most read articles

These are the most read articles in the last six months.

Crystallization of metastable monoclinic carnallite, KCl·MgCl₂·6H₂O: missing structural link in the carnallite family. M. Pannach, I. Paschke, H. Schmidt, D. Freyer & W. Voigt (2020). Acta Cryst. C76, 507-512.

Synthesis of N-substituted 3-(2-aryl-2-oxoethyl)-3-hydroxyindolin-2-ones and their conversion to N-substituted (E)-3-(2-aryl-2-oxoethylidene)indolin-2-ones: synthetic sequence, spectroscopic characterization and structures of four 3-hydroxy compounds and five oxoethylidene products. D. Becerra, J. Castillo, B. Insuasty, J. Cobo & C. Glidewell (2020). Acta Cryst. C76, 433-445.

First COVID-19 molecular docking with a chalcone-based compound: synthesis, single-crystal structure and Hirshfeld surface analysis study. M. A. Alsafi, D. L. Hughes & M. A. Said (2020). Acta Cryst. C76, 1043-1050.

Crystal structures of salts of bedaquiline. M. Okezue, D. Smith, M. Zeller, S. R. Byrn, P. Smith, S. Bogandowich-Knipp, D. K. Purcell & K. L. Clase (2020). Acta Cryst. C76, 1010-1023.

A new hydrate of magnesium carbonate, MgCO₃·6H₂O. C. Rincke, H. Schmidt & W. Voigt (2020). Acta Cryst. C76, 244-249.

There's many a good tune played on an old fiddle – a new colour for Alfred Werner's isomer counting. E. C. Constable (2020). Acta Cryst. C76, 312-313.

Crystal structure of a calcium(II)–pyrroloquinoline quinone (PQQ) complex outside a protein environment. H. Lumpe, P. Mayer & L. J. Daumann (2020). Acta Cryst. C76, 1051-1056.

Deciphering the hydrogen-bonding scheme in the crystal structure of triphenylmethanol: a tribute to George Ferguson and co-workers. T. Rodríguez Tzompantzi, A. G. Amaro Hernández, R. L. Meza-León & S. Bernès (2019). Acta Cryst. C75, 1266-1273.

Improving the solubility of berberine. J. A. Fernandes (2020). Acta Cryst. C76, 117.

The decades-old mystery of bis(diethyl ether)tungsten(IV) chloride solved. A. Schäfer (2021). Acta Cryst. C77, 167-168.

The many flavours of halogen bonds – message from experimental electron density and Raman spectroscopy. R. Wang, J. George, S. K. Potts, M. Kremer, R. Dronskowski & U. Englert (2019). Acta Cryst. C75, 1190-1201.

Regioselective synthesis and characterization of monovanadium-substituted β-octamolybdate [VMo₇O₂₆]⁵⁻. L. Krivosudský, A. Roller & A. Rompel (2019). Acta Cryst. C75, 872-876.

Tolerance factor and phase stability of the garnet structure. Corrigendum. Z. Song, D. Zhou & Q. Liu (2020). Acta Cryst. C76, 311.

(NH₄)Mg(HSO₄)(SO₄)(H₂O)₂ and NaSc(CrO₄)₂(H₂O)₂, two crystal structures comprising kröhnkite-type chains, and the temperature-induced phase transition (NH₄)Mg(HSO₄)(SO₄)(H₂O)₂ $\rightleftharpoons$ (NH₄)MgH(SO₄)₂(H₂O)₂. M. Weil & U. Kolitsch (2021). Acta Cryst. C77, 144-151.

Phase transition and structures of the twinned low-temperature phases of (Et₄N)[ReS₄]. E. Bernhardt & R. Herbst-Irmer (2020). Acta Cryst. C76, 231-235.

HBr or not HBr? That is the question: crystal structure of 6-hydroxy-1,4-diazepane-1,4-diium dibromide redetermined. M. Piontek, B. Morgenstern, N. Steinbrück, B. Oberhausen, G. Kickelbick & K. Hegetschweiler (2019). Acta Cryst. C75, 678-685.

Crystallographic curiosities: polymorphism and structures with Z′ > 1. W. Clegg (2019). Acta Cryst. C75, 833-834.

Intermolecular interactions and disorder in six isostructural celecoxib solvates. A. D. Bond & C. C. Sun (2020). Acta Cryst. C76, 632-638.

