Crystal structure of (3S*,4R*)-4-fluoro-3-(4-meth­oxy­phen­yl)-1-oxo-2-phenyl-1,2,3,4-tetra­hydro­iso­quinoline-4-carb­oxy­lic acid

Lehmann, A.; Lechner, L.; Radacki, K.; Braunschweig, H.; Holzgrabe, U.

doi:10.1107/S2056989017007186

Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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Figure 2
Synthesis scheme to obtain the fluorinated cis-enantiomers (±) 6. Reagents and conditions: (a) absolute THF, DMAP, di-tert-butyl dicarbonate, r.t., 24 h; (b) absolute THF, LiHMDS, NFSI, 201 K–r.t., 42 h; (c) CH₃CN, 85% (w/w) H₃PO₄, 323 K, 4 d.

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 73| Part 6| June 2017| Pages 867-870

https://doi.org/10.1107/S2056989017007186

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