82| Part 3| March 2026| Pages 138-143
https://doi.org/10.1107/S2053229626000811
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