Absolute structure of the chiral pyrrolidine derivative (2S)-methyl (Z)-5-(2-tert-butoxy-1-cyano-2-oxoethylidene)pyrrolidine-2-carboxylate, a compound with low resonant scattering. A. Wang & U. Englert (2019). Acta Cryst. C75, 1448-1453.

Synthesis and characterization of enantiopure planar–chiral phosphorus-linked diferrocenes. P. Honegger, A. Roller & M. Widhalm (2021). Acta Cryst. C77, 152-160.

Crystal structure and characterization of magnesium carbonate chloride heptahydrate. C. Rincke, H. Schmidt, G. Buth & W. Voigt (2020). Acta Cryst. C76, 741-745.

A new tool for finding approximate symmetry. C. P. Brock (2019). Acta Cryst. C75, 835-836.

New node on the block for organic solid-state chemists: rtct-tetrakis(pyridin-4-yl)cyclobutane. E. W. Reinheimer (2021). Acta Cryst. C77, 123-124.

(E)-4-Bromo-2-[(phenylimino)methyl]phenol: a new polymorph and thermochromism. H. E. Mason, J. A. K. Howard & H. A. Sparkes (2020). Acta Cryst. C76, 1001-1004.

Three new acid M⁺ arsenates and phosphates with multiply protonated As/PO₄ groups. K. Schwendtner & U. Kolitsch (2019). Acta Cryst. C75, 1134-1141.

Sweet like chocolate. I. D. H. Oswald (2019). Acta Cryst. C75, 1021-1022.

Understanding of magnetic ordering in Gd-rich compounds. T. Nilges (2019). Acta Cryst. C75, 609.

Δ⁹-Tetrahydrocannabinolic acid A, the precursor to Δ⁹-tetrahydrocannabinol (THC). J. M. Skell, M. Kahn & B. M. Foxman (2021). Acta Cryst. C77, 84-89.

Variants of the X-phase in the Mn–Co–Ge system. V. Shtender, S. R. Larsen & M. Sahlberg (2021). Acta Cryst. C77, 176-180.

Crystallographic evidence for unintended benzisothiazolinone 1-oxide formation from benzothiazinones through oxidation. T. Eckhardt, R. Goddard, C. Lehmann, A. Richter, H. A. Sahile, R. Liu, R. Tiwari, A. G. Oliver, M. J. Miller, R. W. Seidel & P. Imming (2020). Acta Cryst. C76, 907-913.

Synthesis and structures of three isoxazole-containing Schiff bases. H. E. Mason, J. A. K. Howard & H. A. Sparkes (2020). Acta Cryst. C76, 927-931.

Structures of five salt forms of disulfonated monoazo dyes. H. C. Gardner, A. R. Kennedy, K. M. McCarney, E. Staunton, H. Stewart & S. J. Teat (2020). Acta Cryst. C76, 972-981.

Synthesis, decomposition studies and crystal structure of a three-dimensional CuCN network structure with protonated N-methylethanolamine as the guest cation. C. Koenigsmann, L. N. Rachid, C. M. Sheedy & P. W. R. Corfield (2020). Acta Cryst. C76, 405-411.

LaTe_1.82(1): modulated crystal structure and chemical bonding of a chalcogen-deficient rare earth metal polytelluride. H. Poddig, K. Finzel & T. Doert (2020). Acta Cryst. C76, 530-540.

Ammonium bis(salicylaldehyde thiosemicarbazonato)ferrate(III), a supramolecular material containing low-spin Fe^III. R. E. Powell, B. Stöger, C. Knoll, D. Müller, P. Weinberger & P. J. van Koningsbruggen (2020). Acta Cryst. C76, 625-631.

Assembly of two novel coordination polymers by selecting ditopic or chelating auxiliary ligands with naphthalene-2,6-dicarboxylic acid: synthesis, structure and luminescence sensing. Y. Zuo, J. Yang, C. Chen, Y.-S. Xue & J. Zhang (2020). Acta Cryst. C76, 1076-1084.

Sodium sulfite heptahydrate and its relation to sodium carbonate heptahydrate. M. Weil & K. Mereiter (2020). Acta Cryst. C76, 427-432.

