Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 57| Part 12

ISSN: 2056-9890

December 2001 issue

Highlighted illustration

Cover illustration: Radical cyclization of a 1,6-diene by a sulfonyl radical yields this highly substituted piperidine. In this enantiopure compound, one phenyl ring is face-to-face with the p-tolyl ring. See Reynoso-Paz, Olmstead, Kurth & Schore [Acta Cryst. E57, o1177-o1178].

inorganic compounds

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Copper(II) selenate pentahydrate, CuSeO₄·5H₂O

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Tb₂Mo₄O₁₅

H. Naruke and T. Yamase

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Zinc(II) sulfate tetrahydrate

A. J. Blake, P. A. Cooke, P. Hubberstey and C. L. Sampson

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Tripotassium hexahydrogen hexamolybdocobaltate(III) heptahydrate, K₃[H₆CoMo₆O₂₄]·7H₂O

U. Lee, H.-C. Joo, J.-S. Kwon and M.-A. Cho

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Redetermination of the mixed-valence manganese arsenate flinkite, Mn^II₂Mn^III(OH)₄(AsO₄)

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Refinement of pyrobelonite, PbMn^IIVO₄(OH), a member of the descloizite group

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metal-organic compounds

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A trigonal-bipyramidal coordinated ytterbium(III) alkyl: tris(trimethylsilylmethyl)bis(tetrahydrofuran-O)ytterbium(III)

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Hexakis(dimethyl sulfoxide)nickel(II) dinitrate dimethyl sulfoxide disolvate

A. J. Blake, M. Felloni, P. Hubberstey, M. Schröder and C. Wilson

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Metal–nucleobase interaction: dibromobis(cytosine)cadmium(II)

P. T. Muthiah, J. J. Robert, S. B. Raj, G. Bocelli and R. Ollá

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Quinolinium trichloro(quinoline)zinc(II)

W.-G. Wang, X.-F. Zhang, D.-G. Huang, H.-P. Zhu, C.-N. Chen and Q.-T. Liu

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Bis(2-naphthoxy)[5,10,15,20-tetra-p-tolylporphyrinato]tin(IV)

G. D. Fallon, M.A.-P. Lee and S. J. Langford

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Bis(dithioacetato-κ²S)bis(triphenylphosphine-κP)copper(I) 1.5-toluene solvate

T. C. Deivaraj and J. J. Vittal

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Bis(p-chlorothiophenolato)bis(tri-n-butylphosphine)nickel(II)

I. A. Guzei, M. J. Moloto and J. Darkwa

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[Indenyllithium·2(N,N,N′-trimethylethylenediamine)]_∞: N–H hydrogen bridges to the indenyl anion

G. Boche, B. Ledig, M. Marsch and K. Harms

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Diethylammonium heptabromidedicadmium(II)

R. D. Willett and B. Twamley

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Double cyclometallation of bis[3-(3-methoxyphenyl)pyrazol-1-yl]methane in a bis[(acetylacetonato)palladium(II)] complex

O. Juanes, J.-C. Rodriguez-Ubis and C. J. Pastor

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A solvated ytterbium diaryl: bis(1,1′:3′,1′′-terphenyl-C^2′)bis(tetrahydrofuran-O)ytterbium(II)

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Di-μ-chloro-bis{chloro[2-(4-methylphenylamino)-1,2-diphenylethanoximato]copper(II)}

H. Puschmann, J. A. K. Howard, B. Soto, R. Bonne and O. Au-Alvarez

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{[μ-N,N′-Bis(salicylidene)-2,2′-dimethyl-1,3-propanediamine](piperidine)copper(II)}dibromozinc(II)

I. Svoboda, C. Arıcı, H. Nazır, Z. Durmus, O. Atakol and H. Fuess

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Monoclinic form of dichlorobis(quinoline-N)cobalt(II)

W. Wang, D. Huang, H. Zhu, C. Chen and Q. Liu

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Diazido{N,N′-bis[2-(2-pyridyl)ethylene]-1,3-diaminopropane}nickel(II) monohydrate

D.-Z. Niu, B.-W. Sun, Z.-S. Lu, Z.-M. Wang and C.-H. Yan

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Tetraaqua(8-hydroxyquinoline-5-sulfonato-N,O)nickel(II) monohydrate

S. B. Raj, P. T. Muthiah, G. Bocelli and L. Righi

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Double cyclometallation of bis[3-(3-bromophenyl)pyrazol-1-yl]methane in the bis[acetylacetonatopalladium(II)] complex

O. Juanes, J.-C. Rodriguez-Ubis and C. J. Pastor

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Bis(acetato-O)diaqua(2,2′-bipyridyl-N,N′)cobalt(II) (OC-13): a two-dimensional material

R. Carballo, B. Covelo, E. García-Martínez and E. M. Vázquez-López

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Bis(triethanolamine-N,O,O′)zinc(II) disaccharinate

