Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 60| Part 2

ISSN: 2056-9890

February 2004 issue

Highlighted illustration

Cover illustration: The compound tris(quinolin-8-olato)gallium(III) is the gallium congener of the most widely used organic light-emitting diode material, Ga replacing Al in the tris-chelate octahedral complex. See Rajeswaran & Jarikov [Acta Cryst. E60, m217-m218].

inorganic compounds

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Er₃₆Pt_102−xSi₃₂ (x = 2.6), a new structure type of a ternary intermetallic silicide

A. I. Tursina, A. V. Gribanov, H. Noël, P. Rogl and Y. D. Seropegin

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Dirubidium tetrathiotungstate, Rb₂[WS₄]

J. Yao and J. A. Ibers

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La(NO₂)₃, a novel (3,9)-connected lanthanide-based network

Q.-Q. Kang, L.-S. Long, R.-B. Huang and L.-S. Zheng

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Calcium potassium cyclo-triphosphate

M. Sandström and D. Boström

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LiMn₂O₄: a spinel-related low-temperature modification

K. Tateishi, K. Suda, D. du Boulay, N. Ishizawa and S. Oishi

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A novel monoprotonated decavanadate, K₄Na[HV₁₀O₂₈]·10H₂O

U. Lee and H.-C. Joo

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ZnHg(AsO₄)(OH) with a descloizite-type structure

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metal-organic compounds

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Diamminediaquabis(4-pyridylthioacetato)copper(II)

Y.-Q. Huang, H. Zhang, J.-G. Chen, W. Zou, L. Li, Z.-B. Wei and S. W. Ng

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Tetraaquabis(4-pyridylthioacetato)nickel(II)

X.-M. Zhang, R.-Q. Fang, H.-S. Wu and S. W. Ng

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The dimer bis(μ-8-hydroxy-7-iodoquinoline-5-sulfonato-κ³N,O:O′)bis[triaquamagnesium(II)] tetrahydrate

S. Francis, P. T. Muthiah, U. Rychlewska and B. Warżajtis

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catena-Poly[[diaquazinc(II)-μ-benzene-1,3-dioxyacetate] dihydrate]

S. Gao, J.-R. Li, J.-W. Liu and L.-H. Huo

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Tetraaqua(2,2′-bipyridine)zinc(II) terephthalate

H. Xu, Y. Liang, Z. Su, Y. Zhao, K. Shao, H. Zhang and S. Yue

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Di-μ-ethoxy-bis[diethoxy(8-quinolinato)titanium(IV)]

M. M. Amini, M. Mirzaee and S. W. Ng

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Tris(8-hydroxyquinolinato-κ²O,N)oxoniobium(V) dichloromethane disolvate

M. M. Amini, M. Mirzaee, F. Yeganeh and S. W. Ng

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[N,N′-Bis(2-methoxycarbonyl-3-oxobutylidene)ethylenediaminato-κ⁴O,N,N′,O′]cobalt(II)

T. Akitsu, I. Iwakura, H. Tanaka, T. Ikeno, Y. Einaga and T. Yamada

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The rhombohedral polymorph of scandium formate

A. B. Ilyukhin and S. P. Petrosyants

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Bis[tris(2,2′-bipyridyl-κ²N,N′)iron(II)] cyclo-tetravanadate decahydrate

M.-H. Huang, L.-H. Bi and S.-J. Dong

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Poly[diaqua[μ-1,2-bis(4-pyridyl)ethene-κ²N:N′]tetrakis(μ-isonicotinato-κ²N:O)dicadmium(II)]

J.-H. Liao and C.-D. Ho

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Chlorobis[2-(2-pyridyl)ethanol]copper(II) chloride

S. Hamamci, V. T. Yilmaz and C. Thöne

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Carbonyldichlorohydridobis(triphenylphosphine)iridium(III)

J. P. H. Charmant, N. C. Norman, A. G. Orpen and G. R. Whittell

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Carbonyldichlorohydridobis(trimethylphosphine)iridium(III)

