Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 57| Part 10

ISSN: 2056-9890

October 2001 issue

Highlighted illustration

Cover illustration: This zinc porphyrin structure has been determined from a tiny crystal by use of synchrotron radiation. Molecules are linked by hydrogen bonding and [pi] stacking. See Bond et al. [Acta Cryst. E57, m454-m456].

inorganic compounds

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Ru₃Sn₇, a re-investigation

L. Eriksson and J. Lanner

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Hexagonal YbMnO₃ revisited

B. B. Van Aken, A. Meetsma and T. T. M. Palstra

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A new modification of diammonium hexafluorosilicate, (NH₄)₂SiF₆

J. Fábry, J. Chval and V. Petříček

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metal-organic compounds

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Dicarbonylbis(1,4-difluoro-2,3,5,6-tetramethyl-1,4-diboracyclohexa-2,5-diene)molybdenum

K. M. Anderson, E. P. Kündig, N. C. Norman, A. G. Orpen, J. A. J. Pardoe, D. W. Smith and P. L. Timms

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catena-Poly[[dicyanamidobis(3-hydroxypyridine-N)copper(II)]-μ-dicyanamido]

G. A. van Albada, I. Mutikainen, U. Turpeinen and J. Reedijk

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Heptacarbonyl-κ³C,2κ⁴C-{μ-dicyclohexyl[1(η⁵)-cyclopentadienyl]phosphine-2κP}molybdenumrhenium(Mo–Re)

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2-Propenyl 4-ferrocenyl-4-oxobutanoate

J. Giraldés, M. L. McLaughlin and F. R. Fronczek

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Bis(μ-1-acetimido-4-phenylpyrazolone-N²:O)-μ-oxo-tetraoxodimolybdenum(VI) as its diacetonitrile adduct: a novel dinuclear molybdenum complex bridged by a 1-acetimido-4-phenylpyrazolone ligand

S.-L. Guo, M. Wagner and M. Bolte

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Diaquabis(nicotinamide)bis(o-sulfobenzimidato-N)cadmium(II)

S. C˛akir, P. Naumov, İ. Bulut, E. Bic˛er, O. C˛akir, G. Jovanovski, I. A. Razak, S. Chantrapromma, H.-K. Fun and S. W. Ng

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[1,2-Bis(diphenylphosphino)ethane]dibromonickel(II) tetrahydrofuran solvate

S. Beaudoin, D. Zargarian, F. Bélanger-Gariépy and F.-G. Fontaine

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Dichlorobis(sarcosinato)zinc(II)

M. Subha Nandhini, R. V. Krishnakumar and S. Natarajan

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ansa-Calcocenes: rac-[bis(3,3′-biacenaphthylenido)]bis(tetrahydrofuran)calcium

P.-J. Sinnema, B. Twamley and P. J. Shapiro

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Aqua(N,N′-disalicylideneethylenediamino-N,N′,O,O′)(4,5-imidazoledicarboxylato-O)manganese(III) monohydrate

D.-G. Huang, X.-F. Zhang, H.-P. Zhu, C.-N. Chen and Q.-T. Liu

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[mer,trans-(NN′N)RuCl₂(NC₅H₅)]·C₇H₈ {NN′N = 2,6-bis-[(dimethylamino)methyl]pyridine}

S. Back, G. Rheinwald, I. del Río, G. van Koten and H. Lang

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Dinitratodioxobis(4-picoline N-oxide)uranium(VI)

C. E. F. Rickard

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Absolute configuration of Λ-(+)₅₈₉-tris(ethylenediamine)cobalt(III) triiodide monohydrate

R. Matsuki, M. Shiro, T. Asahi and H. Asai

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Square [Pd₄(μ-CN)₄(C₆F₅)₄(PEt₃)₄]·2C₆H₅CH₃

J. P. H. Charmant, P. Espinet and K. Soulantica

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Aqua{5,15-bis[4-(2-trimethylsilylacetylene)phenyl]-2,8,12,18-tetrakis(2-methoxycarbonylethyl)-3,7,13,17-tetramethyl-10,20-dioxoporphyrinato}zinc(II)

