research communications
Synthesis and crystal structures of two new tin bis(carboranylamidinate) complexes
aChemisches Institut der Otto-von-Guericke-Universität Magdeburg, Universitätsplatz 2, 39106 Magdeburg, Germany, and bETH Zurich, Laboratory for Inorganic Chemistry, Vladimir-Prelog-Weg 1-5/10, 8093, Zurich, Switzerland
*Correspondence e-mail: frank.edelmann@ovgu.de
Reaction of 2 equiv. of the lithium carboranylamidinate Li[o-(C2H10B10)C(NCy)(NHCy)] with SnCl2 in THF afforded the stannylene compound bis(N,N′-dicyclohexylamidinatocarboranate)tin(II), SnII[o-(C2H10B10)C(NCy)(NHCy)]2 (1). A similar reaction of SnCl4 with 2 equiv. of Li[o-(C2H10B10)C(NiPr)(NHiPr)] unexpectedly afforded the known solvated pentachloridostannate(IV) salt [Li(THF)4][SnCl5(THF)] as the main reaction product. Small amounts of the new chlorido-tin(IV) bis(carboranylamidinate) bis(N,N′-diisopropylamidinatocarboranate)chloridotin(IV), SnIVCl[o-(C2H10B10)C(NiPr)(NHiPr)][o-(C2H10B10)C(NiPr)2] (2), were isolated as a by-product. Single-crystal X-ray structure analysis revealed a κC,κN-chelating coordination of the carboranylamidinate ligands in both 1 and 2. The Sn atom in 1 adopts a pseudo-trigonal–bipyramidal coordination under participation of a stereoactive lone pair. In 2, a trigonal–bipyramidal coordination of Sn is completed by a chlorido ligand.
Keywords: crystal structure; carborane; amidinate; carboranylamidinate; tin.
1. Chemical context
Amidinates of the general formula [RC(NR′)2]− are the nitrogen analogs of carboxylate anions. These versatile N,N′-chelating ligands form stable coordination compounds with nearly every metallic element in the Periodic Table. In view of this rich coordination chemistry, amidinate ligands are frequently regarded as `steric cyclopentadienyl equivalents'. Metal complexes comprising amidinato ligands are readily available by insertion of the 1,3-diorganocarbodiimide, R–-N=C=N—R, into an M—C bond of an organometallic precursor compound. Another common synthetic route involves salt metathetical reactions between lithium amidinates and metal halides (Collins, 2011; Edelmann, 2008, 2013a,b). Metal amidinates comprising small alkyl substituents are often surprisingly volatile and may serve as useful precursors for metal oxides and nitrides by means of ALD (atomic layer deposition) or MOVCD (metal–organic chemical vapor deposition) processes (Devi 2013; Lim et al., 2003; Li et al., 2005).
A key advantage of the amidinate anions [RC(NR′)2]− is the fact that the substituents R and R′ attached to the N–C–N unit can be varied in many ways. With R = ortho-C2H11B10 (`ortho-carboranyl') we introduced a sterically demanding and chemically versatile moiety in the backbone of the amidinate ligand. are of tremendous scientific and technological interest due to their various applications ever since their discovery in the 1960′s. These applications include the synthesis of polymers and ceramics, catalysts, radiopharmaceuticals and non-linear optics, as well as the BNCT (= boron neutron capture therapy) technique (Belmont et al., 1989; Brown et al., 1992; Felekidis et al., 1997; Murphy et al., 1993; Teixidor et al., 1996; Vaillant et al., 2002). The first ortho-carboranylamidinate ligand [o-(C2H10B10)C(NiPr)(NHiPr)]− (= [HLiPr]−) was synthesized in our lab in 2010 by in situ lithiation of the parent o-carborane, ortho-C2H12B10 (= ortho-dicarba-closo-dodecaborane), followed by treatment with 1 equiv. of N,N′-diisopropylcarbodiimide (Dröse et al., 2010) as shown in Fig. 1. Subsequent reactions of the so-obtained lithium ortho-carboranylamidinate Li[HLiPr] or the related Li[HLCy] with various metal and non-metal chlorides have been reported by us and others to yield carboranylamidinates of e.g. SnII and CrII, RhI and IrI, FeII and FeIII, TiIV, ZrIV, Si and P (Harmgarth et al., 2014; Hillebrand et al., 2014; Yao et al., 2011, 2012, 2013; Xu et al., 2014). In all of these compounds, the ligand adopts a specific κC,κN-chelating mode instead of the κN,κN′-chelating mode usually observed for simple amidinate ligands (Collins, 2011; Edelmann, 2008, 2013a,b). In the case of the carboranylamidinates [HLR]− (R = iPr, Cy), a proton is formally shifted from the carborane C atom to the amidinate unit, resulting in an amidine moiety that usually acts as a monodentate donor functionality as shown in Fig. 2a.
In some cases, subsequent deprotonation of the NH functionality results in formation of a formally dianionic ligand [LR]2–, whose favored coordination mode is still κC,κN (Fig. 2b). Derivatives of Si, P, Ge, SnII, SnIV, FeII and FeIII, RhI and IrI containing this ligand system have been prepared by double lithiation of the parent ortho-carboranylamidine followed by treatment with appropriate element chloride precursors (Yao et al., 2011; Harmgarth et al., 2014, 2017), or through spontaneous of in situ formed [HLR]− to [LR]2– and free carboranylamidine H2LR. The latter reaction has been found to be favored in the case of strongly Lewis-acidic metal precursors, namely Cp2TiCl2, Cp2ZrCl2 and various chlorosilanes (Harmgarth et al., 2014, 2017). While dichlorosilanes R2SiCl2 react with Li[HLiPr] readily to form R2Si[LiPr]-type products, we recently found that for the heavy group 14 analogues Sn and Pb the formation of R2ECl[HLiPr]-type products is much more preferred (Harmgarth et al., 2017).
Among the known carboranylamidinate complexes are only very few compounds with more than one carboranylamidinate ligand per metal atom, and these are exclusively of the type M[HLR]2 (M = SnII, CrII, Dröse et al., 2010; M = CoII, NiII, CuII, Yao et al., 2012; M = FeII, FeIIICl, Hillebrand et al., 2014). We report here the formation and structural characterization of two new tin bis(carboranylamidinate) complexes, namely SnII[o-(C2H10B10)C(NCy)(NHCy)]2 (= Sn[HLCy]2; 1) and SnIVCl[o-(C2H10B10)C(NiPr)(NHiPr)][o-(C2H10B10)C(NiPr)2] (= SnCl[LiPr][HLiPr]; 2). Compound 2 is the first carboranylamidinate complex containing both mono- and dianionic carboranylamidinate ligands in a single molecule.
The mono-lithio-ortho-carboranylamidinate precursors Li[HLCy] and Li[HLiPr] were readily available following a published procedure by reaction of the mono-lithiated o-carborane Li-o-C2B10H11 with a stoichiometric amount of the carbodiimides iPrN=C=NiPr or CyN=C=NCy, respectively, in THF (cf. Fig. 1) (Harmgarth et al., 2014). In a first experiment, reaction of Li[HLCy] with 0.5 equiv. of SnCl2 in THF afforded the stannylene compound Sn[HLCy]2 (1) as colorless, block-like single crystals after recrystallization from toluene. The low isolated yield of ca 20% can be traced back to the very high solubility of 1 even in non-polar organic solvents. In addition to the X-ray diffraction study, compound 1 was also characterized through elemental analysis and the usual set of spectroscopic methods. In the IR spectrum, a characteristic ν(NH) band at 3423 cm−1 confirmed the presence of monoanionic [HLCy]− ligands. The NH functionalities were also observed in the 1H NMR spectrum through a broad singlet at δ 4.50 ppm. A single 119Sn NMR resonance at δ −46 ppm was in agreement with the formation of a single Sn-containing species. The of 1 showed the molecular ion at m/z 818 with 27% relative intensity.
A similar reaction of SnCl4 with 2 equiv. of Li[HLiPr] was carried out with the aim of synthesizing the hitherto unknown tin(IV) bis(carboranylamidinate) Sn[LiPr]2. Cooling of the reaction mixture afforded a fairly large amount of well-formed, colorless crystals, which turned out to be the known solvated pentachloridostannate(IV) salt [Li(THF)4][SnCl5(THF)]. This compound was first prepared and structurally characterized by Junk & Leary (2000). From the concentrated mother liquid of the pentachloridostannate salt, only a small amount (ca 5% isolated yield) of the unexpected tin(IV) carboranylamidinate SnCl[LiPr][HLiPr] (2) could be obtained. The X-ray determination of 2 revealed the presence of the first complex containing both a mono- and a dianionic carboranylamidinate ligand in one molecule. As in 1, the IR spectrum of 2 showed a characteristic ν(NH) band at 3410 cm−1. Elemental analysis and a single resonance in the 119Sn NMR spectrum (δ 290 ppm) confirmed the purity of 2. In the the molecular ion was observed at m/z 692 with 47% relative intensity.
2. Structural commentary
The molecular structures of the title compounds 1 and 2 are illustrated in Figs. 3 and 4, respectively. In both cases, two carboranylamidinate ligands are attached to one Sn atom in a typical κC,κN-chelating mode. In the tin(II) complex Sn[HLCy]2 (1), the coordination of the metal atom can be described as pseudo-trigonal–bipyramidal, with the two N atoms defining the axial positions [N1—Sn—N3 157.76 (4)°]. The two Sn-C bonds are situated in the equatorial plane [C3—Sn—C18 100.12 (5)°], together with the stereoactive lone pair at Sn. The bite angles of the [HLCy]− ligands are 72.01 (5)° (N1—Sn—C3) and 73.27 (5)° (N3—Sn—C18). The coordination geometry of the Sn atom therefore resembles that in the related tin(II) bis(carboranylamidinate) Sn[HLiPr]2 [N—Sn—N 161.4 (1), C—Sn—C 97.0 (1), N—Sn—C 73.03 (7)°; Dröse et al., 2010]. In 1, the Sn—C bond lengths are very similar at 2.311 (2) Å (Sn—C3) and 2.325 (2) Å (Sn—C18), while the difference in the Sn—N bond lengths is larger [Sn—N1 2.556 (1) and Sn—N3 2.469 (1) Å]. These values are in the same range as those observed in the isopropyl substituted analogue Sn[HLiPr]2 [Sn—C 2.318 (2), Sn—N 2.497 (2) Å].
The tin(IV) complex SnCl[LiPr][HLiPr] (2) is structurally closely related to 1, as the Sn atom exhibits a trigonal–bipyramidal coordination with the two amidinate N atoms in the axial positions [N1—Sn—N3 176.3 (1), C2—Sn—C11 124.3 (1), N1—Sn—C2 82.9 (1), N3—Sn—C11 77.7 (1)°]. The lone pair at Sn is formally replaced by a chlorido ligand, which is almost perpendicular to the Sn—N bonds [Cl—Sn—N1 95.78 (8), Cl—Sn—N3 87.93 (7)°]. The Sn—C bond lengths are 2.160 (3) Å (Sn—C2) and 2.154 (3) Å (Sn—C11) and therefore considerably shorter than in compound 1. This finding can be traced back to the higher of the Sn atom. Similar Sn—C bond lengths have been observed in the related tin(IV) derivatives SnCl3[HLiPr] [Sn—C 2.132 (3) Å] and SnCl2[LiPr](THF) [2.130 (2) Å; Harmgarth et al., 2017]. Since the values for protonated [HLiPr]− ligands and deprotonated [LiPr]2– ligands are virtually equal, the Sn—C(carborane) bond is obviously not noteworthily influenced by the bonding situation within the amidinate moiety. In contrast, in 2 the Sn—N contact to the deprotonated carboranylamidinate ligand [Sn—N1, 2.076 (3) Å] is considerably shorter than that to the protonated ligand [Sn—N3, 2.250 (3) Å]. As has been discussed previously, the M—N contact in [LiPr]2– complexes can be regarded as a distinct single bond, while the M—N contact in [HLiPr]− complexes should be described as a secondary coordinative interaction (cf. Fig. 1, SnCl3[HLiPr]: Sn—N 2.255 (3) Å, SnCl2[LiPr](THF): Sn—N 205.0 (2) Å; Harmgarth et al., 2017).
This bonding model is confirmed by the C—N bond lengths within the amidinate group. In 1, the C—N bonds to the tin-attached N atoms [C1—N1 1.284 (2), C16—N3 1.293 (2) Å] are clearly in the range of double bonds, while the C—N bonds to the protonated N atoms [C1—N2 1.354 (2), C16—N4 1.347 (2) Å] can be regarded as single bonds. These values are consistent with those observed in other tin complexes with [HLR]− ligands (e.g. Sn[HLiPr]2: C=N(Sn) 1.287 (3), C—N(H) 1.347 (4) Å; Dröse et al., 2010; SnCl3[HLiPr]: C=N(Sn) 1.288 (4), C—N(H) 1.339 (4) Å; Harmgarth et al. 2017). A comparable bond distribution is given in the protonated amidinate moiety in 2, however the difference is less pronounced in this case [C12—N3 1.304 (5), C12—N4 1.328 (5) Å]. The π electron density within the amidinate group in the [LiPr]2– ligand in 2 is clearly inverted, resulting in a long C—N(Sn) bond [C3—N1 1.372 (4) Å] and a short C=N bond to the non-coordinated N atom [C3—N2 1.269 (5) Å]. Similar values have been obtained in SnCl2[LiPr](THF) [C—N(Sn) 1.378 (3), C—N(free) 1.260 (3) Å; Harmgarth et al., 2017). Besides protonation, the bonding situation within the amidinate group might be affected by the other ligands around the Sn atom, while the of tin has apparently no influence.
In summarizing the results reported here, in tin carboranylamidinates a trigonal–bipyramidal (SnIV) or pseudo-trigonal–bipyramidal (SnII) coordination is highly preferred. Since the [HLR]− and [LR]2– ligands always display a typical κC,κN-chelating mode, this may explain why the formation of the complex SnCl[LiPr][HLiPr] (2) is preferred over a homoleptic complex Sn[LiPr]2, where the Sn atom would be tetrahedrally coordinated. Nonetheless, the example of SnCl2[LiPr](THF) (Harmgarth et al., 2017) demonstrates that penta-coordination of the Sn atom can also be completed by a coordinating solvent. Consequently, related bis(carboranylamidinate) complexes Sn[LiPr]2(solv.) (solv. = solvent) might exist.
3. Supramolecular features
In both 1 and 2, the molecules are well separated in the crystal and no unusually short intermolecular contacts have been observed. The shortest intermolecular contacts are found between cyclohexyl groups and carborane backbones in 1 [B5⋯C14 3.727 (3) Å] and between isopropyl groups in 2 [C5⋯C15 3.670 (7) Å], respectively. In both compounds, the free N—H groups are not involved in hydrogen bonding.