J. P. H. Charmant, N. C. Norman, A. G. Orpen and G. R. Whittell

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Bis[μ-2-benz(oxa/thia)zolyl-2-phenolato-κ³N,O:O]bis{bis[2-benz(oxa/thia)zolyl-2-phenolato-κ²N,O]zinc(II)}

Y.-P. Tong, X.-M. Chen and S. W. Ng

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catena-Poly[[aquamanganese(II)]-di-μ-4-pyridylthioacetato-κ⁶O,O′:N;N:O,O′]

X.-M. Zhang, R.-Q. Fang, H.-S. Wu and S. W. Ng

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Bis(3,5-dimethylpiperazinium) di-μ₅-hydrogenphosphato-penta-μ₂-oxo-pentakis[dioxomolybdenum(V)] dihydrate

X.-M. Zhang, R.-Q. Fang, H.-S. Wu and S. W. Ng

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A mononuclear cobalt(III) complex of the ligand N,N′-bis(pyridin-2-ylmethyl)pyrazine-2,3-dicarboxamide

D. S. Cati and H. Stoeckli-Evans

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A macrocyclic binuclear copper(II) complex of the ligand N,N′-bis(pyridin-2-ylmethyl)pyrazine-2,3-dicarboxamide

D. S. Cati and H. Stoeckli-Evans

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A neutral macrocyclic binuclear copper(II) complex of the deprotonated form of the ligand N,N′-bis(pyridin-2-ylmethyl)pyrazine-2,3-dicarboxamide

D. S. Cati and H. Stoeckli-Evans

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[Tris(2-aminoethyl)amine]manganese(II) heptasulfidotetraantimony(III) hemihydrate

M. Schaefer, D. Kurowski, A. Pfitzner, C. Näther and W. Bensch

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The absolute structure of tetrakis(trimethylphosphine)copper(I) dichlorocopper(I)

G. Margraf, H.-W. Lerner, M. Wagner and M. Bolte

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rac-[2,2′-Bis(1-ethylbenzimidazol-2-yl-κN³)biphenyl]dichloronickel(II)

R. T. Stibrany, M. G. Matturro, S. Zushma and A. O. Patil

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catena-Poly[[trimethyltin(IV)]-μ-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)-3-phenylpropionato-κ²O:O′]

M. Parvez, S. Ahmed, S. Ali, M. H. Bhatti and M. Mazhar

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The two-dimensional coordination polymer poly[[silver(I)-di-μ-1,5-bis(phenylsulfanyl)pentane] tetrafluoroborate]

M. Du and X.-J. Zhao

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Tetrakis(μ-2-bromobenzoato-κ²O,O′)bis[(N,N′-dimethylformamide)copper(II)], a new binuclear complex containing a metal–metal bond

Y.-L. Zhang, S.-W. Chen, W.-S. Liu and D.-Q. Wang

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A novel uranium-containing coordination polymer: poly[[aqua(benzene-1,3,5-tricarboxylato)dioxouranium(VI)] monohydrate]

L. A. Borkowski and C. L. Cahill

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Bis[μ-4-(diphenylphosphino)but-3-ene-2-thiolato]bis[bis(η⁵-cyclopentadienyl)zirconium(IV)] dichloromethane disolvate

E. Ortega, N. Pirio, P. Meunier and P. Richard

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A second tetragonal polymorph of bis(tetra-n-butylammonium) tetrakis[chloro(μ₃-sulfido)copper(I)]molybdate(VI)

N. R. Brooks, W. Clegg, M. H. Sadr, M. Esm-Hosseini and R. Yavari

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mer-Trichlorotris(dimethyl sulfide)ruthenium(III)

P. R. Bolton, W. Levason, G. Reid and M. Webster

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Hexaimidazolemanganese(II) terephthalate tetrahydrate