Y. Topcu, V. T. Yilmaz and C. Thöne

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(N,N-Diethyldithiocarbamato)(tricyclohexylphosphine)gold(I)

S. Y. Ho and E. R. T. Tiekink

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Aqua-di-μ₂-chloro-bis(diethylenetriamine)dicopper(II) dichloride

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organic compounds

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1,3,1′,3′-Tetrahydro-[2,2′]biindenylidene

J. Jovanovic, M. Schürmann, H. Preut and M. Spiteller

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2,4,6-Collidine

A. D. Bond and J. E. Davies

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4,5,4′,5′-Tetrakis(2-methyl-thiophen-3-yl)-[2,2′]bi[[1,3]dithiolylidene]

T. Gelbrich, S. J. Roberts-Bleming, M. Kalaji, P. J. Murphy and M. B. Hursthouse

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(±)-(1RS,2SR)-1,2-Bis(2′-methyl-3′-oxocyclohex-1′-enyl)-1,2-diphenylethane

H. Ibrahim, T. Bach and K. Harms

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1,5-Di-tert-butyl-3-hydroxy-7-methylene-1-azonia-5-azacyclooctane iodide

J. L. Flippen-Anderson, T. Axenrod, L. Qi and R. D. Gilardi

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D-Phenylglycinium perchlorate

S. Ramaswamy, B. Sridhar, V. Ramakrishnan and R. K. Rajaram

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1-[(2-Nitrophenyl)hydrazono]-1H-naphthalen-2-one (Pigment Orange 2) from powder data

A. V. Yatsenko, K. A. Paseshnichenko, V. V. Chernyshev and H. Schenk

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4-Chloro-2-(phenyldiazenyl)phenol from powder data: a form stable at room temperature

A. V. Yatsenko, K. A. Paseshnichenko and H. Schenk

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4-Chloro-2-(phenyldiazenyl)phenol from powder data: a form metastable at room temperature

A. V. Yatsenko, K. A. Paseshnichenko and H. Schenk

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A taxane diterpenoid from the needles of Taxus wallichiana

S. K. Chattopadhyay, A. Sharon, U. Yadav, S. Srivastava, V. K. Mehta and P. R. Maulik

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N,N′-Bis(2-methoxyphenyl)pyridine-2,6-dicarboxamide

Q. Y. Yang, Z. Y. Zhou and J. Y. Qi

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1,3-Bis(8-chlorotheophyllin-7-yl)propane: a molecule with no intramolecular stacking

P. R. Maulik, K. Avasthi, S. Sarkhel, A. Sharon, D. S. Rawat and C. Bal

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2-{5,5-Dimethyl-3-[2-(2-methoxyphenyl)vinyl]cyclohex-2-enylidene}malononitrile

T. Kolev, Z. Glavcheva, M. Schürmann, D.-C. Kleb, H. Preut and P. Bleckmann

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Tetraphenylphosphonium 7-phenylethynyl-8-phenyl-7,8-nido-dicarbadecahydroundecaborate(1–)

G. M. Rosair, F. H. Schmidt and A. J. Welch

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Tetra-n-butylammonium 7-phenylethynyl-8-phenyl-7,8-nido-dicarbadecahydroundecaborate(1−)

G. M. Rosair, F. H. Schmidt and A. J. Welch

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Chloral adduct of N-hydroxypiperidine

W. Kliegel, U. Riebe, B. O. Patrick, S. J. Rettig and J. Trotter

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2H-Chromene-2-thione

P. Munshi and T. N. G. Row

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An enantiopure bicyclic pentasubstituted piperidine

M. Reynoso-Paz, M. M. Olmstead, M. J. Kurth and N. E. Schore

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Hydrogen bonding patterns in trimethoprim sulfate trihydrate [trimethoprim = 2,4-diamino-5-(3,4,5-methoxybenzyl)pyrimidine]

P. T. Muthiah, B. Umadevi, N. Stanley, X. Shui and D. S. Eggleston

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5,5-Dihydroxy-1,3-dipropionyl-1,3-diazacyclohexane

R. D. Gilardi, T. Axenrod, J. Sun and J. L. Flippen-Anderson

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1,5-Diacetyl-7,7-dinitro-1,5-diazacyclooctan-3-one ethylene acetal

R. D. Gilardi, T. Axenrod, X.-P. Guan and J. L. Flippen-Anderson

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3β-Acétoxy nor-31-lanostène-7,11-dione

M. Daoubi, A. Benharref and M. Pierrot

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Styrene at 83 K

N. Yasuda, H. Uekusa and Y. Ohashi

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Styrene at 120 K

A. D. Bond and J. E. Davies

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(2S)-2-Hydroxy-2-[(2S,5R*)-5-(1-hydroxy-1-methylethyl)tetrahydrofuran-2-yl]-1-phenylethanone