4. Database survey
For reviews on amidinate complexes, see: Collins (2011)' Edelmann (2008, 2013a).
For reviews and articles on et al. (1989); Brown et al. (1992); Felekidis et al. (1997); Murphy et al. (1993); Teixidor et al. (1996); Vaillant et al. (2002).
and their various applications, see: BelmontFor reviews on the chemistry of carboranylamidinates, see: Edelmann (2013b); Yao & Jin (2013).
For other structurally characterized tin carboranylamidinate complexes, see: e.g. Cambridge Structural Database (CSD; Groom et al., 2016) depository numbers 791890 (Dröse et al., 2010), 963128 (Harmgarth et al., 2014), 1536241–1536243 and 1536248 (Harmgarth et al., 2017). For crystal structures of bis(carboranylamidinate) complexes of other metals, see depository numbers 791889 (Cr; Dröse et al., 2010), 908987–908990 (Co, Ni and Cu; Yao & Jin, 2012), 986277 and 986278 (Fe; Hillebrand et al., 2014).
5. Synthesis and crystallization
All operations were performed under an argon atmosphere using standard Schlenk techniques. THF and toluene were distilled from sodium/benzophenone under argon. NMR spectra were recorded on a Bruker DPX400 (1H: 400 MHz) spectrometer in THF-d8 at 295 (2) K. 1H and 13C NMR shifts are referenced to Si(CH3)4, 119Sn shifts to Sn(CH3)4 (each δ = 0 ppm). IR spectra were measured on a Bruker Vertex V70 spectrometer equipped with a diamond ATR unit, electron impact mass spectra on a MAT95 spectrometer with an of 70 eV. Elemental analyses (C, H and N) were performed using a VARIO EL cube apparatus.
Preparation of Sn[HLCy]2 (1): o-Carborane (1.0 g, 7.0 mmol) in THF (50 mL) was deprotonated with n-butyllithium (7.0 mmol, 4.4 mL of a 1.6 mol l−1 solution in hexanes), followed by addition of a stoichiometric amount of the carbodiimide CyN=C=NCy (1.44 g, 7.0 mmol). The resulting solution of Li[HLCy] was treated in situ with SnCl2 (0.66 g, 3.5 mmol) and then stirred for 24 h. The solvent was subsequently removed in vacuo, the solid residue extracted with toluene (40 mL) and the insoluble matter filtered off. The filtrate was concentrated to a total volume of ca 10 mL. Cooling to 278 K for 2 d afforded colorless, block-like single-crystals of 1. Yield: 0.58 g (20%). Analysis calculated for C30H66B20N4Sn, M = 817.81 g mol−1: C 44.06, H 8.13, N 6.85%. Found: 43.66, H 8.00, N 6.25%. IR: ν 3423 w (ν NH), 2935 m (ν CH2), 2854 m (ν CH2), 2560 m (ν BH), 1623 m (ν C=N), 1448 m (δ CH2) cm−1. 1H NMR (400.1 MHz, THF-D8, 295 (2) K): δ 4.50 (s br, 2H, NH), 3.24 (m, 4H, CH Cy), 1.70–2.80 (m br, 20H, BH), 1.08–1.98 (m, 40H, CH2 Cy) ppm. 13C NMR (100.6 MHz, THF-D8, 295 (2) K): δ 143.0 (NCN), 80.3 (C—Sn), 77.0 (C—CN2), 54.6 (CH Cy), 34.8 (CH2 Cy), 25.7 (CH2 Cy), 25.4 (CH2 Cy), 25.1 (CH2 Cy), 25.0 (CH2 Cy) ppm. 119Sn NMR (149.2 MHz, THF-D8, 295 (2) K): δ −46 ppm. MS: m/z (%) 818 (27) [M]+, 467 (19) [C15H32B10N2Sn]+, 350 (24) [C15H32B10N2]+, 269 (100) [C9H23B10N2]+, 143 (54) [C2H10B10]+.
Preparation of SnCl[L][HLiPr] (2): In a similar manner as described for 1, a solution of o-carborane (1.0 g, 7.0 mmol) in THF (50 mL) was treated with n-butyllithium (7.0 mmol, 4.4 mL of a 1.6 mol l−1 solution in hexanes) and iPrN=C=NiPr (0.88 g, 7.0 mmol). Subsequently, SnCl4 (0.93 g, 3.5 mmol) was added dropwise and the mixture was stirred for 24 h at r.t. Cooling of the resulting solution to 278 K for several days afforded large, colorless crystals of [Li(THF)4][SnCl5(THF)]. Yield: 2.13 g. In addition to the IR data reported by Junk & Leary (2000), the compound was further characterized by its NMR (7Li and 119Sn) data. 7Li NMR (155.5 MHz, THF-D8, 295 (2) K): δ = −0.76 ppm. 119Sn NMR (149.1 MHz, THF-D8, 295 (2) K): δ = −641 ppm. Concentration of the mother liquid to ca. 10 ml followed by cooling again to 278 K for several days afforded 0.13 g (5%) of 2 as colorless, plate-like single-crystals. Analysis calculated for C18H49B20ClN4Sn, M = 692.00 g mol−1: C 31.24, H 7.14, N 5.12%. Found: 31.02, H 6.88, N 4.98%. IR: ν 3410 w (ν NH), 2964 m, 2930 w (ν CH3, CH), 2616 m, 2569 s (ν BH), 1628 m, 1596 vs (ν C=N), 1461 m, 1372 m (δ CH3, CH) cm−1. 1H NMR (400.1 MHz, THF-D8, 295 (2) K): δ 5.56 (s br, 1H, NH), 4.33–4.39 (m, 2H, CH iPr), 3.30–3.42 (m, 2H, CH iPr), 1.7–3.2 (m br, 20H, BH), 1.23–1.56 (m, 14H, CH3), 0.96–1.05 (m, 10H, CH3) ppm. 13C NMR (100.6 MHz, THF-D8, 295 (2) K): δ 140.6 (NCN), 139.1 (NCN), 74.4 (C—CN2), 73.2 (C—CN2), 69.8 (C—Sn), 52.0 (CH iPr), 48.3 (CH iPr), 25.5 (CH3), 23.1 (CH3) ppm. 119Sn NMR (149.2 MHz, THF-D8, 295 (2) K): δ 290 ppm. MS: m/z (%) 692 (49) [M]+, 656 (76) [C18H49B20N4Sn]+, 423 (48) [C9H24B10ClN2Sn]+, 388 (82) [C9H24B10N2Sn]+, 211 (100) [C5H13B10N2]+, 171 (18) [C3H10B10N]+.
6. Refinement
Crystal data, data collection and structure . H atoms attached to C atoms were fixed geometrically and refined using a riding model. The CH3 groups in 2 were allowed to rotate freely around the C—C vector, the corresponding C—H distances were constrained to 0.98 Å. C—H distances within CH2 groups were constrained to 0.99 Å, C—H distances within CH groups to 1.00 Å. H atoms attached to B and N atoms were located in the difference-Fourier map, B—H distances were restrained to 1.12 (2) Å and N—H distances to 0.88 (2) Å. The Uiso(H) values were set at 1.5Ueq(C) for the methyl groups in 2, and at 1.2Ueq(X) (X = B, C, N) in all other cases. For 1, the reflections (100) and (00) disagreed strongly with the structural model and were therefore omitted from the refinement.
details are summarized in Table 1Supporting information
https://doi.org/10.1107/S2056989017012671/zl2714sup1.cif
contains datablocks compound_1, compound_2. DOI:Structure factors: contains datablock compound_1. DOI: https://doi.org/10.1107/S2056989017012671/zl2714compound_1sup2.hkl
Structure factors: contains datablock compound_2. DOI: https://doi.org/10.1107/S2056989017012671/zl2714compound_2sup3.hkl
For both structures, data collection: X-AREA (Stoe & Cie, 2002); cell
X-AREA (Stoe & Cie, 2002); data reduction: X-AREA and X-RED (Stoe & Cie, 2002); program(s) used to solve structure: SIR97 (Altomare et al., 1999); program(s) used to refine structure: SHELXL2016/4 (Sheldrick, 2015); molecular graphics: DIAMOND (Brandenburg, 1999); software used to prepare material for publication: publCIF (Westrip, 2010).[Sn(C15H33B10N2)2] | Z = 2 |
Mr = 817.75 | F(000) = 848 |
Triclinic, P1 | Dx = 1.301 Mg m−3 |
a = 10.9097 (3) Å | Mo Kα radiation, λ = 0.71073 Å |
b = 12.9481 (3) Å | Cell parameters from 28532 reflections |
c = 15.4066 (4) Å | θ = 1.9–29.2° |
α = 97.780 (2)° | µ = 0.64 mm−1 |
β = 99.924 (2)° | T = 133 K |
γ = 99.003 (2)° | Block, colorless |
V = 2087.67 (9) Å3 | 0.29 × 0.27 × 0.26 mm |
Stoe IPDS 2T diffractometer | 8436 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.031 |
Detector resolution: 6.67 pixels mm-1 | θmax = 27.0°, θmin = 2.1° |
area detector scans | h = −13→13 |
23428 measured reflections | k = −16→16 |
9102 independent reflections | l = −16→19 |
Refinement on F2 | Primary atom site location: heavy-atom method |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.022 | Hydrogen site location: mixed |
wR(F2) = 0.058 | H atoms treated by a mixture of independent and constrained refinement |
S = 1.05 | w = 1/[σ2(Fo2) + (0.0298P)2 + 0.9924P] where P = (Fo2 + 2Fc2)/3 |
9102 reflections | (Δ/σ)max = 0.002 |
562 parameters | Δρmax = 0.48 e Å−3 |
21 restraints | Δρmin = −0.62 e Å−3 |
Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. |
x | y | z | Uiso*/Ueq | ||
C1 | −0.11416 (14) | 0.11380 (12) | 0.72392 (10) | 0.0125 (3) | |
C2 | 0.00983 (13) | 0.13613 (11) | 0.79178 (10) | 0.0112 (3) | |
C3 | 0.10797 (14) | 0.24815 (12) | 0.79304 (10) | 0.0125 (3) | |
C4 | −0.22894 (14) | 0.14758 (12) | 0.58599 (10) | 0.0133 (3) | |
H12 | −0.310449 | 0.125827 | 0.605684 | 0.016* | |
C5 | −0.20260 (15) | 0.05378 (12) | 0.52480 (11) | 0.0168 (3) | |
H14 | −0.115600 | 0.070897 | 0.513662 | 0.020* | |
H13 | −0.207704 | −0.009033 | 0.555103 | 0.020* | |
C6 | −0.29621 (16) | 0.02717 (13) | 0.43577 (11) | 0.0196 (3) | |
H16 | −0.275133 | −0.032624 | 0.397421 | 0.024* | |
H15 | −0.382969 | 0.005452 | 0.446031 | 0.024* | |
C7 | −0.29039 (16) | 0.12377 (14) | 0.38940 (11) | 0.0215 (3) | |
H17 | −0.349829 | 0.106237 | 0.330952 | 0.026* | |
H18 | −0.203871 | 0.144937 | 0.378525 | 0.026* | |
C8 | −0.32548 (17) | 0.21514 (14) | 0.44765 (11) | 0.0222 (3) | |