S.-Y. Niu, S.-S. Zhang, X.-M. Li, Y.-H. Wen and K. Jiao

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Diazidobis(2,2′-bipyridine)manganese(II)

Y.-Q. Cheng, M.-L. Hu, S.-R. Fan and W. Zhang

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Di-μ-phenylselenolato-bis[chloro(triphenylphosphine)palladium(II)]

M. S. Hannu-Kuure, R. Oilunkaniemi, R. S. Laitinen and M. Ahlgren

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Tris(quinolin-8-olato)gallium(III)

M. Rajeswaran and V. V. Jarikov

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Triaqua(dihydrogen 1,2,4,5-benzenetetracarboxylato)(1,10-phenanthroline)cobalt(II) monohydrate

M.-D. Ye, H.-P. Xiao, Y.-Q. Cheng and M.-L. Hu

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The arsenic(V) compound PhAs(O)(OH)(OSiPh₃)

G. Ferguson, B. J. O'Leary and T. R. Spalding

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Bis(μ-5-phenyltetrazolate-κ²N²:N³)bis[(2,2′-bipyridine-κ²N,N′)bis(5-phenyltetrazolate-κN²)copper(II)]

Z.-H. Shao, J. Luo, R.-F. Cai, X.-G. Zhou, L.-H.. Weng and Z.-X.. Chen

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Bis(triethanolamine-κ³N,O,O′)nickel(II) squarate

O. Z. Yeşilel, A. Bulut, İ. Uçar, H. İçbudak, H. Ölmez and O. Büyükgüngör

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Tris(tetraethylammonium) tris(μ₃-sulfido)bis[bromocopper(I)][dibromocopper(I)]oxomolybdate(VI) acetone solvate

A. Beheshti, N. R. Brooks, W. Clegg and R. Khorrmdin

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Bis(N,N-dimethylethylenediamine-κ²N,N′)bis(perchlorato-κO)copper(II)

T. Akitsu and Y. Einaga

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Diazidobis(2,2′-biimidazoline)nickel(II)

G. A. van Albada, A. Mohamadou, I. Mutikainen, U. Turpeinen and J. Reedijk

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Dichlorobis[N-(2-oxymethylphenyl)salicylideneiminato]diiron(III)

M. Koikawa, K. Iwashita and T. Tokii

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μ-Benzene-1,2,4,5-tetracarboxylato-bis[triaqua(2,2′-bipyridine)nickel(II)] dihydrate

X.-H. Li, H.-P. Xiao and M.-L. Hu

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Di-μ-chloro-bis[(2,2′:6,2′′-terpyridine-κ³N)copper(II)] diperchlorate: the triclinic polymorph

G. Gasser, G. Labat and H. Stoeckli-Evans

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α-Dichlorobis(2-phenylazo-4,6-dimethylpyridine)ruthenium(II) chloroform solvate

H. Kooijman, A. C. G. Hotze, S. E. Caspers, J. G. Haasnoot, J. Reedijk and A. L. Spek

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organic compounds

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3,7,17-Tri-O-acetyl-5-O-butanoyl-13,15-dihydroxymyrisinol

M. Parvez, V. U. Ahmad, J. Hussain, H. Hussain and U. Farooq

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n-Butyl hydrogen phthalate

M. Parvez, Sadiq-ur-Rahman, S. Ali and M. Mazhar

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Diethyl phenyl(4-pyridylcarbonylamino)methylphosphonate

H. Fang, J.-F. Wang, X.-X. Liu, Y.-F. Zhao and S. W. Ng

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5-Methyl-2-phenyl-4-[(Z)-(2-tolylamino)phenylmethylene]pyrazol-3(2H)-one

F. Bao, X. Lü, Q. Wu, B. Kang and S. W. Ng

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2,9-Bis(methoxymethyl)-1,3,8,10-tetrathiacyclotetradecane

Z. Gültekin, H. Bayrak, W. Frey and T. Hökelek

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3-Cyano-4,6-dimethyl-2-pyridone (Guareschi pyridone)

