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Figure 1 Synthesis of the title compound 3. Reagents and conditions: (i) 2 eq Li[AlH4], Et2O, −78°C to room temperature, 1.5 h; (ii) 3 eq [Cp2ZrCl2], Et2O, room temperature, 12 h.

Journal logoCRYSTALLOGRAPHIC
COMMUNICATIONS
ISSN: 2056-9890
Volume 69| Part 10| September 2013| Pages m534-m535
doi:10.1107/S1600536813023933
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