4-Styrylquinolines from cyclocondensation reactions between (2-aminophenyl)chalcones and 1,3-diketones: crystal structures and regiochemistry. D. Rodríguez, S. A. Guerrero, A. Palma, J. Cobo & C. Glidewell (2020). Acta Cryst. C76, 883-890.

7-Iodo-5-aza-7-deazaguanine ribonucleoside: crystal structure, physical properties, base-pair stability and functionalization. D. Kondhare, S. Budow-Busse, C. Daniliuc & F. Seela (2020). Acta Cryst. C76, 513-523.

Polymorphism and phase transformation in the dimethyl sulfoxide solvate of 2,3,5,6-tetrafluoro-1,4-diiodobenzene. A. D. Bond & C. L. Truscott (2020). Acta Cryst. C76, 524-529.

Can we trust the experiment? Anisotropic displacement parameters in 1-(halomethyl)-3-nitrobenzene (halogen = Cl or Br). D. Mroz, R. Wang, U. Englert & R. Dronskowski (2020). Acta Cryst. C76, 591-597.

A new P,S-coordinating ferrocenyl ligand: synthesis of a precursor and its coordination compounds with Pd^II and Pt^II. Corrigendum. T. N. Mouas, J.-C. Daran, H. Merazig & E. Manoury (2020). Acta Cryst. C76, 1000.

The effect of cation–π interactions on the stability and electronic properties of anticancer drug Altretamine: a theoretical study. F. Alirezapour & A. Khanmohammadi (2020). Acta Cryst. C76, 982-991.

Bis(tetraphenylarsonium) hexafluoridotechnetate(IV) dihydrate: preparation, structure and spectroscopic analysis. S. M. Balasekaran & F. Poineau (2019). Acta Cryst. C75, 1613-1616.

Syntheses and solid-state structures of two cofacial (bis)dipyrrin dichromium complexes in different charge states. K. Carsch, S. E. Elder, D. K. Dogutan, D. G. Nocera, J. Yang, S.-L. Zheng, T. Daniel & T. A. Betley (2021). Acta Cryst. C77, 161-166.

Regio- and stereospecific assembly of dispiro[indoline-3,3′-pyrrolizine-1′,5′′-thiazolidines] from simple precursors using a one-pot procedure: synthesis, spectroscopic and structural characterization, and a proposed mechanism of formation. P. Romo, J. Quiroga, J. Cobo & C. Glidewell (2020). Acta Cryst. C76, 779-785.

Manganese(II) complexes derived from acyclic ligands having flexible alcohol arms: structural chracterization and SOD and catalase mimetic studies. V. McKee & M. Kose (2021). Acta Cryst. C77, 100-110.

The α-D-anomer of 2′-deoxycytidine: crystal structure, nucleoside conformation and Hirshfeld surface analysis. S. Budow-Busse, Y. Chai, S. L. Müller, C. Daniliuc & F. Seela (2021). Acta Cryst. C77, 202-208.

Conversion of 3-amino-4-arylamino-1H-isochromen-1-ones to 1-arylisochromeno[3,4-d][1,2,3]triazol-5(1H)-ones: synthesis, spectroscopic characterization and the structures of four products and one ring-opened derivative. D. E. Vicentes, A. L. Romero, R. Rodríguez, J. Cobo & C. Glidewell (2020). Acta Cryst. C76, 446-453.

The influence of the type of halogen substituent and its position on the molecular conformation, intermolecular interactions and crystal packing for a series of 1-benzoyl-3-(halogenophenyl)thioureas. D. Rosiak, A. Okuniewski & J. Chojnacki (2021). Acta Cryst. C77, 11-19.

Synthesis, structure and photophysical properties of two tetranuclear copper(I) iodide complexes based on acetylpyridine and diphosphine mixed ligands. B.-J. Cao, R. Li & X.-H. Huang (2021). Acta Cryst. C77, 61-67.

Crystal structure refinements of stoichiometric Ni₃Se₂ and NiSe. K. Unoki, A. Yoshiasa, G. Kitahara, T. Nishiayama, M. Tokuda, K. Sugiyama & A. Nakatsuka (2021). Acta Cryst. C77, 169-175.

Solid-state conformations of linear depsipeptide amides with an alternating sequence of α,α-disubstituted α-amino acid and α-hydroxy acid. A. Linden, J. E. F. Magirius & H. Heimgartner (2020). Acta Cryst. C76, 1-9.