H19 | −0.413889 | 0.195084 | 0.455241 | 0.027* | |
H20 | −0.320347 | 0.278056 | 0.417470 | 0.027* | |
C9 | −0.23742 (15) | 0.24343 (12) | 0.53957 (11) | 0.0171 (3) | |
H22 | −0.151709 | 0.274929 | 0.532519 | 0.020* | |
H21 | −0.268630 | 0.297413 | 0.577592 | 0.020* | |
C10 | −0.33271 (14) | −0.00110 (12) | 0.71104 (10) | 0.0146 (3) | |
H23 | −0.358930 | −0.009969 | 0.644590 | 0.018* | |
C11 | −0.39596 (15) | 0.08449 (13) | 0.75406 (11) | 0.0175 (3) | |
H24 | −0.360476 | 0.153926 | 0.739810 | 0.021* | |
H25 | −0.487759 | 0.068625 | 0.728160 | 0.021* | |
C12 | −0.37712 (16) | 0.09195 (14) | 0.85542 (12) | 0.0213 (3) | |
H26 | −0.286484 | 0.118080 | 0.882330 | 0.026* | |
H27 | −0.425951 | 0.143678 | 0.879282 | 0.026* | |
C13 | −0.41987 (16) | −0.01526 (14) | 0.88186 (12) | 0.0216 (3) | |
H28 | −0.401460 | −0.008350 | 0.947806 | 0.026* | |
H29 | −0.512506 | −0.037551 | 0.860864 | 0.026* | |
C14 | −0.35329 (15) | −0.09960 (13) | 0.84209 (11) | 0.0182 (3) | |
H31 | −0.387844 | −0.169057 | 0.856731 | 0.022* | |
H30 | −0.261846 | −0.081933 | 0.869049 | 0.022* | |
C15 | −0.37045 (15) | −0.10775 (12) | 0.74081 (11) | 0.0167 (3) | |
H32 | −0.460260 | −0.137147 | 0.713454 | 0.020* | |
H33 | −0.318685 | −0.157852 | 0.718408 | 0.020* | |
C16 | 0.31859 (14) | 0.47432 (11) | 0.70647 (10) | 0.0130 (3) | |
C17 | 0.28318 (13) | 0.41073 (12) | 0.61218 (10) | 0.0119 (3) | |
C18 | 0.14315 (14) | 0.33148 (12) | 0.58673 (10) | 0.0128 (3) | |
C19 | 0.23568 (15) | 0.57196 (12) | 0.82159 (10) | 0.0152 (3) | |
H45 | 0.307927 | 0.570908 | 0.870980 | 0.018* | |
C20 | 0.25677 (17) | 0.67761 (13) | 0.78688 (12) | 0.0212 (3) | |
H46 | 0.187093 | 0.677226 | 0.736231 | 0.025* | |
H47 | 0.337108 | 0.685802 | 0.764696 | 0.025* | |
C21 | 0.26204 (19) | 0.77176 (14) | 0.86052 (14) | 0.0291 (4) | |
H49 | 0.336564 | 0.776213 | 0.908651 | 0.035* | |
H48 | 0.271895 | 0.838370 | 0.835450 | 0.035* | |
C22 | 0.14225 (19) | 0.75993 (14) | 0.89946 (14) | 0.0285 (4) | |
H51 | 0.151005 | 0.818350 | 0.950014 | 0.034* | |
H50 | 0.069026 | 0.764782 | 0.853290 | 0.034* | |
C23 | 0.11870 (17) | 0.65455 (14) | 0.93165 (12) | 0.0228 (3) | |
H52 | 0.037756 | 0.646504 | 0.953041 | 0.027* | |
H53 | 0.187319 | 0.653076 | 0.982465 | 0.027* | |
C24 | 0.11324 (15) | 0.56241 (13) | 0.85708 (11) | 0.0178 (3) | |
H55 | 0.098409 | 0.494724 | 0.880134 | 0.021* | |
H54 | 0.041503 | 0.561438 | 0.807726 | 0.021* | |
C25 | 0.51973 (14) | 0.56385 (13) | 0.81933 (10) | 0.0161 (3) | |
H56 | 0.482231 | 0.623151 | 0.846298 | 0.019* | |
C26 | 0.65291 (15) | 0.60854 (13) | 0.80871 (11) | 0.0193 (3) | |
H58 | 0.699643 | 0.652674 | 0.865881 | 0.023* | |
H57 | 0.647321 | 0.655075 | 0.762754 | 0.023* | |
C27 | 0.72730 (16) | 0.52297 (16) | 0.78193 (12) | 0.0243 (4) | |
H59 | 0.687323 | 0.484621 | 0.721111 | 0.029* | |
H60 | 0.814776 | 0.556632 | 0.780608 | 0.029* | |
C28 | 0.73118 (18) | 0.44483 (17) | 0.84694 (14) | 0.0308 (4) | |
H62 | 0.778348 | 0.481726 | 0.906646 | 0.037* | |
H61 | 0.775950 | 0.388121 | 0.826440 | 0.037* | |
C29 | 0.59738 (18) | 0.39607 (15) | 0.85348 (14) | 0.0284 (4) | |
H64 | 0.601467 | 0.347390 | 0.897785 | 0.034* | |
H63 | 0.552882 | 0.354124 | 0.794849 | 0.034* | |
C30 | 0.52318 (16) | 0.48122 (14) | 0.88119 (11) | 0.0216 (3) | |
H66 | 0.562167 | 0.517180 | 0.942888 | 0.026* | |
H65 | 0.435406 | 0.447070 | 0.881203 | 0.026* | |
B1 | 0.14297 (16) | 0.12971 (14) | 0.74892 (12) | 0.0145 (3) | |
H2 | 0.1300 (18) | 0.1113 (15) | 0.6776 (10) | 0.017* | |
B2 | 0.08805 (16) | 0.03507 (14) | 0.81413 (12) | 0.0150 (3) | |
H3 | 0.0439 (18) | −0.0445 (12) | 0.7803 (13) | 0.018* | |
B3 | 0.01701 (16) | 0.10089 (14) | 0.89549 (12) | 0.0151 (3) | |
H4 | −0.0698 (15) | 0.0625 (15) | 0.9116 (13) | 0.018* | |
B4 | 0.02671 (16) | 0.23545 (14) | 0.87955 (11) | 0.0148 (3) | |
H5 | −0.0512 (16) | 0.2773 (15) | 0.8812 (13) | 0.018* | |
B5 | 0.17205 (17) | 0.07622 (14) | 0.92563 (12) | 0.0169 (3) | |
H6 | 0.1871 (19) | 0.0167 (14) | 0.9662 (13) | 0.020* | |
B6 | 0.13306 (16) | 0.20070 (15) | 0.96705 (12) | 0.0164 (3) | |
H7 | 0.1257 (19) | 0.2231 (16) | 1.0363 (10) | 0.020* | |
B7 | 0.26059 (16) | 0.22856 (14) | 0.82147 (12) | 0.0157 (3) | |
H8 | 0.3340 (16) | 0.2737 (15) | 0.7953 (13) | 0.019* | |
B8 | 0.25023 (16) | 0.09419 (14) | 0.83482 (12) | 0.0167 (3) | |
H9 | 0.3217 (17) | 0.0484 (15) | 0.8160 (14) | 0.020* | |
B9 | 0.18873 (16) | 0.29350 (14) | 0.90120 (12) | 0.0155 (3) | |
H10 | 0.2141 (18) | 0.3779 (12) | 0.9235 (13) | 0.019* | |
B10 | 0.27885 (16) | 0.19592 (14) | 0.93032 (12) | 0.0161 (3) | |
H11 | 0.3663 (19) | 0.2203 (16) | 0.9762 (14) | 0.019* | |
B11 | 0.27956 (16) | 0.27721 (13) | 0.59623 (12) | 0.0137 (3) | |
H35 | 0.3081 (18) | 0.2402 (15) | 0.6538 (11) | 0.016* | |
B12 | 0.39067 (16) | 0.36406 (14) | 0.55529 (12) | 0.0141 (3) | |
H36 | 0.4881 (14) | 0.3792 (15) | 0.5892 (12) | 0.017* | |
B13 | 0.16204 (16) | 0.44953 (14) | 0.54558 (12) | 0.0152 (3) | |
H37 | 0.1211 (18) | 0.5161 (14) | 0.5738 (13) | 0.018* | |
B14 | 0.14878 (17) | 0.22590 (14) | 0.50799 (12) | 0.0159 (3) | |
H38 | 0.0918 (17) | 0.1500 (13) | 0.5099 (14) | 0.019* | |
B15 | 0.07798 (17) | 0.33208 (15) | 0.47631 (12) | 0.0165 (3) | |
H39 | −0.0239 (14) | 0.3241 (16) | 0.4545 (13) | 0.020* | |
B16 | 0.30530 (17) | 0.24568 (14) | 0.48624 (12) | 0.0159 (3) | |
H40 | 0.3525 (18) | 0.1793 (14) | 0.4716 (14) | 0.019* | |
B17 | 0.31896 (17) | 0.47129 (14) | 0.52457 (12) | 0.0159 (3) | |
H41 | 0.3735 (17) | 0.5515 (12) | 0.5392 (13) | 0.019* | |
B18 | 0.32931 (17) | 0.36563 (15) | 0.44173 (12) | 0.0166 (3) | |
H42 | 0.3941 (17) | 0.3771 (16) | 0.3954 (12) | 0.020* | |
B19 | 0.18760 (18) | 0.41939 (15) | 0.43589 (12) | 0.0183 (3) | |
H43 | 0.1547 (19) | 0.4634 (15) | 0.3853 (12) | 0.022* | |
B20 | 0.17989 (17) | 0.27947 (15) | 0.41158 (12) | 0.0182 (3) | |
H44 | 0.1438 (19) | 0.2332 (15) | 0.3446 (11) | 0.022* | |
N1 | −0.12440 (12) | 0.17515 (10) | 0.66519 (9) | 0.0136 (2) | |
N2 | −0.19351 (12) | 0.02767 (11) | 0.73572 (9) | 0.0149 (3) | |
H1 | −0.1636 (18) | −0.0031 (15) | 0.7740 (12) | 0.018* | |
N3 | 0.22665 (12) | 0.48252 (10) | 0.74832 (9) | 0.0138 (2) | |
N4 | 0.44228 (12) | 0.51868 (11) | 0.73005 (9) | 0.0152 (3) | |
H34 | 0.4835 (18) | 0.5085 (16) | 0.6891 (12) | 0.018* | |
SN | 0.02544 (2) | 0.35454 (2) | 0.69779 (2) | 0.01185 (4) |
U11 | U22 | U33 | U12 | U13 | U23 | |
C1 | 0.0101 (6) | 0.0134 (7) | 0.0127 (7) | 0.0025 (5) | 0.0011 (5) | −0.0007 (5) |
C2 | 0.0102 (6) | 0.0132 (6) | 0.0103 (7) | 0.0019 (5) | 0.0017 (5) | 0.0024 (5) |
C3 | 0.0114 (7) | 0.0132 (7) | 0.0122 (7) | 0.0007 (5) | 0.0014 (5) | 0.0025 (5) |
C4 | 0.0120 (7) | 0.0144 (7) | 0.0119 (7) | 0.0015 (5) | −0.0002 (5) | 0.0010 (6) |
C5 | 0.0167 (7) | 0.0170 (7) | 0.0149 (7) | 0.0049 (6) | −0.0007 (6) | −0.0004 (6) |
C6 | 0.0184 (8) | 0.0214 (8) | 0.0157 (8) | 0.0045 (6) | −0.0020 (6) | −0.0030 (6) |
C7 | 0.0210 (8) | 0.0284 (9) | 0.0130 (7) | 0.0044 (7) | −0.0015 (6) | 0.0023 (6) |
C8 | 0.0239 (8) | 0.0226 (8) | 0.0178 (8) | 0.0080 (7) | −0.0058 (6) | 0.0031 (6) |
C9 | 0.0177 (7) | 0.0156 (7) | 0.0160 (7) | 0.0030 (6) | −0.0022 (6) | 0.0033 (6) |
C10 | 0.0103 (7) | 0.0174 (7) | 0.0142 (7) | 0.0002 (5) | −0.0004 (5) | 0.0022 (6) |
C11 | 0.0128 (7) | 0.0187 (7) | 0.0213 (8) | 0.0038 (6) | 0.0025 (6) | 0.0043 (6) |
C12 | 0.0192 (8) | 0.0239 (8) | 0.0211 (8) | 0.0071 (6) | 0.0044 (6) | −0.0001 (7) |
C13 | 0.0176 (8) | 0.0309 (9) | 0.0190 (8) | 0.0082 (7) | 0.0055 (6) | 0.0064 (7) |
C14 | 0.0161 (7) | 0.0208 (8) | 0.0188 (8) | 0.0036 (6) | 0.0031 (6) | 0.0071 (6) |
C15 | 0.0150 (7) | 0.0163 (7) | 0.0168 (8) | −0.0002 (6) | 0.0008 (6) | 0.0017 (6) |
C16 | 0.0143 (7) | 0.0116 (6) | 0.0126 (7) | 0.0030 (5) | 0.0015 (5) | 0.0010 (5) |
C17 | 0.0097 (6) | 0.0134 (7) | 0.0125 (7) | 0.0018 (5) | 0.0031 (5) | 0.0010 (5) |
C18 | 0.0100 (6) | 0.0140 (7) | 0.0133 (7) | 0.0010 (5) | 0.0022 (5) | 0.0003 (5) |
C19 | 0.0150 (7) | 0.0155 (7) | 0.0149 (7) | 0.0037 (6) | 0.0048 (6) | −0.0018 (6) |
C20 | 0.0238 (8) | 0.0181 (8) | 0.0234 (8) | 0.0039 (6) | 0.0101 (7) | 0.0026 (7) |
C21 | 0.0334 (10) | 0.0150 (8) | 0.0389 (11) | 0.0013 (7) | 0.0147 (8) | −0.0015 (7) |
C22 | 0.0353 (10) | 0.0179 (8) | 0.0342 (10) | 0.0084 (7) | 0.0152 (8) | −0.0037 (7) |
C23 | 0.0265 (9) | 0.0219 (8) | 0.0218 (8) | 0.0071 (7) | 0.0113 (7) | −0.0010 (7) |
C24 | 0.0167 (7) | 0.0160 (7) | 0.0211 (8) | 0.0041 (6) | 0.0071 (6) | −0.0008 (6) |