V. B. Rybakov, A. A. Bush, E. V. Babaev and L. A. Aslanov

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Benzoylmethyltriphenylphosphonium hydrogen maleate: supramolecular layer formation due to C—H⋯O interactions

M. Baby Mariyatra, E. C. Spencer, K. Panchanatheswaran and J. A. K. Howard

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(Z)-3-(3,4-Dimethoxyphenyl)-2-(2-methoxyphenoxy)-2-propenoic acid

V. Langer, S. Li, K. Lundquist and R. Stomberg

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3-(2,4-Dichlorophenyl)-1-(2-furyl)-3-hydroxypropan-1-one

Z. Yu, X. Gu, B. Zhao and X. Cao

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cis-7-Azabicyclo[4.2.0]octan-8-one

Gy. Argay, L. Fábián, A. Kálmán, G. Bernáth and Zs. Cs. Gyarmati

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cis-8-Azabicyclo[5.2.0]nonan-9-one

Gy. Argay, A. Kálmán, Gy. Bernáth and Zs. Cs. Gyarmati

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4-(4-Methylphenylazo)-2-allylphenol monohydrate

N. Karadayı, G. Turgut, M. Odabaşoğlu and O. Büyükgüngör

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4′-Methylazobenzene-2-sulfenyl cyanide

K. Sanjib, P. Kabita, P. Barman, D. Hazarika and S. K. Bhattacharjee

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(S)-N-Nitrosoazetidine-2-carboxylic acid

M. Gdaniec, M. J. Milewska and T. Połoński

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2,5,6-Trichloro-4-iodoisophthalonitrile

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{3-[(4-Chloroanilino)carbonyl]-2-[(3,4-dichlorophenyl)imino]-8-methyl-2H-pyrano[2,3-c]pyridin-5-yl}methyl acetate

S. M. Kovalenko, V. N. Baumer, I. O. Zhuravel and V. P. Chernykh

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4-[(3-Chlorophenyl)diazenyl]-6-methoxy-2-{[tris(hydroxymethyl)methyl]aminomethylene}cyclohexa-3,5-dien-1(2H)-one

B. Koşar, Ç. Albayrak, M. Odabaşoğlu and O. Büyükgüngör

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2-[2-(2,6-Dimethylphenylamino)phenylmethyleneamino]-1,3-diisopropylbenzene

H. Gao, Q. Wu and S. W. Ng

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1-Benzyl-3-(α-hydroxybenzylidene)pyrrolidine-2,4-dione

Y.-Q. Zhu, H.-B. Song, J.-R. Li, C.-S. Yao, F.-Z. Hu, X.-M. Zou and H.-Z. Yang

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O-(3,5-Dimethoxyphenyl) N,N-dimethylthiocarbamate

C. M. L. Vande Velde, H. J. Geise and F. Blockhuys

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4,6-Dimethyl-5-nitro-1H-pyridin-2-one

V. B. Rybakov, A. A. Bush, E. V. Babaev and L. A. Aslanov

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2-[Hydroxy(2-pyridyl)methyl]-2-cyclopenten-1-one: the Baylis–Hillman adduct of 2-pyridinecarboxaldehyde and 2-cyclopenten-1-one

F. Huo, C. Yin, W. Guo and C. Xia

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3,5-Bis(4-methylbenzoyl)-2,6-bis(4-methylphenyl)-4H-pyran-4-one

M. Dinçer, İ. Yıldırım, İ. Koca and N. Özdemir

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An orthorhombic polymorph of N,N′-bis(2-pyridylmethyl)pyrazine-2,3-dicarboxamide

D. S. Cati and H. Stoeckli-Evans

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Tetramethyl 1,2-bis(2-aminophenoxy)ethane-N,N,N′,N′-tetraacetate