A. D. Bond, N. Feeder, S. J. Teat, Z. Clyde-Watson, N. Bampos and J. K. M. Sanders

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Low-temperature structure of a twinned crystal of tris(2,4-pentanedionato)(1,10-phenanthroline)samarium(III)

U. K. Urs, K. Shalini, T. S. Cameron, S. A. Shivashankar and T. N. Guru Row

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trans-Dichloro(meso-2,3,7,11,12-pentamethyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene-κ⁴N^3,7,11,17)rhodium(III) hexafluorophosphate

A. J. Blake, T. I. Hyde and M. Schröder

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Diaquabis(N,N-diethylnicotinamide)bis(2-hydroxybenzoato)zinc(II)

H. Necefoglu, W. Clegg and A. J. Scott

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Diaquabis(N,N-diethylnicotinamide)bis(4-nitrobenzoato)zinc(II)

H. Necefoglu, W. Clegg and A. J. Scott

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trans-Bis(1,4-butanediamine)dichlorocobalt(III) chloride monohydrate

K. Fujimoto, K. Nagata, H. Suzuki and K. Kanamori

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trans-Bis(1,4-butanediamine)bis(isothiocyanato)cobalt(III) thiocyanate

K. Fujimoto, K. Nagata, H. Suzuki and K. Kanamori

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Diaquabis(4-nitrobenzoato)zinc(II): a redetermination

H. Necefoglu, W. Clegg and A. J. Scott

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The unexpected fixation of CO₂ employing a Cu^IBr(bpy)₂ complex

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[5,15-Bis(4-pyridyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato]zinc(II) chloroform solvate

K. Y. Wild, B. Therrien, P. G. Plieger, D. L. Officer and A. K. Burrell

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Dichlorobis(triphenylphosphine oxide)zinc(II) tetrahydrofuran disolvate

A. Zeller, E. Herdtweck and T. Strassner

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Tetrakis(4-acetylpyridine)diisothiocyanatocobalt(II)

G. K. Patra and I. Goldberg

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Hexaaquanickel(II) bis(p-tolylsulfonate)

A. S. Batsanov, J. A. K. Howard, N. S. Moore and M. Kilner

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catena-Poly[[aqua(benzoato)(N,N′-dimethylformamide)calcium(II)]-μ-benzoato]

S. Yano, M. Numata, M. Kato, S. Motoo and T. Nishimura

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A heteroleptic tetranuclear copper amide/aryl complex: 1,4:2,3-bis(μ-2,4,6-trimethylphenyl-C,C)-1,2:3,4-bis[μ-bis(trimethylsilyl)amido-N,N]tetracopper(I)

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organic compounds

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(1R,6S,7R)-Himachal-2-ène-6,7-diol

H. E. Jamili, A. Auhmani, M. Dakir, A. Benharref, E. Kossareva and M. Pierrot

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(+)-(3R)-N-Hydroxy-2-[(S)-ethoxy(4-methoxyphenyl)phosphoryl]-1,2,3,4-tetrahydroisoquinoline-3-carboxamide

K. Kurokawa, N. Kanehisa, M. Sawa, H. Kondo and Y. Kai

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Cycloechinulin, a Trp-Ala-derived alkaloid from the fungus Aspergillus ochraceus

L. K. Hansen, F. C. Størmer, D. Petersen and A. J. Aasen

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2,5-Dinitro-7,9-dioxa-2,5-diazabicyclo[4.3.0]nonan-8-one

R. D. Gilardi and R. J. Butcher

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L-Phenylalanine–nitric acid (2/1)

N. Srinivasan, B. Sridhar and R. K. Rajaram

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2-Cyano-2′-nitrodiazoaminobenzene

J. G. O'Brien, K. E. Grousnick and R. G. Baughman

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β-Alaninium maleate

K. Rajagopal, R. V. Krishnakumar and S. Natarajan

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(1S,2S,3R,6S,7R)-3,6-Epoxyhimachalane-2,7-diol

H. El Jamili, A. Auhmani, M. Dakir, A. Benharref, E. Kossareva and M. Pierrot

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Diethylammonium diphenylphosphinate

H. Dorn, A. J. Lough and I. Manners

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Phenyl 2,4,6-tribromophenyl ether