C25 | 0.0130 (7) | 0.0197 (7) | 0.0130 (7) | 0.0006 (6) | 0.0012 (6) | −0.0025 (6) |
C26 | 0.0141 (7) | 0.0230 (8) | 0.0173 (8) | −0.0034 (6) | 0.0004 (6) | 0.0022 (6) |
C27 | 0.0135 (7) | 0.0385 (10) | 0.0217 (8) | 0.0049 (7) | 0.0048 (6) | 0.0059 (7) |
C28 | 0.0200 (9) | 0.0397 (11) | 0.0362 (11) | 0.0119 (8) | 0.0037 (8) | 0.0134 (9) |
C29 | 0.0250 (9) | 0.0282 (9) | 0.0342 (10) | 0.0064 (7) | 0.0036 (8) | 0.0145 (8) |
C30 | 0.0171 (8) | 0.0302 (9) | 0.0162 (8) | −0.0008 (7) | 0.0033 (6) | 0.0057 (7) |
B1 | 0.0117 (7) | 0.0170 (8) | 0.0149 (8) | 0.0029 (6) | 0.0032 (6) | 0.0022 (6) |
B2 | 0.0134 (8) | 0.0157 (8) | 0.0165 (8) | 0.0042 (6) | 0.0019 (6) | 0.0040 (6) |
B3 | 0.0135 (8) | 0.0197 (8) | 0.0121 (8) | 0.0015 (6) | 0.0016 (6) | 0.0056 (6) |
B4 | 0.0135 (8) | 0.0191 (8) | 0.0109 (8) | 0.0033 (6) | 0.0018 (6) | 0.0001 (6) |
B5 | 0.0145 (8) | 0.0191 (8) | 0.0171 (8) | 0.0029 (6) | 0.0001 (6) | 0.0071 (7) |
B6 | 0.0134 (8) | 0.0229 (9) | 0.0119 (8) | 0.0028 (7) | 0.0005 (6) | 0.0024 (7) |
B7 | 0.0113 (7) | 0.0199 (8) | 0.0152 (8) | 0.0012 (6) | 0.0014 (6) | 0.0035 (7) |
B8 | 0.0125 (8) | 0.0199 (8) | 0.0180 (8) | 0.0051 (6) | 0.0017 (6) | 0.0037 (7) |
B9 | 0.0139 (8) | 0.0173 (8) | 0.0131 (8) | 0.0018 (6) | −0.0012 (6) | 0.0009 (6) |
B10 | 0.0115 (8) | 0.0203 (8) | 0.0152 (8) | 0.0018 (6) | −0.0005 (6) | 0.0037 (7) |
B11 | 0.0136 (8) | 0.0129 (7) | 0.0154 (8) | 0.0029 (6) | 0.0050 (6) | 0.0013 (6) |
B12 | 0.0128 (8) | 0.0160 (8) | 0.0142 (8) | 0.0028 (6) | 0.0060 (6) | 0.0005 (6) |
B13 | 0.0135 (8) | 0.0175 (8) | 0.0153 (8) | 0.0042 (6) | 0.0026 (6) | 0.0046 (6) |
B14 | 0.0154 (8) | 0.0156 (8) | 0.0156 (8) | 0.0009 (6) | 0.0054 (6) | −0.0021 (6) |
B15 | 0.0137 (8) | 0.0219 (8) | 0.0128 (8) | 0.0029 (7) | 0.0016 (6) | 0.0002 (7) |
B16 | 0.0155 (8) | 0.0165 (8) | 0.0154 (8) | 0.0018 (6) | 0.0064 (6) | −0.0016 (6) |
B17 | 0.0158 (8) | 0.0169 (8) | 0.0164 (8) | 0.0025 (6) | 0.0063 (6) | 0.0045 (7) |
B18 | 0.0161 (8) | 0.0199 (8) | 0.0136 (8) | 0.0016 (7) | 0.0052 (6) | 0.0017 (7) |
B19 | 0.0181 (8) | 0.0240 (9) | 0.0138 (8) | 0.0042 (7) | 0.0042 (7) | 0.0055 (7) |
B20 | 0.0157 (8) | 0.0245 (9) | 0.0127 (8) | 0.0016 (7) | 0.0036 (6) | −0.0010 (7) |
N1 | 0.0122 (6) | 0.0147 (6) | 0.0120 (6) | 0.0021 (5) | −0.0012 (5) | 0.0007 (5) |
N2 | 0.0098 (6) | 0.0178 (6) | 0.0164 (6) | 0.0012 (5) | −0.0007 (5) | 0.0058 (5) |
N3 | 0.0135 (6) | 0.0137 (6) | 0.0140 (6) | 0.0032 (5) | 0.0036 (5) | −0.0004 (5) |
N4 | 0.0111 (6) | 0.0209 (6) | 0.0120 (6) | 0.0008 (5) | 0.0025 (5) | −0.0006 (5) |
SN | 0.01086 (5) | 0.01295 (5) | 0.01233 (5) | 0.00372 (4) | 0.00290 (4) | 0.00161 (4) |
C1—N1 | 1.284 (2) | C25—C30 | 1.527 (2) |
C1—N2 | 1.354 (2) | C25—H56 | 1.0000 |
C1—C2 | 1.521 (2) | C26—C27 | 1.526 (2) |
C2—C3 | 1.658 (2) | C26—H58 | 0.9900 |
C2—B4 | 1.699 (2) | C26—H57 | 0.9900 |
C2—B1 | 1.705 (2) | C27—C28 | 1.517 (3) |
C2—B2 | 1.711 (2) | C27—H59 | 0.9900 |
C2—B3 | 1.712 (2) | C27—H60 | 0.9900 |
C3—B7 | 1.715 (2) | C28—C29 | 1.523 (3) |
C3—B1 | 1.718 (2) | C28—H62 | 0.9900 |
C3—B9 | 1.722 (2) | C28—H61 | 0.9900 |
C3—B4 | 1.735 (2) | C29—C30 | 1.524 (3) |
C3—SN | 2.3112 (15) | C29—H64 | 0.9900 |
C4—N1 | 1.4805 (19) | C29—H63 | 0.9900 |
C4—C9 | 1.521 (2) | C30—H66 | 0.9900 |
C4—C5 | 1.529 (2) | C30—H65 | 0.9900 |
C4—H12 | 1.0000 | B1—B8 | 1.770 (2) |
C5—C6 | 1.524 (2) | B1—B7 | 1.772 (3) |
C5—H14 | 0.9900 | B1—B2 | 1.784 (3) |
C5—H13 | 0.9900 | B1—H2 | 1.072 (14) |
C6—C7 | 1.520 (2) | B2—B5 | 1.770 (3) |
C6—H16 | 0.9900 | B2—B8 | 1.770 (2) |
C6—H15 | 0.9900 | B2—B3 | 1.775 (2) |
C7—C8 | 1.525 (2) | B2—H3 | 1.085 (14) |
C7—H17 | 0.9900 | B3—B6 | 1.763 (3) |
C7—H18 | 0.9900 | B3—B5 | 1.766 (2) |
C8—C9 | 1.531 (2) | B3—B4 | 1.782 (3) |
C8—H19 | 0.9900 | B3—H4 | 1.083 (14) |
C8—H20 | 0.9900 | B4—B9 | 1.765 (2) |
C9—H22 | 0.9900 | B4—B6 | 1.776 (2) |
C9—H21 | 0.9900 | B4—H5 | 1.079 (14) |
C10—N2 | 1.4749 (19) | B5—B10 | 1.772 (3) |
C10—C11 | 1.530 (2) | B5—B8 | 1.782 (3) |
C10—C15 | 1.531 (2) | B5—B6 | 1.793 (3) |
C10—H23 | 1.0000 | B5—H6 | 1.070 (15) |
C11—C12 | 1.527 (2) | B6—B9 | 1.776 (3) |
C11—H24 | 0.9900 | B6—B10 | 1.785 (2) |
C11—H25 | 0.9900 | B6—H7 | 1.087 (15) |
C12—C13 | 1.525 (2) | B7—B9 | 1.758 (3) |
C12—H26 | 0.9900 | B7—B8 | 1.768 (3) |
C12—H27 | 0.9900 | B7—B10 | 1.770 (3) |
C13—C14 | 1.522 (2) | B7—H8 | 1.083 (15) |
C13—H28 | 0.9900 | B8—B10 | 1.785 (3) |
C13—H29 | 0.9900 | B8—H9 | 1.105 (14) |
C14—C15 | 1.526 (2) | B9—B10 | 1.776 (3) |
C14—H31 | 0.9900 | B9—H10 | 1.077 (15) |
C14—H30 | 0.9900 | B10—H11 | 1.06 (2) |
C15—H32 | 0.9900 | B11—B14 | 1.765 (2) |
C15—H33 | 0.9900 | B11—B16 | 1.769 (2) |
C16—N3 | 1.293 (2) | B11—B12 | 1.778 (2) |
C16—N4 | 1.347 (2) | B11—H35 | 1.087 (14) |
C16—C17 | 1.523 (2) | B12—B16 | 1.766 (2) |
C17—C18 | 1.654 (2) | B12—B18 | 1.766 (3) |
C17—B11 | 1.706 (2) | B12—B17 | 1.776 (2) |
C17—B13 | 1.712 (2) | B12—H36 | 1.075 (14) |
C17—B12 | 1.715 (2) | B13—B15 | 1.755 (3) |
C17—B17 | 1.721 (2) | B13—B19 | 1.762 (3) |
C18—B14 | 1.717 (2) | B13—B17 | 1.783 (2) |
C18—B15 | 1.729 (2) | B13—H37 | 1.103 (14) |
C18—B13 | 1.729 (2) | B14—B15 | 1.763 (3) |
C18—B11 | 1.735 (2) | B14—B16 | 1.783 (2) |
C18—SN | 2.3249 (15) | B14—B20 | 1.784 (3) |
C19—N3 | 1.4822 (19) | B14—H38 | 1.084 (15) |
C19—C24 | 1.522 (2) | B15—B19 | 1.766 (3) |
C19—C20 | 1.534 (2) | B15—B20 | 1.769 (3) |
C19—H45 | 1.0000 | B15—H39 | 1.088 (15) |
C20—C21 | 1.536 (2) | B16—B20 | 1.780 (3) |
C20—H46 | 0.9900 | B16—B18 | 1.782 (3) |
C20—H47 | 0.9900 | B16—H40 | 1.087 (14) |
C21—C22 | 1.524 (3) | B17—B18 | 1.772 (3) |
C21—H49 | 0.9900 | B17—B19 | 1.774 (3) |
C21—H48 | 0.9900 | B17—H41 | 1.086 (15) |
C22—C23 | 1.514 (3) | B18—B20 | 1.774 (3) |
C22—H51 | 0.9900 | B18—B19 | 1.786 (3) |
C22—H50 | 0.9900 | B18—H42 | 1.096 (15) |
C23—C24 | 1.526 (2) | B19—B20 | 1.785 (3) |
C23—H52 | 0.9900 | B19—H43 | 1.072 (15) |
C23—H53 | 0.9900 | B20—H44 | 1.094 (15) |
C24—H55 | 0.9900 | N1—SN | 2.5560 (13) |
C24—H54 | 0.9900 | N2—H1 | 0.807 (15) |
C25—N4 | 1.4747 (19) | N3—SN | 2.4686 (13) |
C25—C26 | 1.522 (2) | N4—H34 | 0.843 (15) |
N1—C1—N2 | 131.54 (14) | B6—B4—B3 | 59.43 (10) |
N1—C1—C2 | 116.65 (13) | C2—B4—H5 | 116.7 (11) |
N2—C1—C2 | 111.77 (13) | C3—B4—H5 | 117.1 (11) |
C1—C2—C3 | 116.58 (12) | B9—B4—H5 | 126.1 (11) |
C1—C2—B4 | 116.93 (12) | B6—B4—H5 | 131.1 (11) |
C3—C2—B4 | 62.23 (9) | B3—B4—H5 | 123.0 (11) |
C1—C2—B1 | 115.88 (12) | B3—B5—B2 | 60.27 (10) |
C3—C2—B1 | 61.41 (9) | B3—B5—B10 | 107.65 (12) |
B4—C2—B1 | 114.69 (12) | B2—B5—B10 | 108.14 (12) |
C1—C2—B2 | 120.26 (12) | B3—B5—B8 | 107.84 (12) |
C3—C2—B2 | 112.43 (11) | B2—B5—B8 | 59.79 (10) |
B4—C2—B2 | 114.90 (12) | B10—B5—B8 | 60.29 (10) |
B1—C2—B2 | 62.94 (10) | B3—B5—B6 | 59.40 (10) |
C1—C2—B3 | 121.28 (12) | B2—B5—B6 | 107.87 (12) |
C3—C2—B3 | 112.70 (11) | B10—B5—B6 | 60.07 (10) |
B4—C2—B3 | 62.97 (10) | B8—B5—B6 | 108.07 (12) |
B1—C2—B3 | 114.54 (12) | B3—B5—H6 | 118.6 (11) |
B2—C2—B3 | 62.45 (10) | B2—B5—H6 | 118.3 (11) |
C2—C3—B7 | 108.79 (11) | B10—B5—H6 | 125.8 (11) |
C2—C3—B1 | 60.63 (9) | B8—B5—H6 | 122.9 (11) |
B7—C3—B1 | 62.15 (10) | B6—B5—H6 | 123.1 (11) |
C2—C3—B9 | 108.15 (11) | B3—B6—B4 | 60.44 (10) |
B7—C3—B9 | 61.52 (10) | B3—B6—B9 | 107.58 (12) |
B1—C3—B9 | 112.39 (12) | B4—B6—B9 | 59.56 (10) |
C2—C3—B4 | 60.03 (9) | B3—B6—B10 | 107.19 (12) |
B7—C3—B4 | 111.76 (11) | B4—B6—B10 | 107.52 (12) |
B1—C3—B4 | 112.18 (12) | B9—B6—B10 | 59.83 (10) |
B9—C3—B4 | 61.38 (10) | B3—B6—B5 | 59.52 (10) |
C2—C3—SN | 113.65 (9) | B4—B6—B5 | 107.64 (12) |
B7—C3—SN | 129.66 (10) | B9—B6—B5 | 107.05 (12) |
B1—C3—SN | 119.32 (10) | B10—B6—B5 | 59.38 (10) |
B9—C3—SN | 124.42 (10) | B3—B6—H7 | 120.1 (11) |
B4—C3—SN | 112.20 (9) | B4—B6—H7 | 120.3 (11) |
N1—C4—C9 | 109.78 (12) | B9—B6—H7 | 123.1 (11) |
N1—C4—C5 | 107.60 (12) | B10—B6—H7 | 124.2 (11) |
C9—C4—C5 | 112.01 (13) | B5—B6—H7 | 122.6 (11) |
N1—C4—H12 | 109.1 | C3—B7—B9 | 59.45 (9) |
C9—C4—H12 | 109.1 | C3—B7—B8 | 106.32 (12) |
C5—C4—H12 | 109.1 | B9—B7—B8 | 108.83 (13) |
C6—C5—C4 | 111.97 (13) | C3—B7—B10 | 106.82 (12) |
C6—C5—H14 | 109.2 | B9—B7—B10 | 60.46 (10) |
C4—C5—H14 | 109.2 | B8—B7—B10 | 60.60 (10) |
C6—C5—H13 | 109.2 | C3—B7—B1 | 59.01 (9) |
C4—C5—H13 | 109.2 | B9—B7—B1 | 108.16 (12) |
H14—C5—H13 | 107.9 | B8—B7—B1 | 60.00 (10) |
C7—C6—C5 | 109.56 (14) | B10—B7—B1 | 108.57 (12) |
C7—C6—H16 | 109.8 | C3—B7—H8 | 118.8 (11) |
C5—C6—H16 | 109.8 | B9—B7—H8 | 119.6 (11) |
C7—C6—H15 | 109.8 | B8—B7—H8 | 125.4 (11) |