M. Rademeyer, D. A. Barkhuizen and G. E. M. Maguire

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(R,R)-(–)-trans-1,4-Dioxaspiro[4,4]nonane-2,3-diylbis(diphenylmethanol)–N-allyl-N-propyl-3-oxocyclohexene-1-carboxamide (2/1)

S. Ohba and H. Miyamoto

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1,3-Bis(2-phenylethyl)benzimidazolium-2-dithiocarboxylate

M. Akkurt, S. Öztürk, H. Küçükbay, E. Orhan and O. Büyükgüngör

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1,3,5-Tribromo-2,6-dihydroxybenzene

P. Kirsop, J. M. D. Storey and W. T. A. Harrison

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2-Chloroethyl ethyl sulfide: a mustard gas analogue

A. Zawadski and S. Parsons

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2-Chloro-3-chloromethylbenzo[h]quinoline

A. Beghidja, A. Benboudiaf, C. Beghidja and R. Welter

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6-Methoxy-5-(phenyldiazenyl)salicylaldehyde

C. C. Ersanlı, M. Odabaşoğlu, Ç. Albayrak and A. Erdönmez

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(2S)-[(2S)-2-Hydroxy-2-phenylethanoyloxy]phenylacetic acid

R. K. Mughal, R. G. Pritchard and R. J. Davey

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C—H⋯O and C—H⋯π(arene) interactions in (2S,4S,5R)-(–)-2-(4-propoxyphenyl)-3,4-dimethyl-5-phenyl-1,3-oxazolidine

M. Duffy, J. F. Gallagher and A. J. Lough

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(1RS,3aSR)-1-(chloromethyl)-1λ⁵-phospha-2,6a-diazaperhydropentalene 1-oxide dihydrate

D. Chen, P. Zhong, J. Ding and C. Yuan

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5-Chloro-2-benzofuran-1,3-dione

Z. S. Jin, W. X. Wang, W. X. Hu, Z. Y. Yang, H. W. Chen and R. C. Xuan

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4-Amino-2,6-dichloro-5-nitropyrimidine

D. McKeveney, R. J. Quinn, C. O. Janssen and P. C. Healy

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5-Chloro-6-(2-fluorobenzoyl)-1,3-benzoxazol-2(3H)-one

A. Aydın, T. Önkol, M. Akkurt, O. Büyükgüngör and S. Ünlü

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4-[(4-Methylphenyl)diazenyl]-6-methoxy-2-{[tris(hydroxymethyl)methyl]aminomethylene}cyclohexa-3,5-dien-1(2H)-one

B. Koşar, Ç. Albayrak, M. Odabaşoğlu and O. Büyükgüngör

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2-(4-Methylphenyl)-1,1-diphenylethene

C. M. L. V. Vande Velde, C. Wuyts, H. J. Geise and F. Blockhuys

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(1-Benzylpiperidin-4-ylidene)acetonitrile

M. Li, C. Yin and P. Yang

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4-[(4-Chlorobenzylidene)amino]phenol

C. Kazak, M. Aygün, G. Turgut, M. Odabaşoğlu, O. Büyükgüngör and N. Kahveci

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4-(4-Benzyloxyphenoxy)phthalonitrile

N. Karadayı, Ş. Işık, N. Akdemir, E. Ağar and M. Özil

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4-(Anthracen-9-ylmethoxy)phthalonitrile

H. Petek, Ş. Işık, N. Akdemir, C. Kantar, E. Ağar and İ. Şenel

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A new sydnone structure: 4-(phenylamino)sydno[3,4-a]quinoxaline

G. B. Riddle, D. A. Grossie and K. Turnbull

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4-Ammonio-5-chloro-N-[2-(N,N-diethylammonio)ethyl]-2-methoxybenzamide sulfate

C. R. Girija and N. S. Begum

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N,N,N′,N′-Tetrakis(2-pyridylmethyl)-1,2-diaminoethane: a multidentate ligand

T. Fujihara, M. Saito and A. Nagasawa

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2-[2-(Hydroxymethyl)phenyliminomethyl]phenol