M. E. Light and M. B. Hursthouse

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(2S)-1-(4-Fluorophenyl)-2-hydroxy-2-[(2S,5R)-5-(1-hydroxy-1-methylethyl)-tetrahydrofuran-2-yl]ethanone

M. E. Light and M. B. Hursthouse

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Orthorhombic form of 6-phenylhex-5-ene-2,4-dione

A. F. Arrieta and A. Mostad

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2,9,18-Trioxo-3,5,8,19-tetraaza-[5^5,13][11]metaphane monohydrate

T. H. Kim, S. Y. Yang, S. S. Lee, J. S. Kim and J. Kim

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2,5-Dichloroaniline, a monoclinic structure with a pseudo-tetragonal unit cell

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N—H⋯O and O—H⋯O hydrogen bonds in crystal engineering: trimethoprim hydrogen glutarate

J. J. Robert, S. B. Raj and P. T. Muthiah

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2-Chlorobenzoxazolo[3,2-b]isoquinolin-6-one

T. Ravishankar, K. Chinnakali, A. Senthilvelan, H.-K. Fun, V. T. Ramakrishnan, S. Chantrapromma, I. A. Razak and A. Usman

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trans-2-(2-Bromo-4-methylphenyloxy)cyclohexanol

T. Ravishankar, K. Chinnakali, K. Sriraghavan, V. T. Ramakrishnan, H.-K. Fun, S. Chantrapromma, I. A. Razak and A. Usman

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O,O-Diphenyl 2-methyl-1-(3-phenylthioureido)propanephosphonate

L. Chęcińska, M. Małecka, T. A. Olszak and Z. H. Kudzin

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O,O-Diphenyl 1-(3-phenylthioureido)ethanephosphonate

L. Chęcińska, M. Małecka, T. A. Olszak and Z. H. Kudzin

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erythro-2-(2,6-Dimethoxyphenoxy)-1-(3,4,5-trimethoxyphenyl)-1,3-propanediol

V. Langer and K. Lundquist

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Tri(2-thienyl)arsine oxide

H. Mahalakshmi, V. K. Jain and E. R. T. Tiekink

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2,3-Dihydroxybenzoic acid

N. Okabe and H. Kyoyama

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Intermolecular hydrogen bonding in (2S)-2-(1-oxo-1H-2,3-dihydroisoindol-2-yl)propanoic acid

J. F. Gallagher and C. Murphy

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Spiro[2-carbomethoxy-5-(4-methoxyphenyl)-3-phenylpyrrolidine-4,3′-chroman-4′-one]

M. N. Nissa, V. Rajakannan, M.-J. Kim and D. Velmurugan

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1,4-Benzenedimethanol

N. Shan and W. Jones

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8a-Ethyl 2-methyl (4aR,8aS)-3-oxoperhydro-2,8a-naphthalenedicarboxylate

H. Surya Prakash Rao, S. Rajamathe, S. Shanmuga Sundara Raj and H.-K. Fun

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3,6-Di-2-pyridyl-4-{[(2-pyridyl)carbonyldiazenyl](2-pyridyl)methyl}-1H-1,2,4,5-tetrazine: the proton-assisted hydrolysis product of 3,6-di-2-pyridyl-1,2,4,5-tetrazine (dptz)

L.-Y. Wang, C.-X. Du and Y.-Q. Fu

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5-(4-Chlorophenyl)-3-oxa-4-azatricyclo[5.2.1.0^2,6]dec-4-ene

A. Thiruvalluvar, V. Parthasarathi, V. Kabaleeswaran, S. S. Rajan, A. Nagarajan and M. K. Pillay

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2,6-Lutidine

A. D. Bond, J. E. Davies and A. J. Kirby

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Methyl 5-methyl-3,4-diphenyl-1H-pyrrole-2-carboxylate

M. E. Light, S. Camiolo, P. A. Gale and M. B. Hursthouse

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1-(2,6-Dimethylphenylamino)propane-1,2-dione dioxime

T. Hökelek, A. Zülfikaroğlu and H. Batı

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Redetermination of N,N-dimethyl-N-{4-[(E)-(4-methyl-3-nitrophenyl)diazenyl]phenyl}amine at 193 K: another example of dynamic disorder of substituted azobenzene compounds

O. Ya. Borbulevych and M. Yu. Antipin

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Photochemical formation of 2-acetyl-7-methylbenz[e]indole

A. Višnjevac, N. Basarić, B. Kojić-Prodić and M. Šindler-Kulyk

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(4R,5R)-2-(N-Methyl-benzylamino)-3-nitro-4-(1′,2′,3′,4′,5′-penta-O-acetyl-D-manno-pentitol-1-yl)-5-phenyl-5-phenylcarbamoyl-4,5-dihydrothiophene at 150 K

M. J. Diánez, M. D. Estrada, A. López-Castro and S. Pérez-Garrido

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2-Dihydroxymethyl-3H-benzoimidazol-1-ium chloride monohydrate

A. J. Blake, S. J. Hill and P. Hubberstey

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