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Figure 1 Single-crystal X-ray structure (top view) of (TEA)2[Cu(12—MCCuIIN(shi)-4)](DMF)2 (1). The thermal ellipsoid plot of 1 is at a 50% probability level with the disordered portions of the molecule shown only at the higher occupancy positions. All non-carbon atoms are labeled. Hydrogen atoms and the lattice TEA have been omitted for clarity (symmetry operator (i): −x + 1, −y + 1, −z + 1). Color scheme for all figures: orange - CuII, red - oxygen, blue - nitrogen, and gray - carbon. |