C. C. Ersanlı, M. Odabaşoğlu, Ç. Albayrak and A. Erdönmez

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Benzyl(1,1-dimethyl-3-oxobutyl)ammonium iodide

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(S)-Alanine–(S)-mandelic acid (1/1)

Z.-Q. Hu, D.-J. Xu and Y.-Z. Xu

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D-Phenylglycinium nitrate

K. Bouchouit, L. Bendheif and N. Benali-Cherif

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N,N′-Dibenzyl-4,7-phenanthrolinium dibromide methanol solvate

M. M. Olmstead, J. T. Suri and B. Singaram

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N-[2-(Hydroxymethoxyboryl)benzyl]-4,7-phenanthrolinium bromide methanol solvate

M. M. Olmstead, J. T. Suri and B. Singaram

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(11R)-(–)-N,N′-Dimethylcinchonidinium diiodide

N. Yoshikawa, K. Takemoto, J. Sakamoto, N. Kanehisa, Y. Kai, H. Takashima and K. Tsukahara

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Methyl 6-amino-5-cyano-2-methoxycarbonylmethyl-4-phenyl-4H-pyran-3-carboxylate

S. Öztürk, M. Akkurt, E. Stoyanov, O. Büyükgüngör and D. Heber

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4-(2-Methoxy-1-naphthylmethoxy)phthalonitrile

Y. Köysal, Ş. Işık, N. Akdemir, E. Ağar and C. Kantar

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(2R,4S,5R)-3,4-Dimethyl-5-phenyl-2-[4-(trifluoromethyl)phenyl]-1,3,2-oxazaphospholidine(P—B)borane

M. J. Johansson, N. Kann and K. Larsson

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4′-(Dimethylamino)-4-nitroazobenzene

H. Adams, R. W. K. Allen, J. Chin, B. O'Sullivan, P. Styring and L. R. Sutton

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1-{2-[4-(2,4-Dinitrophenyl)piperazin-1-yl]ethyl}-4-aza-1-azoniabicyclo[2.2.2]octane chloride

W. Clegg, B. T. Golding, R. W. Harrington and R. Scott

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5-Benzyl-7,9-dimethoxy-3-phenyl-5H-pyrazolo[4,3-c]quinolin-1-ium chloride acetic acid solvate

V. N. Baumer, O. V. Silin, T. I. Savchenko, V. M. Nikitchenko and S. M. Kovalenko

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1-(2,4-Dichlorophenyl)-2-phthalimidoethanone

X. Zhang, P. Zhong, M. Hu and H. Xiao

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1-Cyclohexylmethoxymethyl-5-[2-hydroxy-1-(hydroxymethyl)ethylamino]cyclohexane-1,2,3,4-tetraol

H. Zhang, W.-F.. Li, K.-W. Wang and Y. J. Pan

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1,2-Bis(carbazol-9-ylmethylene)-3,4-diphenylcyclobutane

R. I. Zubatyuk, O. I. Kharanenko, O. V. Shishkin, V. I. Dulenko and A. V. Kibalny

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C—H⋯π interactions in 4,5-bis(2-isopropyl-5-methylphenoxy)phthalonitrile

Ş. Atalay, U. Çoruh, N. Akdemir and E. Ağar

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N-(4-Methyl-1-piperazinyl)phthalimide

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2-(2,2,2-Trifluoroacetylamino)pyridin-3-yl trifluoromethanesulfonate

X. Huang, H. Liu, X. Hu and S. W. Ng

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Ethyl phenylsulfonylacetate

J.-C. Ding, W.-K. Su, H.-Y. Wu, M.-C. Liu and S. W. Ng

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6-Hydroxymexicanolide

K. Chantrapromma, N. Saewan, H.-K. Fun, S. Chantrapromma and A. A. Rahman

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3-Methyl-3-pyrazolin-5-one

Z. Zhang, S. Jin, S. Wang, B. Liu and J. Guo

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Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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