C5—C6—H15 | 109.8 | B10—B7—H8 | 125.1 (11) |
H16—C6—H15 | 108.2 | B1—B7—H8 | 120.1 (11) |
C6—C7—C8 | 109.74 (14) | B7—B8—B1 | 60.11 (10) |
C6—C7—H17 | 109.7 | B7—B8—B2 | 108.13 (12) |
C8—C7—H17 | 109.7 | B1—B8—B2 | 60.51 (10) |
C6—C7—H18 | 109.7 | B7—B8—B5 | 107.47 (12) |
C8—C7—H18 | 109.7 | B1—B8—B5 | 108.16 (12) |
H17—C7—H18 | 108.2 | B2—B8—B5 | 59.75 (10) |
C7—C8—C9 | 111.47 (13) | B7—B8—B10 | 59.77 (10) |
C7—C8—H19 | 109.3 | B1—B8—B10 | 108.00 (12) |
C9—C8—H19 | 109.3 | B2—B8—B10 | 107.54 (12) |
C7—C8—H20 | 109.3 | B5—B8—B10 | 59.57 (10) |
C9—C8—H20 | 109.3 | B7—B8—H9 | 120.8 (11) |
H19—C8—H20 | 108.0 | B1—B8—H9 | 118.6 (11) |
C4—C9—C8 | 112.47 (13) | B2—B8—H9 | 120.9 (11) |
C4—C9—H22 | 109.1 | B5—B8—H9 | 124.4 (11) |
C8—C9—H22 | 109.1 | B10—B8—H9 | 124.2 (11) |
C4—C9—H21 | 109.1 | C3—B9—B7 | 59.03 (9) |
C8—C9—H21 | 109.1 | C3—B9—B4 | 59.67 (9) |
H22—C9—H21 | 107.8 | B7—B9—B4 | 108.35 (12) |
N2—C10—C11 | 111.43 (13) | C3—B9—B10 | 106.23 (12) |
N2—C10—C15 | 106.94 (12) | B7—B9—B10 | 60.12 (10) |
C11—C10—C15 | 111.62 (13) | B4—B9—B10 | 108.41 (13) |
N2—C10—H23 | 108.9 | C3—B9—B6 | 106.77 (12) |
C11—C10—H23 | 108.9 | B7—B9—B6 | 108.57 (12) |
C15—C10—H23 | 108.9 | B4—B9—B6 | 60.21 (10) |
C12—C11—C10 | 112.50 (13) | B10—B9—B6 | 60.32 (10) |
C12—C11—H24 | 109.1 | C3—B9—H10 | 118.2 (11) |
C10—C11—H24 | 109.1 | B7—B9—H10 | 121.5 (11) |
C12—C11—H25 | 109.1 | B4—B9—H10 | 117.7 (11) |
C10—C11—H25 | 109.1 | B10—B9—H10 | 127.2 (11) |
H24—C11—H25 | 107.8 | B6—B9—H10 | 124.5 (11) |
C13—C12—C11 | 111.59 (14) | B7—B10—B5 | 107.81 (12) |
C13—C12—H26 | 109.3 | B7—B10—B9 | 59.42 (10) |
C11—C12—H26 | 109.3 | B5—B10—B9 | 107.99 (12) |
C13—C12—H27 | 109.3 | B7—B10—B6 | 107.64 (12) |
C11—C12—H27 | 109.3 | B5—B10—B6 | 60.55 (10) |
H26—C12—H27 | 108.0 | B9—B10—B6 | 59.85 (10) |
C14—C13—C12 | 111.49 (14) | B7—B10—B8 | 59.63 (10) |
C14—C13—H28 | 109.3 | B5—B10—B8 | 60.14 (10) |
C12—C13—H28 | 109.3 | B9—B10—B8 | 107.24 (12) |
C14—C13—H29 | 109.3 | B6—B10—B8 | 108.33 (12) |
C12—C13—H29 | 109.3 | B7—B10—H11 | 121.0 (11) |
H28—C13—H29 | 108.0 | B5—B10—H11 | 124.3 (11) |
C13—C14—C15 | 111.51 (13) | B9—B10—H11 | 118.8 (11) |
C13—C14—H31 | 109.3 | B6—B10—H11 | 120.4 (11) |
C15—C14—H31 | 109.3 | B8—B10—H11 | 124.5 (11) |
C13—C14—H30 | 109.3 | C17—B11—C18 | 57.43 (9) |
C15—C14—H30 | 109.3 | C17—B11—B14 | 104.20 (12) |
H31—C14—H30 | 108.0 | C18—B11—B14 | 58.74 (9) |
C14—C15—C10 | 113.21 (13) | C17—B11—B16 | 104.87 (12) |
C14—C15—H32 | 108.9 | C18—B11—B16 | 106.21 (12) |
C10—C15—H32 | 108.9 | B14—B11—B16 | 60.58 (10) |
C14—C15—H33 | 108.9 | C17—B11—B12 | 58.93 (9) |
C10—C15—H33 | 108.9 | C18—B11—B12 | 105.83 (12) |
H32—C15—H33 | 107.7 | B14—B11—B12 | 107.87 (12) |
N3—C16—N4 | 130.59 (14) | B16—B11—B12 | 59.72 (10) |
N3—C16—C17 | 116.38 (13) | C17—B11—H35 | 118.7 (10) |
N4—C16—C17 | 112.89 (13) | C18—B11—H35 | 119.7 (10) |
C16—C17—C18 | 115.68 (12) | B14—B11—H35 | 125.9 (11) |
C16—C17—B11 | 119.82 (12) | B16—B11—H35 | 128.4 (10) |
C18—C17—B11 | 62.16 (9) | B12—B11—H35 | 121.6 (10) |
C16—C17—B13 | 113.33 (12) | C17—B12—B16 | 104.63 (11) |
C18—C17—B13 | 61.79 (9) | C17—B12—B18 | 104.94 (12) |
B11—C17—B13 | 114.36 (12) | B16—B12—B18 | 60.58 (10) |
C16—C17—B12 | 123.74 (12) | C17—B12—B17 | 59.04 (9) |
C18—C17—B12 | 112.59 (11) | B16—B12—B17 | 108.57 (13) |
B11—C17—B12 | 62.62 (9) | B18—B12—B17 | 60.02 (10) |
B13—C17—B12 | 113.86 (12) | C17—B12—B11 | 58.45 (9) |
C16—C17—B17 | 119.07 (12) | B16—B12—B11 | 59.89 (10) |
C18—C17—B17 | 112.66 (12) | B18—B12—B11 | 108.37 (12) |
B11—C17—B17 | 114.37 (12) | B17—B12—B11 | 108.28 (12) |
B13—C17—B17 | 62.59 (10) | C17—B12—H36 | 117.6 (10) |
B12—C17—B17 | 62.25 (10) | B16—B12—H36 | 127.2 (10) |
C17—C18—B14 | 108.73 (11) | B18—B12—H36 | 128.4 (11) |
C17—C18—B15 | 108.38 (12) | B17—B12—H36 | 119.6 (11) |
B14—C18—B15 | 61.56 (10) | B11—B12—H36 | 118.0 (11) |
C17—C18—B13 | 60.77 (9) | C17—B13—C18 | 57.44 (9) |
B14—C18—B13 | 111.65 (12) | C17—B13—B15 | 104.59 (12) |
B15—C18—B13 | 61.00 (10) | C18—B13—B15 | 59.49 (10) |
C17—C18—B11 | 60.41 (9) | C17—B13—B19 | 105.22 (12) |
B14—C18—B11 | 61.51 (10) | C18—B13—B19 | 106.88 (12) |
B15—C18—B11 | 111.52 (11) | B15—B13—B19 | 60.30 (10) |
B13—C18—B11 | 112.07 (11) | C17—B13—B17 | 58.94 (9) |
C17—C18—SN | 112.43 (9) | C18—B13—B17 | 106.19 (11) |
B14—C18—SN | 133.77 (10) | B15—B13—B17 | 108.01 (12) |
B15—C18—SN | 120.85 (9) | B19—B13—B17 | 60.05 (10) |
B13—C18—SN | 106.25 (9) | C17—B13—H37 | 118.5 (11) |
B11—C18—SN | 125.30 (10) | C18—B13—H37 | 119.8 (11) |
N3—C19—C24 | 109.96 (13) | B15—B13—H37 | 126.3 (11) |
N3—C19—C20 | 110.05 (13) | B19—B13—H37 | 127.8 (11) |
C24—C19—C20 | 108.32 (13) | B17—B13—H37 | 120.8 (11) |
N3—C19—H45 | 109.5 | C18—B14—B15 | 59.55 (9) |
C24—C19—H45 | 109.5 | C18—B14—B11 | 59.75 (9) |
C20—C19—H45 | 109.5 | B15—B14—B11 | 108.49 (12) |
C19—C20—C21 | 111.32 (14) | C18—B14—B16 | 106.41 (12) |
C19—C20—H46 | 109.4 | B15—B14—B16 | 107.81 (13) |
C21—C20—H46 | 109.4 | B11—B14—B16 | 59.82 (10) |
C19—C20—H47 | 109.4 | C18—B14—B20 | 106.43 (12) |
C21—C20—H47 | 109.4 | B15—B14—B20 | 59.84 (10) |
H46—C20—H47 | 108.0 | B11—B14—B20 | 108.00 (12) |
C22—C21—C20 | 111.13 (15) | B16—B14—B20 | 59.87 (10) |
C22—C21—H49 | 109.4 | C18—B14—H38 | 117.5 (11) |
C20—C21—H49 | 109.4 | B15—B14—H38 | 121.2 (11) |
C22—C21—H48 | 109.4 | B11—B14—H38 | 118.0 (11) |
C20—C21—H48 | 109.4 | B16—B14—H38 | 125.6 (10) |
H49—C21—H48 | 108.0 | B20—B14—H38 | 127.5 (11) |
C23—C22—C21 | 110.72 (15) | C18—B15—B13 | 59.51 (10) |
C23—C22—H51 | 109.5 | C18—B15—B14 | 58.89 (10) |
C21—C22—H51 | 109.5 | B13—B15—B14 | 108.25 (12) |
C23—C22—H50 | 109.5 | C18—B15—B19 | 106.70 (12) |
C21—C22—H50 | 109.5 | B13—B15—B19 | 60.04 (10) |
H51—C22—H50 | 108.1 | B14—B15—B19 | 109.16 (12) |
C22—C23—C24 | 111.18 (15) | C18—B15—B20 | 106.56 (12) |
C22—C23—H52 | 109.4 | B13—B15—B20 | 108.61 (13) |
C24—C23—H52 | 109.4 | B14—B15—B20 | 60.66 (10) |
C22—C23—H53 | 109.4 | B19—B15—B20 | 60.66 (11) |
C24—C23—H53 | 109.4 | C18—B15—H39 | 120.7 (11) |
H52—C23—H53 | 108.0 | B13—B15—H39 | 118.6 (11) |
C19—C24—C23 | 111.23 (14) | B14—B15—H39 | 122.3 (11) |
C19—C24—H55 | 109.4 | B19—B15—H39 | 122.3 (11) |
C23—C24—H55 | 109.4 | B20—B15—H39 | 124.9 (11) |
C19—C24—H54 | 109.4 | B12—B16—B11 | 60.39 (10) |
C23—C24—H54 | 109.4 | B12—B16—B20 | 107.63 (12) |
H55—C24—H54 | 108.0 | B11—B16—B20 | 108.00 (12) |
N4—C25—C26 | 108.61 (13) | B12—B16—B18 | 59.72 (10) |
N4—C25—C30 | 111.66 (13) | B11—B16—B18 | 108.08 (12) |
C26—C25—C30 | 110.56 (13) | B20—B16—B18 | 59.75 (10) |
N4—C25—H56 | 108.7 | B12—B16—B14 | 107.63 (12) |
C26—C25—H56 | 108.7 | B11—B16—B14 | 59.60 (10) |
C30—C25—H56 | 108.7 | B20—B16—B14 | 60.10 (10) |
C25—C26—C27 | 113.27 (14) | B18—B16—B14 | 107.61 (12) |
C25—C26—H58 | 108.9 | B12—B16—H40 | 120.1 (11) |
C27—C26—H58 | 108.9 | B11—B16—H40 | 117.9 (11) |
C25—C26—H57 | 108.9 | B20—B16—H40 | 125.1 (11) |
C27—C26—H57 | 108.9 | B18—B16—H40 | 124.5 (11) |
H58—C26—H57 | 107.7 | B14—B16—H40 | 121.4 (11) |
C28—C27—C26 | 111.13 (15) | C17—B17—B18 | 104.46 (12) |
C28—C27—H59 | 109.4 | C17—B17—B19 | 104.33 (12) |
C26—C27—H59 | 109.4 | B18—B17—B19 | 60.48 (10) |
C28—C27—H60 | 109.4 | C17—B17—B12 | 58.72 (9) |
C26—C27—H60 | 109.4 | B18—B17—B12 | 59.72 (10) |
H59—C27—H60 | 108.0 | B19—B17—B12 | 108.06 (13) |
C27—C28—C29 | 110.30 (15) | C17—B17—B13 | 58.47 (9) |
C27—C28—H62 | 109.6 | B18—B17—B13 | 107.58 (12) |
C29—C28—H62 | 109.6 | B19—B17—B13 | 59.38 (10) |
C27—C28—H61 | 109.6 | B12—B17—B13 | 107.60 (12) |
C29—C28—H61 | 109.6 | C17—B17—H41 | 118.6 (11) |
H62—C28—H61 | 108.1 | B18—B17—H41 | 128.0 (11) |
C28—C29—C30 | 111.30 (16) | B19—B17—H41 | 126.8 (11) |
C28—C29—H64 | 109.4 | B12—B17—H41 | 120.2 (11) |
C30—C29—H64 | 109.4 | B13—B17—H41 | 118.9 (10) |
C28—C29—H63 | 109.4 | B12—B18—B17 | 60.26 (10) |
C30—C29—H63 | 109.4 | B12—B18—B20 | 107.87 (12) |
H64—C29—H63 | 108.0 | B17—B18—B20 | 108.12 (12) |
C29—C30—C25 | 112.63 (14) | B12—B18—B16 | 59.70 (10) |
C29—C30—H66 | 109.1 | B17—B18—B16 | 108.07 (12) |
C25—C30—H66 | 109.1 | B20—B18—B16 | 60.07 (10) |
C29—C30—H65 | 109.1 | B12—B18—B19 | 107.97 (12) |
C25—C30—H65 | 109.1 | B17—B18—B19 | 59.83 (10) |
H66—C30—H65 | 107.8 | B20—B18—B19 | 60.20 (10) |
C2—B1—C3 | 57.96 (9) | B16—B18—B19 | 108.13 (12) |
C2—B1—B8 | 104.58 (12) | B12—B18—H42 | 119.7 (11) |
C3—B1—B8 | 106.11 (12) | B17—B18—H42 | 121.0 (11) |
C2—B1—B7 | 104.15 (12) | B20—B18—H42 | 123.3 (11) |
C3—B1—B7 | 58.84 (9) | B16—B18—H42 | 121.0 (11) |