L. Eriksson and J.-W. Hu

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Intermolecular N–H⋯O hydrogen-bonding interactions in 5-fluorocytosinium salicylate

P. Prabakaran, S. Murugesan, P. T. Muthiah, G. Bocelli and L. Righi

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11-Chloro-5,7-dihydro-6H-benzothiazolo[2,3-b]benzo[h]quinazoline

J. N. Low, J. Cobo, M. Nogueras, A. Sánchez, J. Quiroga and P. Hernández

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7-Acetoxy-4-(1-chloroethyl)coumarin

W. Errington, V. S. Parmar, A. Singh and I. Singh

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1,1,1,3,3,3-Hexafluoro-2-(4-nitrophenyl)-N-phenylisopropylamine

S. F. Pavkovic, D. W. Nelson and J. R. Owens

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A BONBON 6-membered ring heterocycle

W. Kliegel, L. Preu, U. Riebe, B. O. Patrick, S. J. Rettig and J. Trotter

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Acridinium isophthalate

Z. Shaameri, N. Shan and W. Jones

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Quinoline

J. E. Davies and A. D. Bond

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Octafluoronaphthalene–1,8-diaminonaphthalene (1/1)

A. S. Batsanov, J. C. Collings, J. A. K. Howard and T. B. Marder

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N,N′-Bis[(4-ethoxyphenyl)aminoacetyl]-4,5-dimethyl-o-phenylenediamine

R. Kruszynski, T. J. Bartczak and E. Mikiciuk-Olasik

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(Z)-2-Nitroethenamine

R. N. Evans and R. Gilardi

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(2SR,4RS)-(4-Iodo-5,5-dimethyl-2-hexylsulfonyl)benzene

G. J. Reiß and M. Masnyk

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(2R,4R)-(4-Iodo-5,5-dimethyl-2-hexylsulfonyl)benzene

G. J. Reiß and M. Masnyk

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Monoclinic form of 2-{5,5-dimethyl-3-[2-(2,4,6-trimethoxyphenyl)vinyl]cyclohex-2-enylidene}malononitrile

T. Kolev, Z. Glavcheva, M. Schürmann, D.-C. Kleb, H. Preut and P. Bleckmann

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Triclinic form of 2-{5,5-dimethyl-3-[2-(2,4,6-trimethoxyphenyl)vinyl]cyclohex-2-enylidene}malononitrile

T. Kolev, Z. Glavcheva, D. Yancheva, M. Schürmann, D.-C. Kleb, H. Preut and P. Bleckmann

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L-Phenylalaninium maleate

M. Alagar, R. V. Krishnakumar and S. Natarajan

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(R)-N-(1-Phenylethyl)quinoline-2-carboxamide

Q.-Y. Yang, Z.-Y. Zhou and J.-Y. Qi

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Pachypodol (4,5′-dihydroxy-3,3′,7-trimethoxyflavone)

G. Smith, E. Wang, J. P. Bartley and R. C. Bott

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2-Ethyl 5-methyl 3-hydroxythiophene-2,5-dicarboxylate

S. J. Coles, H. Guthmann, M. B. Hursthouse and P. J. Murphy

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(η⁶-Benzene)dichloro(diallylphenylphosphine)ruthenium(II), the first structurally characterized complex with the diallylphosphine ligand

S. B. Jensen and M. D. Spicer

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Ethyl 6-nitro-2-phenylaminoimidazo[1,2-a]pyridine-3-carboxylate

D. W. Jeffery, R. H. Prager and M. R. Taylor

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12-Benzoyl-2,3,5,6,9,10,11,12-octahydro-8H-1,4,7,12-benzotrioxaazacyclotetradecine

G. D. Fallon, T. Ventrice, W. R. Jackson, E. M. Campi and A. F. Patti

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3-(2-Bromophenyl)-4-(triisopropylsilyl)sydnone

D. A. Grossie, K. Turnbull and D. M. Krein

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N,N′-Bis(4-cyanopyridylidene)benzil dihydrazone

G. K. Patra and I. Goldberg

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1,5-Dichloro-3,6-diphenyl-3-azabicyclo[3.2.0]hept-6-ene-2,4-dione

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, B.-G. Zhao and J.-H. Xu

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Kudos

Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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