Synthesis, crystal structure, and electronic structure of Li₂PbSiS₄: a quaternary thiosilicate with a compressed chalcopyrite-like structure. S. S. Stoyko, A. J. Craig, J. W. Kotchey & J. A. Aitken (2021). Acta Cryst. C77, 1-10.

The structure of Ce₂Al₃Ge₄ refined for the first time from single-crystal X-ray diffraction data. P. Tobash & S. Bobev (2021). Acta Cryst. C77, 81-83.

Trithiocyanuric acid: novel cocrystals and analysis of its tautomeric forms. K. Wzgarda-Raj, A. J. Rybarczyk-Pirek, S. Wojtulewski & M. Palusiak (2021). Acta Cryst. C77, 49-55.

Syntheses and structures of three macrocyclic supramolecular complexes and one Zn^II-containing coordination polymer generated from a semi-rigid multidentate N-containing ligand. X.-L. Niu, L. Wei, J.-C. Liu, W.-H. Jia, J.-P. Ma, L. Wang, J.-C. Wang & Y.-B. Dong (2021). Acta Cryst. C77, 29-39.

Synthesis, crystal structures, antiproliferative activities and reverse docking studies of eight novel Schiff bases derived from benzil. X.-J. Tan, D. Wang, X.-M. Hei, F.-C. Yang, Y.-L. Zhu, D.-X. Xing & J.-P. Ma (2020). Acta Cryst. C76, 44-63.

Two-step crystal–crystal phase transformation of N-salicylidene-p-aminobenzoic acid by gas–solid reaction with aqua–ammonia vapour. H. Sugiyama & H. Uekusa (2021). Acta Cryst. C77, 56-60.

Structural characterization and theoretical calculations of the monohydrate of the 1:2 cocrystal salt formed from acriflavine and 3,5-dinitrobenzoic acid. M. Marczak, K. Biereg, B. Zadykowicz & A. Sikorski (2021). Acta Cryst. C77, 116-122.

Dibenzoate esters of cis-tetralin-2,3-diol as analogs of (–)-epigallocatechin gallate: synthesis and crystal structure of anticancer drug candidates. R. N. Rutherford, S. Ura, T.-H. Chan, K. Fukumoto, T. Nishioka & A. Renzetti (2020). Acta Cryst. C76, 1085-1095.

Alkali and alkaline earth coordination polymers constructed from benzene-1,2,4,5-tetracarboxylic acid and flexible dicarboxylate acid ligands: syntheses, structures and spectroscopic and thermal properties. S. Lifa, C. Trifa, S. Bouacida, C. Boudaren & H. Merazig (2021). Acta Cryst. C77, 90-99.

Crystal structure and Hirshfeld surface analysis of the elusive trichlorobis(diethyl ether)oxomolybdenum(V). T. E. Shaw, P. LeMagueres, A. P. Sattelberger & T. Jurca (2020). Acta Cryst. C76, 947-951.

Honeycomb molecular network based upon a hydrate of 4,6-dichlororesorcinol and the photoproduct rtct-tetrakis(pyridin-4-yl)cyclobutane. C. L. Santana, J. D. Battle, D. K. Unruh & R. H. Groeneman (2021). Acta Cryst. C77, 111-115.

Polymorphism of methyl 4-amino-3-phenylisothiazole-5-carboxylate: an experimental and theoretical study. S. V. Shishkina, I. S. Konovalova, S. M. Kovalenko, D. V. Kravchenko & N. D. Bunyatyan (2021). Acta Cryst. C77, 40-48.

Nitroxide radicals appended to phthalonitriles: synthesis, structural characterization and photophysical properties. I. Fidan, E. Onal & C. Hirel (2021). Acta Cryst. C77, 137-143.

Conformational polymorphs of 3-cyclopropyl-5-(3-methyl-[1,2,4]triazolo[4,3-a]pyridin-7-yl)-1,2,4-oxadiazole. S. V. Shishkina, I. S. Konovalova, S. S. Kovalenko, L. L. Nikolaeva, N. D. Bunyatyan & S. M. Kovalenko (2021). Acta Cryst. C77, 20-28.

Structural and theoretical analysis of 2-chloro-4-nitroaniline and 2-methyl-6-nitroaniline salts. V. Medviediev & M. Daszkiewicz (2021). Acta Cryst. C77, 125-136.