B8—B1—B7 | 59.89 (10) | B19—B18—H42 | 123.4 (11) |
C2—B1—B2 | 58.71 (9) | B13—B19—B15 | 59.65 (10) |
C3—B1—B2 | 106.24 (12) | B13—B19—B17 | 60.57 (10) |
B8—B1—B2 | 59.76 (10) | B15—B19—B17 | 107.90 (12) |
B7—B1—B2 | 107.37 (12) | B13—B19—B20 | 107.57 (13) |
C2—B1—H2 | 116.6 (11) | B15—B19—B20 | 59.75 (10) |
C3—B1—H2 | 117.3 (10) | B17—B19—B20 | 107.51 (13) |
B8—B1—H2 | 131.2 (10) | B13—B19—B18 | 107.90 (12) |
B7—B1—H2 | 127.0 (11) | B15—B19—B18 | 107.29 (13) |
B2—B1—H2 | 122.1 (11) | B17—B19—B18 | 59.69 (10) |
C2—B2—B5 | 104.64 (12) | B20—B19—B18 | 59.57 (10) |
C2—B2—B8 | 104.27 (12) | B13—B19—H43 | 120.9 (11) |
B5—B2—B8 | 60.46 (10) | B15—B19—H43 | 120.0 (11) |
C2—B2—B3 | 58.81 (9) | B17—B19—H43 | 123.3 (12) |
B5—B2—B3 | 59.75 (10) | B20—B19—H43 | 121.5 (11) |
B8—B2—B3 | 107.96 (13) | B18—B19—H43 | 123.9 (11) |
C2—B2—B1 | 58.34 (9) | B15—B20—B18 | 107.68 (13) |
B5—B2—B1 | 108.11 (12) | B15—B20—B16 | 107.67 (12) |
B8—B2—B1 | 59.73 (10) | B18—B20—B16 | 60.17 (10) |
B3—B2—B1 | 107.77 (12) | B15—B20—B14 | 59.51 (10) |
C2—B2—H3 | 117.5 (11) | B18—B20—B14 | 107.89 (13) |
B5—B2—H3 | 128.5 (11) | B16—B20—B14 | 60.03 (10) |
B8—B2—H3 | 127.9 (10) | B15—B20—B19 | 59.59 (10) |
B3—B2—H3 | 119.5 (10) | B18—B20—B19 | 60.22 (10) |
B1—B2—H3 | 118.5 (11) | B16—B20—B19 | 108.22 (13) |
C2—B3—B6 | 104.79 (12) | B14—B20—B19 | 107.40 (12) |
C2—B3—B5 | 104.76 (12) | B15—B20—H44 | 121.6 (11) |
B6—B3—B5 | 61.08 (10) | B18—B20—H44 | 122.9 (11) |
C2—B3—B2 | 58.75 (9) | B16—B20—H44 | 121.2 (11) |
B6—B3—B2 | 108.97 (12) | B14—B20—H44 | 120.6 (11) |
B5—B3—B2 | 59.97 (10) | B19—B20—H44 | 122.9 (11) |
C2—B3—B4 | 58.14 (9) | C1—N1—C4 | 120.66 (13) |
B6—B3—B4 | 60.13 (10) | C1—N1—SN | 117.98 (10) |
B5—B3—B4 | 108.62 (12) | C4—N1—SN | 121.02 (9) |
B2—B3—B4 | 107.85 (12) | C1—N2—C10 | 130.17 (13) |
C2—B3—H4 | 117.9 (11) | C1—N2—H1 | 114.2 (15) |
B6—B3—H4 | 126.0 (11) | C10—N2—H1 | 112.9 (15) |
B5—B3—H4 | 128.8 (11) | C16—N3—C19 | 121.43 (13) |
B2—B3—H4 | 120.7 (11) | C16—N3—SN | 119.37 (10) |
B4—B3—H4 | 117.2 (11) | C19—N3—SN | 119.02 (9) |
C2—B4—C3 | 57.74 (9) | C16—N4—C25 | 129.66 (13) |
C2—B4—B9 | 104.45 (11) | C16—N4—H34 | 114.1 (14) |
C3—B4—B9 | 58.94 (9) | C25—N4—H34 | 115.1 (14) |
C2—B4—B6 | 104.83 (12) | C3—SN—C18 | 100.12 (5) |
C3—B4—B6 | 106.21 (12) | C3—SN—N3 | 87.83 (5) |
B9—B4—B6 | 60.23 (10) | C18—SN—N3 | 73.27 (5) |
C2—B4—B3 | 58.90 (9) | C3—SN—N1 | 72.01 (5) |
C3—B4—B3 | 105.87 (12) | C18—SN—N1 | 100.52 (5) |
B9—B4—B3 | 107.31 (12) | N3—SN—N1 | 157.76 (4) |
N1—C1—C2—C3 | 9.78 (19) | B4—B9—B10—B5 | 0.57 (17) |
N2—C1—C2—C3 | −172.44 (12) | B6—B9—B10—B5 | 38.14 (12) |
N1—C1—C2—B4 | 80.50 (17) | C3—B9—B10—B6 | −100.36 (13) |
N2—C1—C2—B4 | −101.72 (15) | B7—B9—B10—B6 | −138.61 (13) |
N1—C1—C2—B1 | −59.61 (17) | B4—B9—B10—B6 | −37.58 (12) |
N2—C1—C2—B1 | 118.17 (14) | C3—B9—B10—B8 | 1.21 (16) |
N1—C1—C2—B2 | −132.02 (14) | B7—B9—B10—B8 | −37.04 (12) |
N2—C1—C2—B2 | 45.76 (18) | B4—B9—B10—B8 | 64.00 (15) |
N1—C1—C2—B3 | 153.77 (14) | B6—B9—B10—B8 | 101.57 (13) |
N2—C1—C2—B3 | −28.44 (19) | B3—B6—B10—B7 | 64.04 (15) |
C1—C2—C3—B7 | −147.19 (12) | B4—B6—B10—B7 | 0.39 (17) |
B4—C2—C3—B7 | 104.82 (12) | B9—B6—B10—B7 | −36.68 (12) |
B1—C2—C3—B7 | −40.73 (11) | B5—B6—B10—B7 | 100.90 (13) |
B2—C2—C3—B7 | −2.49 (16) | B3—B6—B10—B5 | −36.86 (12) |
B3—C2—C3—B7 | 65.81 (15) | B4—B6—B10—B5 | −100.51 (13) |
C1—C2—C3—B1 | −106.45 (14) | B9—B6—B10—B5 | −137.58 (13) |
B4—C2—C3—B1 | 145.55 (12) | B3—B6—B10—B9 | 100.72 (13) |
B2—C2—C3—B1 | 38.25 (12) | B4—B6—B10—B9 | 37.07 (12) |
B3—C2—C3—B1 | 106.55 (13) | B5—B6—B10—B9 | 137.58 (13) |
C1—C2—C3—B9 | 147.55 (12) | B3—B6—B10—B8 | 1.01 (16) |
B4—C2—C3—B9 | 39.56 (11) | B4—B6—B10—B8 | −62.64 (16) |
B1—C2—C3—B9 | −105.99 (12) | B9—B6—B10—B8 | −99.71 (13) |
B2—C2—C3—B9 | −67.75 (14) | B5—B6—B10—B8 | 37.87 (12) |
B3—C2—C3—B9 | 0.55 (15) | B1—B8—B10—B7 | −37.27 (12) |
C1—C2—C3—B4 | 107.99 (14) | B2—B8—B10—B7 | −101.16 (13) |
B1—C2—C3—B4 | −145.55 (12) | B5—B8—B10—B7 | −138.18 (12) |
B2—C2—C3—B4 | −107.30 (13) | B7—B8—B10—B5 | 138.18 (12) |
B3—C2—C3—B4 | −39.01 (11) | B1—B8—B10—B5 | 100.91 (13) |
C1—C2—C3—SN | 5.08 (15) | B2—B8—B10—B5 | 37.02 (12) |
B4—C2—C3—SN | −102.92 (10) | B7—B8—B10—B9 | 36.95 (12) |
B1—C2—C3—SN | 111.53 (11) | B1—B8—B10—B9 | −0.33 (16) |
B2—C2—C3—SN | 149.78 (10) | B2—B8—B10—B9 | −64.21 (15) |
B3—C2—C3—SN | −141.92 (10) | B5—B8—B10—B9 | −101.23 (13) |
N1—C4—C5—C6 | −173.15 (13) | B7—B8—B10—B6 | 100.13 (13) |
C9—C4—C5—C6 | −52.41 (18) | B1—B8—B10—B6 | 62.86 (16) |
C4—C5—C6—C7 | 58.06 (18) | B2—B8—B10—B6 | −1.03 (16) |
C5—C6—C7—C8 | −60.56 (18) | B5—B8—B10—B6 | −38.05 (12) |
C6—C7—C8—C9 | 58.22 (19) | C16—C17—B11—C18 | 105.20 (14) |
N1—C4—C9—C8 | 168.77 (13) | B13—C17—B11—C18 | −34.30 (12) |
C5—C4—C9—C8 | 49.31 (18) | B12—C17—B11—C18 | −139.71 (12) |
C7—C8—C9—C4 | −52.70 (19) | B17—C17—B11—C18 | −103.83 (13) |
N2—C10—C11—C12 | −68.30 (17) | C16—C17—B11—B14 | 142.37 (13) |
C15—C10—C11—C12 | 51.19 (17) | C18—C17—B11—B14 | 37.17 (11) |
C10—C11—C12—C13 | −53.98 (18) | B13—C17—B11—B14 | 2.87 (16) |
C11—C12—C13—C14 | 55.56 (18) | B12—C17—B11—B14 | −102.53 (12) |
C12—C13—C14—C15 | −54.77 (18) | B17—C17—B11—B14 | −66.66 (15) |
C13—C14—C15—C10 | 52.85 (18) | C16—C17—B11—B16 | −154.82 (13) |
N2—C10—C15—C14 | 71.29 (16) | C18—C17—B11—B16 | 99.97 (12) |
C11—C10—C15—C14 | −50.83 (17) | B13—C17—B11—B16 | 65.67 (15) |
N3—C16—C17—C18 | −17.75 (19) | B12—C17—B11—B16 | −39.73 (11) |
N4—C16—C17—C18 | 166.19 (12) | B17—C17—B11—B16 | −3.86 (16) |
N3—C16—C17—B11 | −88.99 (17) | C16—C17—B11—B12 | −115.09 (14) |
N4—C16—C17—B11 | 94.96 (16) | C18—C17—B11—B12 | 139.71 (12) |
N3—C16—C17—B13 | 50.91 (18) | B13—C17—B11—B12 | 105.40 (13) |
N4—C16—C17—B13 | −125.15 (14) | B17—C17—B11—B12 | 35.87 (12) |
N3—C16—C17—B12 | −164.23 (13) | B14—C18—B11—C17 | 136.75 (12) |
N4—C16—C17—B12 | 19.7 (2) | B15—C18—B11—C17 | 99.55 (13) |
N3—C16—C17—B17 | 121.40 (15) | B13—C18—B11—C17 | 33.27 (11) |
N4—C16—C17—B17 | −54.66 (18) | SN—C18—B11—C17 | −97.79 (12) |
C16—C17—C18—B14 | −151.20 (13) | C17—C18—B11—B14 | −136.75 (12) |
B11—C17—C18—B14 | −39.49 (12) | B15—C18—B11—B14 | −37.20 (12) |
B13—C17—C18—B14 | 104.88 (13) | B13—C18—B11—B14 | −103.47 (13) |
B12—C17—C18—B14 | −1.03 (16) | SN—C18—B11—B14 | 125.46 (13) |
B17—C17—C18—B14 | 67.08 (15) | C17—C18—B11—B16 | −97.55 (12) |
C16—C17—C18—B15 | 143.46 (12) | B14—C18—B11—B16 | 39.20 (11) |
B11—C17—C18—B15 | −104.83 (12) | B15—C18—B11—B16 | 2.00 (16) |
B13—C17—C18—B15 | 39.54 (11) | B13—C18—B11—B16 | −64.28 (15) |
B12—C17—C18—B15 | −66.37 (15) | SN—C18—B11—B16 | 164.66 (10) |
B17—C17—C18—B15 | 1.74 (15) | C17—C18—B11—B12 | −35.15 (11) |
C16—C17—C18—B13 | 103.92 (14) | B14—C18—B11—B12 | 101.59 (13) |
B11—C17—C18—B13 | −144.37 (12) | B15—C18—B11—B12 | 64.39 (15) |
B12—C17—C18—B13 | −105.91 (13) | B13—C18—B11—B12 | −1.88 (16) |
B17—C17—C18—B13 | −37.80 (12) | SN—C18—B11—B12 | −132.95 (11) |
C16—C17—C18—B11 | −111.71 (14) | C16—C17—B12—B16 | 148.88 (14) |
B13—C17—C18—B11 | 144.37 (12) | C18—C17—B12—B16 | 1.50 (16) |
B12—C17—C18—B11 | 38.46 (12) | B11—C17—B12—B16 | 39.76 (12) |
B17—C17—C18—B11 | 106.57 (13) | B13—C17—B12—B16 | −66.43 (15) |
C16—C17—C18—SN | 7.26 (15) | B17—C17—B12—B16 | −103.14 (13) |
B11—C17—C18—SN | 118.98 (11) | C16—C17—B12—B18 | −148.24 (14) |
B13—C17—C18—SN | −96.66 (10) | C18—C17—B12—B18 | 64.38 (15) |
B12—C17—C18—SN | 157.43 (10) | B11—C17—B12—B18 | 102.65 (13) |
B17—C17—C18—SN | −134.46 (10) | B13—C17—B12—B18 | −3.54 (16) |
N3—C19—C20—C21 | 178.08 (14) | B17—C17—B12—B18 | −40.25 (11) |
C24—C19—C20—C21 | 57.83 (18) | C16—C17—B12—B17 | −107.99 (15) |
C19—C20—C21—C22 | −56.6 (2) | C18—C17—B12—B17 | 104.63 (13) |
C20—C21—C22—C23 | 54.5 (2) | B11—C17—B12—B17 | 142.90 (13) |
C21—C22—C23—C24 | −55.4 (2) | B13—C17—B12—B17 | 36.71 (12) |
N3—C19—C24—C23 | −179.02 (13) | C16—C17—B12—B11 | 109.11 (15) |
C20—C19—C24—C23 | −58.72 (18) | C18—C17—B12—B11 | −38.27 (12) |
C22—C23—C24—C19 | 58.64 (19) | B13—C17—B12—B11 | −106.19 (13) |
N4—C25—C26—C27 | −71.10 (17) | B17—C17—B12—B11 | −142.90 (13) |
C30—C25—C26—C27 | 51.73 (18) | C18—B11—B12—C17 | 34.51 (10) |
C25—C26—C27—C28 | −54.8 (2) | B14—B11—B12—C17 | 96.13 (12) |
C26—C27—C28—C29 | 56.3 (2) | B16—B11—B12—C17 | 134.32 (13) |
C27—C28—C29—C30 | −56.9 (2) | C17—B11—B12—B16 | −134.32 (13) |
C28—C29—C30—C25 | 55.4 (2) | C18—B11—B12—B16 | −99.82 (13) |
N4—C25—C30—C29 | 69.15 (18) | B14—B11—B12—B16 | −38.20 (11) |
C26—C25—C30—C29 | −51.88 (19) | C17—B11—B12—B18 | −96.59 (13) |
C1—C2—B1—C3 | 107.58 (14) | C18—B11—B12—B18 | −62.08 (14) |
B4—C2—B1—C3 | −33.43 (12) | B14—B11—B12—B18 | −0.46 (15) |
B2—C2—B1—C3 | −140.02 (12) | B16—B11—B12—B18 | 37.73 (12) |
B3—C2—B1—C3 | −103.55 (13) | C17—B11—B12—B17 | −33.01 (11) |
C1—C2—B1—B8 | −152.32 (12) | C18—B11—B12—B17 | 1.50 (15) |
C3—C2—B1—B8 | 100.10 (12) | B14—B11—B12—B17 | 63.12 (15) |
B4—C2—B1—B8 | 66.67 (15) | B16—B11—B12—B17 | 101.32 (13) |
B2—C2—B1—B8 | −39.92 (11) | C16—C17—B13—C18 | −107.71 (13) |
B3—C2—B1—B8 | −3.45 (16) | B11—C17—B13—C18 | 34.44 (11) |
C1—C2—B1—B7 | 145.65 (13) | B12—C17—B13—C18 | 103.84 (13) |
C3—C2—B1—B7 | 38.07 (11) | B17—C17—B13—C18 | 140.42 (12) |
B4—C2—B1—B7 | 4.64 (16) | C16—C17—B13—B15 | −145.65 (13) |
B2—C2—B1—B7 | −101.95 (13) | C18—C17—B13—B15 | −37.94 (11) |
B3—C2—B1—B7 | −65.48 (15) | B11—C17—B13—B15 | −3.50 (16) |
C1—C2—B1—B2 | −112.40 (14) | B12—C17—B13—B15 | 65.90 (15) |
C3—C2—B1—B2 | 140.02 (12) | B17—C17—B13—B15 | 102.48 (13) |
B4—C2—B1—B2 | 106.59 (13) | C16—C17—B13—B19 | 151.72 (13) |
B3—C2—B1—B2 | 36.47 (12) | C18—C17—B13—B19 | −100.57 (13) |
B7—C3—B1—C2 | 135.68 (12) | B11—C17—B13—B19 | −66.13 (15) |
B9—C3—B1—C2 | 98.90 (13) | B12—C17—B13—B19 | 3.27 (16) |
B4—C3—B1—C2 | 31.95 (11) | B17—C17—B13—B19 | 39.85 (12) |
SN—C3—B1—C2 | −102.23 (11) | C16—C17—B13—B17 | 111.87 (14) |
C2—C3—B1—B8 | −97.38 (13) | C18—C17—B13—B17 | −140.42 (12) |
B7—C3—B1—B8 | 38.30 (11) | B11—C17—B13—B17 | −105.98 (13) |
B9—C3—B1—B8 | 1.52 (16) | B12—C17—B13—B17 | −36.58 (12) |
B4—C3—B1—B8 | −65.43 (15) | B14—C18—B13—C17 | −100.00 (12) |
SN—C3—B1—B8 | 160.39 (10) | B15—C18—B13—C17 | −136.32 (12) |
C2—C3—B1—B7 | −135.68 (12) | B11—C18—B13—C17 | −33.14 (11) |
B9—C3—B1—B7 | −36.78 (12) | SN—C18—B13—C17 | 107.00 (9) |
B4—C3—B1—B7 | −103.73 (13) | C17—C18—B13—B15 | 136.32 (12) |
SN—C3—B1—B7 | 122.09 (12) | B14—C18—B13—B15 | 36.32 (12) |
C2—C3—B1—B2 | −34.88 (11) | B11—C18—B13—B15 | 103.18 (13) |
B7—C3—B1—B2 | 100.80 (13) | SN—C18—B13—B15 | −116.69 (10) |
B9—C3—B1—B2 | 64.02 (15) | C17—C18—B13—B19 | 97.56 (12) |
B4—C3—B1—B2 | −2.94 (15) | B14—C18—B13—B19 | −2.44 (16) |
SN—C3—B1—B2 | −137.11 (10) | B15—C18—B13—B19 | −38.75 (12) |
C1—C2—B2—B5 | −151.87 (13) | B11—C18—B13—B19 | 64.42 (15) |
C3—C2—B2—B5 | 64.87 (15) | SN—C18—B13—B19 | −155.44 (10) |
B4—C2—B2—B5 | −3.77 (16) | C17—C18—B13—B17 | 34.64 (11) |
B1—C2—B2—B5 | 102.49 (13) | B14—C18—B13—B17 | −65.37 (15) |
B3—C2—B2—B5 | −39.93 (11) | B15—C18—B13—B17 | −101.68 (13) |
C1—C2—B2—B8 | 145.47 (13) | B11—C18—B13—B17 | 1.50 (16) |
C3—C2—B2—B8 | 2.22 (16) | SN—C18—B13—B17 | 141.63 (10) |
B4—C2—B2—B8 | −66.43 (15) | C17—C18—B14—B15 | −101.25 (13) |
B1—C2—B2—B8 | 39.83 (11) | B13—C18—B14—B15 | −36.09 (12) |
B3—C2—B2—B8 | −102.59 (13) | B11—C18—B14—B15 | −140.24 (12) |
C1—C2—B2—B3 | −111.94 (15) | SN—C18—B14—B15 | 106.78 (14) |
C3—C2—B2—B3 | 104.81 (13) | C17—C18—B14—B11 | 38.99 (11) |
B4—C2—B2—B3 | 36.16 (12) | B15—C18—B14—B11 | 140.24 (12) |
B1—C2—B2—B3 | 142.42 (13) | B13—C18—B14—B11 | 104.15 (13) |
C1—C2—B2—B1 | 105.64 (15) | SN—C18—B14—B11 | −112.98 (14) |
C3—C2—B2—B1 | −37.62 (11) | C17—C18—B14—B16 | 0.10 (16) |
B4—C2—B2—B1 | −106.26 (14) | B15—C18—B14—B16 | 101.35 (13) |
B3—C2—B2—B1 | −142.42 (13) | B13—C18—B14—B16 | 65.26 (15) |
C3—B1—B2—C2 | 34.56 (10) | B11—C18—B14—B16 | −38.89 (12) |
B8—B1—B2—C2 | 134.05 (13) | SN—C18—B14—B16 | −151.87 (11) |
B7—B1—B2—C2 | 96.29 (12) | C17—C18—B14—B20 | −62.60 (15) |
C2—B1—B2—B5 | −96.36 (13) | B15—C18—B14—B20 | 38.65 (12) |
C3—B1—B2—B5 | −61.80 (14) | B13—C18—B14—B20 | 2.55 (16) |
B8—B1—B2—B5 | 37.68 (12) | B11—C18—B14—B20 | −101.59 (13) |
B7—B1—B2—B5 | −0.07 (15) | SN—C18—B14—B20 | 145.43 (12) |
C2—B1—B2—B8 | −134.05 (13) | C17—B11—B14—C18 | −36.56 (10) |
C3—B1—B2—B8 | −99.48 (13) | B16—B11—B14—C18 | −135.84 (12) |
B7—B1—B2—B8 | −37.75 (11) | B12—B11—B14—C18 | −98.03 (12) |
C2—B1—B2—B3 | −33.22 (11) | C17—B11—B14—B15 | −1.01 (15) |
C3—B1—B2—B3 | 1.35 (15) | C18—B11—B14—B15 | 35.55 (11) |
B8—B1—B2—B3 | 100.83 (13) | B16—B11—B14—B15 | −100.29 (13) |
B7—B1—B2—B3 | 63.08 (15) | B12—B11—B14—B15 | −62.48 (15) |
C1—C2—B3—B6 | −146.16 (13) | C17—B11—B14—B16 | 99.28 (12) |
C3—C2—B3—B6 | −0.90 (15) | C18—B11—B14—B16 | 135.84 (12) |
B4—C2—B3—B6 | −39.60 (11) | B12—B11—B14—B16 | 37.81 (11) |
B1—C2—B3—B6 | 66.81 (15) | C17—B11—B14—B20 | 62.34 (14) |
B2—C2—B3—B6 | 103.47 (13) | C18—B11—B14—B20 | 98.91 (13) |
C1—C2—B3—B5 | 150.44 (13) | B16—B11—B14—B20 | −36.93 (12) |
C3—C2—B3—B5 | −64.31 (15) | B12—B11—B14—B20 | 0.88 (15) |
B4—C2—B3—B5 | −103.00 (13) | C17—C18—B15—B13 | −39.43 (11) |
B1—C2—B3—B5 | 3.41 (16) | B14—C18—B15—B13 | −141.25 (12) |
B2—C2—B3—B5 | 40.07 (11) | B11—C18—B15—B13 | −104.07 (13) |
C1—C2—B3—B2 | 110.37 (15) | SN—C18—B15—B13 | 92.39 (11) |
C3—C2—B3—B2 | −104.37 (13) | C17—C18—B15—B14 | 101.82 (12) |
B4—C2—B3—B2 | −143.07 (12) | B13—C18—B15—B14 | 141.25 (12) |
B1—C2—B3—B2 | −36.66 (12) | B11—C18—B15—B14 | 37.18 (12) |
C1—C2—B3—B4 | −106.56 (15) | SN—C18—B15—B14 | −126.36 (12) |
C3—C2—B3—B4 | 38.70 (11) | C17—C18—B15—B19 | −0.84 (15) |
B1—C2—B3—B4 | 106.41 (13) | B14—C18—B15—B19 | −102.66 (13) |
B2—C2—B3—B4 | 143.07 (12) | B13—C18—B15—B19 | 38.59 (11) |
B5—B2—B3—C2 | 134.04 (13) | B11—C18—B15—B19 | −65.48 (15) |
B8—B2—B3—C2 | 96.12 (13) | SN—C18—B15—B19 | 130.98 (11) |
B1—B2—B3—C2 | 33.03 (11) | C17—C18—B15—B20 | 62.76 (15) |
C2—B2—B3—B6 | −96.15 (13) | B14—C18—B15—B20 | −39.05 (12) |
B5—B2—B3—B6 | 37.88 (12) | B13—C18—B15—B20 | 102.20 (13) |
B8—B2—B3—B6 | −0.03 (16) | B11—C18—B15—B20 | −1.88 (16) |
B1—B2—B3—B6 | −63.12 (15) | SN—C18—B15—B20 | −165.42 (10) |
C2—B2—B3—B5 | −134.04 (13) | C17—B13—B15—C18 | 36.98 (10) |
B8—B2—B3—B5 | −37.91 (12) | B19—B13—B15—C18 | 136.41 (12) |
B1—B2—B3—B5 | −101.00 (13) | B17—B13—B15—C18 | 98.56 (12) |
C2—B2—B3—B4 | −32.42 (11) | C17—B13—B15—B14 | 2.62 (16) |
B5—B2—B3—B4 | 101.62 (13) | C18—B13—B15—B14 | −34.36 (11) |
B8—B2—B3—B4 | 63.71 (15) | B19—B13—B15—B14 | 102.05 (13) |
B1—B2—B3—B4 | 0.61 (16) | B17—B13—B15—B14 | 64.20 (15) |
C1—C2—B4—C3 | −107.44 (14) | C17—B13—B15—B19 | −99.43 (13) |
B1—C2—B4—C3 | 33.14 (11) | C18—B13—B15—B19 | −136.41 (12) |
B2—C2—B4—C3 | 103.35 (13) | B17—B13—B15—B19 | −37.85 (12) |
B3—C2—B4—C3 | 139.32 (12) | C17—B13—B15—B20 | −61.69 (15) |
C1—C2—B4—B9 | −145.02 (13) | C18—B13—B15—B20 | −98.67 (13) |
C3—C2—B4—B9 | −37.58 (11) | B19—B13—B15—B20 | 37.74 (12) |
B1—C2—B4—B9 | −4.44 (16) | B17—B13—B15—B20 | −0.11 (17) |
B2—C2—B4—B9 | 65.77 (15) | B11—B14—B15—C18 | −35.64 (11) |
B3—C2—B4—B9 | 101.74 (13) | B16—B14—B15—C18 | −98.93 (13) |
C1—C2—B4—B6 | 152.51 (13) | B20—B14—B15—C18 | −136.15 (12) |
C3—C2—B4—B6 | −100.05 (12) | C18—B14—B15—B13 | 34.61 (11) |
B1—C2—B4—B6 | −66.91 (15) | B11—B14—B15—B13 | −1.03 (16) |
B2—C2—B4—B6 | 3.30 (16) | B16—B14—B15—B13 | −64.33 (15) |
B3—C2—B4—B6 | 39.27 (11) | B20—B14—B15—B13 | −101.54 (14) |
C1—C2—B4—B3 | 113.24 (14) | C18—B14—B15—B19 | 98.37 (13) |
C3—C2—B4—B3 | −139.32 (12) | B11—B14—B15—B19 | 62.74 (15) |
B1—C2—B4—B3 | −106.18 (13) | B16—B14—B15—B19 | −0.56 (16) |
B2—C2—B4—B3 | −35.97 (12) | B20—B14—B15—B19 | −37.77 (12) |
B7—C3—B4—C2 | −99.80 (13) | C18—B14—B15—B20 | 136.15 (12) |
B1—C3—B4—C2 | −32.16 (11) | B11—B14—B15—B20 | 100.51 (13) |
B9—C3—B4—C2 | −136.42 (12) | B16—B14—B15—B20 | 37.21 (12) |
SN—C3—B4—C2 | 105.36 (10) | C17—B12—B16—B11 | −39.06 (11) |
C2—C3—B4—B9 | 136.42 (12) | B18—B12—B16—B11 | −138.18 (12) |
B7—C3—B4—B9 | 36.62 (12) | B17—B12—B16—B11 | −100.81 (13) |
B1—C3—B4—B9 | 104.26 (13) | C17—B12—B16—B20 | 62.03 (15) |
SN—C3—B4—B9 | −118.22 (11) | B18—B12—B16—B20 | −37.10 (11) |
C2—C3—B4—B6 | 97.56 (13) | B17—B12—B16—B20 | 0.27 (16) |
B7—C3—B4—B6 | −2.24 (16) | B11—B12—B16—B20 | 101.09 (13) |
B1—C3—B4—B6 | 65.40 (15) | C17—B12—B16—B18 | 99.13 (12) |
B9—C3—B4—B6 | −38.86 (11) | B17—B12—B16—B18 | 37.37 (11) |
SN—C3—B4—B6 | −157.08 (10) | B11—B12—B16—B18 | 138.18 (12) |
C2—C3—B4—B3 | 35.47 (10) | C17—B12—B16—B14 | −1.36 (16) |
B7—C3—B4—B3 | −64.33 (15) | B18—B12—B16—B14 | −100.49 (13) |
B1—C3—B4—B3 | 3.31 (15) | B17—B12—B16—B14 | −63.12 (15) |
B9—C3—B4—B3 | −100.95 (13) | B11—B12—B16—B14 | 37.70 (12) |
SN—C3—B4—B3 | 140.83 (10) | C17—B11—B16—B12 | 39.35 (11) |
B6—B3—B4—C2 | 134.71 (12) | C18—B11—B16—B12 | 99.16 (12) |
B5—B3—B4—C2 | 96.15 (13) | B14—B11—B16—B12 | 137.49 (13) |
B2—B3—B4—C2 | 32.66 (11) | C17—B11—B16—B20 | −61.12 (15) |