Crystal structure of monoclinic hafnia (HfO₂) revisited with synchrotron X-ray, neutron diffraction and first-principles calculations. S. Pathak, P. Das, T. Das, G. Mandal, B. Joseph, M. Sahu, S. D. Kaushik & V. Siruguri (2020). Acta Cryst. C76, 1034-1042.

Conformational analysis of two new organotin(IV) structures completed with a CSD survey. F. Sabbaghi, A. As'habi, A. Saneei, M. Pourayoubi, A. A. Abdul Salam, M. Nečas, M. Dušek, M. Kučeráková & S. Acharya (2021). Acta Cryst. C77, 68-80.

A smorgasbord of halogen bonds?. G. R. Desiraju (2019). Acta Cryst. C75, 1188-1189.

Conformational flexibility in amidophosphoesters: a CSD analysis completed with two new crystal structures of (C₆H₅O)₂P(O)X [X = NHC₇H₁₃ and N(CH₂C₆H₅)₂]. B. Vahdani Alviri, M. Pourayoubi, A. A. Abdul Salam, M. Nečas, A. van der Lee, A. Chithran & K. Damodaran (2020). Acta Cryst. C76, 104-116.

Albofungin and chloroalbofungin: antibiotic crystals with 2D but not 3D isostructurality. W. Ye, W. She, H. H.-Y. Sung, P. Qian & I. D. Williams (2020). Acta Cryst. C76, 1100-1107.

A 35-year-old mystery solved: a facile synthetic route and structural confirmation of tetrachlorobis(diethyl ether)tungsten(IV). T. E. Shaw, A. P. Sattelberger & T. Jurca (2021). Acta Cryst. C77, 181-185.

Crystallographic study of the energetic salt 1,2,4-triazolium perchlorate. M. Kumasaki, S. Gontani, K. Mori, S. Matsumoto & K. Inoue (2021). Acta Cryst. C77, 197-201.

Crystal structure and photophysical properties of a novel polyoxomolybdate porphyrin. W.-T. Chen (2020). Acta Cryst. C76, 1062-1067.

A two-dimensional organic–inorganic lead iodide perovskite: poly[bis(3-fluorocyclobutylammonium) [di-μ-iodido-diiodidoplumbate(VI)]]. C.-R. Huang, P.-F. Li & X.-Z. Luo (2020). Acta Cryst. C76, 1096-1099.

Tolerance factor and phase stability of the garnet structure. Z. Song, D. Zhou & Q. Liu (2019). Acta Cryst. C75, 1353-1358.

Structure determination of a new cocrystal of carbamazepine and DL-tartaric acid by synchrotron powder X-ray diffraction. M. Guerain, P. Derollez, L. Roca-Paixão, C. Dejoie, N. T. Correia & F. Affouard (2020). Acta Cryst. C76, 225-230.

Synthesis, crystal structure and luminescence properties of a new samarium borate phosphate, CsNa₂Sm₂(BO₃)(PO₄)₂. D. Zhao, L.-Y. Shi, R.-J. Zhang & Y.-L. Xue (2020). Acta Cryst. C76, 1068-1075.

A tolbutamide–metformin salt based on antidiabetic drug combinations: synthesis, crystal structure analysis and pharmaceutical properties. L. Jia, S. Wu & J. Gong (2019). Acta Cryst. C75, 1250-1258.

Synthesis, structural characterization, and electronic structure of the novel Zintl phase Ba₂ZnP₂. A. Balvanz, S. Baranets & S. Bobev (2020). Acta Cryst. C76, 869-873.

Two new Cd^II MOFs of 1,4-bis(1H-benzimidazol-1-yl)butane and flexible dicarboxylate ligands: luminescence sensing towards Fe³⁺. F.-H. Zhao, S.-Y. Li, W.-Y. Guo, Z.-H. Zhao, X.-W. Guo, Y.-S. Li, S.-Q. Fan & Z.-L. Li (2020). Acta Cryst. C76, 1024-1033.

Removing the C-terminal protecting group enlarges the crystal size: Z–(Gly–Aib)₂–OH·H₂O. R. Gessmann, H. Brückner & K. Petratos (2020). Acta Cryst. C76, 1057-1061.

Structure and photophysical and electrochemical properties of a copper porphyrin complex with a three-dimensional framework. W.-T. Chen (2020). Acta Cryst. C76, 133-138.

Three coordination polymers built by quaternary-ammonium-modified isophthalic acid. L.-F. Wang, X.-G. Liu, M.-M. Meng, Y.-K. Xu, R. Zhu, R. Zhang, Z.-Z. Lu & W. Huang (2021). Acta Cryst. C77, 221-226.

Structural diversity among some dialkyltin(IV) benzoate and related derivatives. A. Linden & T. S. Basu Baul (2021). Acta Cryst. C77, 209-220.

A new crystalline form of αβ-D-lactose prepared by oven drying a concentrated aqueous solution of D-lactose. D. Nicholls, C. Elleman, N. Shankland & K. Shankland (2019). Acta Cryst. C75, 904-909.

Bond length of perchlorate at different temperatures: X-ray and neutron comparison. M. M. Olmstead (2020). Acta Cryst. C76, 159-163.

A five-coordinate iron(III) porphyrin complex including a neutral axial pyridine N-oxide ligand. M. A. Short, R. D. Sommer, A. J. Falzone, T. Huang, W. W. Weare & J. L. Roizen (2019). Acta Cryst. C75, 717-722.

Crystal structure and energetic features of the cocrystal of carbamazepine with 3,5-dinitrobenzoic acid. S. Pawlędzio, D. Trzybiński & K. Woźniak (2019). Acta Cryst. C75, 1150-1156.

A new heteroleptic phosphorescent cuprous complex supported by a BINAP ligand: synthesis, structure, luminescence properties and theoretical analyses. D.-D. Wang, J.-T. Wang, L. Song, Y.-Y. Wang & W.-X. Chai (2020). Acta Cryst. C76, 177-185.

Platinum(II) complex with 4-nitro-N-(pyridin-2-ylmethylidene)aniline: synthesis, characterization, crystal structure and antioxidant activity. M. Khalaj, A. Olyaei, M. Sadeghpour, A. Lalegani, J. Lipkowski & A. J. Lough (2020). Acta Cryst. C76, 1005-1009.

Solvent-assisted planar structure of a stilbene-based salicylhydrazone compound: crystal structure, solvent- and aggregation-induced emission, and switchable luminescence colouration. Z.-B. Fang, B. Zhang, Q.-Z. Yang, W. Zheng, X.-L. Hu, X.-H. Huang, C.-C. Huang, N.-F. Zhuang & S.-T. Wu (2020). Acta Cryst. C76, 734-740.

Polymorphism and photoluminescence properties of K₃ErSi₂O₇. P. Dabić, M. G. Nikolić, S. Kovač & A. Kremenović (2019). Acta Cryst. C75, 1417-1423.

Structural and enhanced hydrogen storage properties of the Li₁₂Mg₃Si₃Al phase. V. Pavlyuk, W. Ciesielski, D. Kulawik, N. Pavlyuk & G. Dmytriv (2021). Acta Cryst. C77, 227-234.

Synthesis, structure and photocatalytic degradation of organic dyes of a copper(II) metal–organic framework (Cu–MOF) with a 4-coordinated three-dimensional CdSO₄ topology. L.-L. Qian, Z.-X. Wang, H.-X. Tian, M. Li, B.-L. Li & H.-Y. Li (2019). Acta Cryst. C75, 1053-1059.

Multicomponent solid forms of the uric acid reabsorption inhibitor lesinurad and cocrystal polymorphs with urea: DFT simulation and solubility study. V. Palanisamy, P. Sanphui, M. Prakash & V. Chernyshev (2019). Acta Cryst. C75, 1102-1117.

Modified polyoxometalate: a novel monocapped bi-supporting and reduced α-Keggin structure {PMo₁₂O₄₀[Cu(2,2′-bpy)]}[Cu(2,2′-bpy)(en)(H₂O)]₂. Y.-K. Lu, Y.-P. Li, L.-Y. Yang, W.-H. Wang, Y. Pan, W.-F. Yan & Y.-Q. Liu (2019). Acta Cryst. C75, 1344-1352.

Crystal structure and DFT analyses of a pentacoordinated PCP pincer nickel(II) complex. V. Subramaniyan, A. Kumar, A. Govindaraj & G. Mani (2019). Acta Cryst. C75, 734-739.

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