C2—B3—B4—C3 | −34.97 (10) | C18—B11—B16—B20 | −1.30 (16) |
B6—B3—B4—C3 | 99.74 (12) | B14—B11—B16—B20 | 37.03 (12) |
B5—B3—B4—C3 | 61.19 (15) | B12—B11—B16—B20 | −100.47 (13) |
B2—B3—B4—C3 | −2.31 (15) | C17—B11—B16—B18 | 2.07 (15) |
C2—B3—B4—B9 | −96.73 (12) | C18—B11—B16—B18 | 61.88 (15) |
B6—B3—B4—B9 | 37.99 (12) | B14—B11—B16—B18 | 100.22 (13) |
B5—B3—B4—B9 | −0.57 (16) | B12—B11—B16—B18 | −37.28 (11) |
B2—B3—B4—B9 | −64.07 (15) | C17—B11—B16—B14 | −98.15 (12) |
C2—B3—B4—B6 | −134.71 (12) | C18—B11—B16—B14 | −38.33 (11) |
B5—B3—B4—B6 | −38.56 (12) | B12—B11—B16—B14 | −137.49 (13) |
B2—B3—B4—B6 | −102.05 (13) | C18—B14—B16—B12 | 0.81 (16) |
C2—B3—B5—B2 | −39.46 (11) | B15—B14—B16—B12 | 63.40 (15) |
B6—B3—B5—B2 | −138.44 (13) | B11—B14—B16—B12 | −38.05 (12) |
B4—B3—B5—B2 | −100.30 (13) | B20—B14—B16—B12 | 100.60 (14) |
C2—B3—B5—B10 | 61.76 (15) | C18—B14—B16—B11 | 38.86 (11) |
B6—B3—B5—B10 | −37.21 (12) | B15—B14—B16—B11 | 101.45 (13) |
B2—B3—B5—B10 | 101.22 (14) | B20—B14—B16—B11 | 138.65 (13) |
B4—B3—B5—B10 | 0.92 (16) | C18—B14—B16—B20 | −99.79 (13) |
C2—B3—B5—B8 | −1.88 (16) | B15—B14—B16—B20 | −37.20 (12) |
B6—B3—B5—B8 | −100.85 (14) | B11—B14—B16—B20 | −138.65 (13) |
B2—B3—B5—B8 | 37.58 (12) | C18—B14—B16—B18 | −62.17 (15) |
B4—B3—B5—B8 | −62.72 (15) | B15—B14—B16—B18 | 0.42 (16) |
C2—B3—B5—B6 | 98.98 (13) | B11—B14—B16—B18 | −101.03 (13) |
B2—B3—B5—B6 | 138.44 (13) | B20—B14—B16—B18 | 37.61 (12) |
B4—B3—B5—B6 | 38.14 (12) | C16—C17—B17—B18 | 155.18 (13) |
C2—B2—B5—B3 | 39.46 (11) | C18—C17—B17—B18 | −64.51 (14) |
B8—B2—B5—B3 | 137.79 (13) | B11—C17—B17—B18 | 3.99 (16) |
B1—B2—B5—B3 | 100.44 (13) | B13—C17—B17—B18 | −101.99 (13) |
C2—B2—B5—B10 | −60.92 (15) | B12—C17—B17—B18 | 40.00 (11) |
B8—B2—B5—B10 | 37.41 (12) | C16—C17—B17—B19 | −142.16 (13) |
B3—B2—B5—B10 | −100.39 (13) | C18—C17—B17—B19 | −1.86 (15) |
B1—B2—B5—B10 | 0.05 (16) | B11—C17—B17—B19 | 66.64 (15) |
C2—B2—B5—B8 | −98.33 (13) | B13—C17—B17—B19 | −39.33 (11) |
B3—B2—B5—B8 | −137.79 (13) | B12—C17—B17—B19 | 102.66 (13) |
B1—B2—B5—B8 | −37.36 (11) | C16—C17—B17—B12 | 115.18 (14) |
C2—B2—B5—B6 | 2.59 (16) | C18—C17—B17—B12 | −104.51 (13) |
B8—B2—B5—B6 | 100.92 (13) | B11—C17—B17—B12 | −36.02 (12) |
B3—B2—B5—B6 | −36.87 (12) | B13—C17—B17—B12 | −141.99 (12) |
B1—B2—B5—B6 | 63.56 (15) | C16—C17—B17—B13 | −102.83 (14) |
C2—B3—B6—B4 | 38.63 (11) | C18—C17—B17—B13 | 37.47 (11) |
B5—B3—B6—B4 | 137.56 (13) | B11—C17—B17—B13 | 105.97 (13) |
B2—B3—B6—B4 | 100.16 (13) | B12—C17—B17—B13 | 141.99 (12) |
C2—B3—B6—B9 | 0.88 (15) | B16—B12—B17—C17 | 96.27 (12) |
B5—B3—B6—B9 | 99.81 (13) | B18—B12—B17—C17 | 133.88 (12) |
B2—B3—B6—B9 | 62.41 (15) | B11—B12—B17—C17 | 32.78 (11) |
B4—B3—B6—B9 | −37.75 (11) | C17—B12—B17—B18 | −133.88 (12) |
C2—B3—B6—B10 | −62.14 (14) | B16—B12—B17—B18 | −37.61 (12) |
B5—B3—B6—B10 | 36.80 (12) | B11—B12—B17—B18 | −101.11 (13) |
B2—B3—B6—B10 | −0.60 (16) | C17—B12—B17—B19 | −96.11 (13) |
B4—B3—B6—B10 | −100.76 (13) | B16—B12—B17—B19 | 0.16 (16) |
C2—B3—B6—B5 | −98.93 (13) | B18—B12—B17—B19 | 37.77 (12) |
B2—B3—B6—B5 | −37.40 (12) | B11—B12—B17—B19 | −63.34 (15) |
B4—B3—B6—B5 | −137.56 (13) | C17—B12—B17—B13 | −33.41 (11) |
C2—B4—B6—B3 | −39.01 (11) | B16—B12—B17—B13 | 62.85 (15) |
C3—B4—B6—B3 | −99.14 (13) | B18—B12—B17—B13 | 100.47 (13) |
B9—B4—B6—B3 | −137.40 (13) | B11—B12—B17—B13 | −0.64 (16) |
C2—B4—B6—B9 | 98.39 (12) | C18—B13—B17—C17 | −34.00 (11) |
C3—B4—B6—B9 | 38.25 (11) | B15—B13—B17—C17 | −96.51 (13) |
B3—B4—B6—B9 | 137.40 (13) | B19—B13—B17—C17 | −134.47 (13) |
C2—B4—B6—B10 | 61.20 (15) | C17—B13—B17—B18 | 96.49 (13) |
C3—B4—B6—B10 | 1.07 (16) | C18—B13—B17—B18 | 62.49 (15) |
B9—B4—B6—B10 | −37.19 (12) | B15—B13—B17—B18 | −0.02 (16) |
B3—B4—B6—B10 | 100.21 (13) | B19—B13—B17—B18 | −37.99 (12) |
C2—B4—B6—B5 | −1.40 (16) | C17—B13—B17—B19 | 134.47 (13) |
C3—B4—B6—B5 | −61.53 (15) | C18—B13—B17—B19 | 100.47 (13) |
B9—B4—B6—B5 | −99.79 (13) | B15—B13—B17—B19 | 37.96 (12) |
B3—B4—B6—B5 | 37.61 (12) | C17—B13—B17—B12 | 33.51 (11) |
B2—B5—B6—B3 | 37.25 (12) | C18—B13—B17—B12 | −0.49 (16) |
B10—B5—B6—B3 | 138.32 (13) | B15—B13—B17—B12 | −63.00 (15) |
B8—B5—B6—B3 | 100.45 (13) | B19—B13—B17—B12 | −100.96 (14) |
B3—B5—B6—B4 | −38.02 (12) | C17—B12—B18—B17 | 39.77 (11) |
B2—B5—B6—B4 | −0.77 (16) | B16—B12—B18—B17 | 138.38 (12) |
B10—B5—B6—B4 | 100.30 (13) | B11—B12—B18—B17 | 100.95 (13) |
B8—B5—B6—B4 | 62.43 (15) | C17—B12—B18—B20 | −61.31 (15) |
B3—B5—B6—B9 | −100.73 (13) | B16—B12—B18—B20 | 37.30 (11) |
B2—B5—B6—B9 | −63.47 (15) | B17—B12—B18—B20 | −101.08 (13) |
B10—B5—B6—B9 | 37.59 (12) | B11—B12—B18—B20 | −0.13 (16) |
B8—B5—B6—B9 | −0.27 (16) | C17—B12—B18—B16 | −98.61 (12) |
B3—B5—B6—B10 | −138.32 (13) | B17—B12—B18—B16 | −138.38 (12) |
B2—B5—B6—B10 | −101.07 (13) | B11—B12—B18—B16 | −37.43 (11) |
B8—B5—B6—B10 | −37.87 (12) | C17—B12—B18—B19 | 2.31 (16) |
C2—C3—B7—B9 | −100.94 (13) | B16—B12—B18—B19 | 100.92 (13) |
B1—C3—B7—B9 | −140.97 (13) | B17—B12—B18—B19 | −37.46 (12) |
B4—C3—B7—B9 | −36.56 (12) | B11—B12—B18—B19 | 63.49 (15) |
SN—C3—B7—B9 | 112.68 (13) | C17—B17—B18—B12 | −39.50 (11) |
C2—C3—B7—B8 | 1.63 (15) | B19—B17—B18—B12 | −137.99 (13) |
B1—C3—B7—B8 | −38.40 (12) | B13—B17—B18—B12 | −100.50 (13) |
B9—C3—B7—B8 | 102.57 (13) | C17—B17—B18—B20 | 61.15 (15) |
B4—C3—B7—B8 | 66.01 (15) | B19—B17—B18—B20 | −37.34 (12) |
SN—C3—B7—B8 | −144.74 (11) | B12—B17—B18—B20 | 100.65 (14) |
C2—C3—B7—B10 | −61.89 (15) | B13—B17—B18—B20 | 0.15 (17) |
B1—C3—B7—B10 | −101.92 (13) | C17—B17—B18—B16 | −2.40 (16) |
B9—C3—B7—B10 | 39.05 (12) | B19—B17—B18—B16 | −100.89 (13) |
B4—C3—B7—B10 | 2.49 (16) | B12—B17—B18—B16 | 37.10 (12) |
SN—C3—B7—B10 | 151.74 (11) | B13—B17—B18—B16 | −63.40 (15) |
C2—C3—B7—B1 | 40.03 (11) | C17—B17—B18—B19 | 98.49 (13) |
B9—C3—B7—B1 | 140.97 (13) | B12—B17—B18—B19 | 137.99 (13) |
B4—C3—B7—B1 | 104.41 (13) | B13—B17—B18—B19 | 37.49 (12) |
SN—C3—B7—B1 | −106.35 (13) | B11—B16—B18—B12 | 37.58 (11) |
C2—B1—B7—C3 | −37.65 (10) | B20—B16—B18—B12 | 138.29 (12) |
B8—B1—B7—C3 | −136.50 (12) | B14—B16—B18—B12 | 100.52 (13) |
B2—B1—B7—C3 | −98.81 (12) | B12—B16—B18—B17 | −37.35 (11) |
C2—B1—B7—B9 | −2.85 (15) | B11—B16—B18—B17 | 0.23 (16) |
C3—B1—B7—B9 | 34.80 (11) | B20—B16—B18—B17 | 100.94 (13) |
B8—B1—B7—B9 | −101.70 (13) | B14—B16—B18—B17 | 63.17 (15) |
B2—B1—B7—B9 | −64.01 (15) | B12—B16—B18—B20 | −138.29 (12) |
C2—B1—B7—B8 | 98.86 (13) | B11—B16—B18—B20 | −100.71 (13) |
C3—B1—B7—B8 | 136.50 (12) | B14—B16—B18—B20 | −37.77 (12) |
B2—B1—B7—B8 | 37.69 (11) | B12—B16—B18—B19 | −100.64 (13) |
C2—B1—B7—B10 | 61.23 (14) | B11—B16—B18—B19 | −63.07 (15) |
C3—B1—B7—B10 | 98.87 (13) | B20—B16—B18—B19 | 37.64 (12) |
B8—B1—B7—B10 | −37.63 (12) | B14—B16—B18—B19 | −0.12 (16) |
B2—B1—B7—B10 | 0.06 (16) | C17—B13—B19—B15 | 98.36 (13) |
C3—B7—B8—B1 | 37.94 (11) | C18—B13—B19—B15 | 38.38 (11) |
B9—B7—B8—B1 | 100.57 (13) | B17—B13—B19—B15 | 137.67 (13) |
B10—B7—B8—B1 | 138.37 (12) | C17—B13—B19—B17 | −39.31 (11) |
C3—B7—B8—B2 | −0.27 (16) | C18—B13—B19—B17 | −99.29 (13) |
B9—B7—B8—B2 | 62.35 (16) | B15—B13—B19—B17 | −137.67 (13) |
B10—B7—B8—B2 | 100.15 (13) | C17—B13—B19—B20 | 61.28 (15) |
B1—B7—B8—B2 | −38.22 (12) | C18—B13—B19—B20 | 1.30 (16) |
C3—B7—B8—B5 | −63.36 (15) | B15—B13—B19—B20 | −37.08 (12) |
B9—B7—B8—B5 | −0.73 (16) | B17—B13—B19—B20 | 100.59 (13) |
B10—B7—B8—B5 | 37.07 (11) | C17—B13—B19—B18 | −1.60 (16) |
B1—B7—B8—B5 | −101.30 (13) | C18—B13—B19—B18 | −61.58 (15) |
C3—B7—B8—B10 | −100.43 (13) | B15—B13—B19—B18 | −99.95 (14) |
B9—B7—B8—B10 | −37.80 (12) | B17—B13—B19—B18 | 37.71 (12) |
B1—B7—B8—B10 | −138.37 (12) | C18—B15—B19—B13 | −38.34 (11) |
C2—B1—B8—B7 | −98.12 (13) | B14—B15—B19—B13 | −100.51 (13) |
C3—B1—B8—B7 | −37.81 (11) | B20—B15—B19—B13 | −138.29 (13) |
B2—B1—B8—B7 | −137.51 (13) | C18—B15—B19—B17 | −0.29 (16) |
C2—B1—B8—B2 | 39.40 (11) | B13—B15—B19—B17 | 38.05 (12) |
C3—B1—B8—B2 | 99.70 (13) | B14—B15—B19—B17 | −62.46 (16) |
B7—B1—B8—B2 | 137.51 (13) | B20—B15—B19—B17 | −100.23 (13) |
C2—B1—B8—B5 | 2.02 (16) | C18—B15—B19—B20 | 99.94 (13) |
C3—B1—B8—B5 | 62.32 (15) | B13—B15—B19—B20 | 138.29 (13) |
B7—B1—B8—B5 | 100.13 (13) | B14—B15—B19—B20 | 37.77 (12) |
B2—B1—B8—B5 | −37.38 (12) | C18—B15—B19—B18 | 62.65 (15) |
C2—B1—B8—B10 | −60.99 (15) | B13—B15—B19—B18 | 100.99 (13) |
C3—B1—B8—B10 | −0.69 (16) | B14—B15—B19—B18 | 0.48 (17) |
B7—B1—B8—B10 | 37.12 (12) | B20—B15—B19—B18 | −37.29 (12) |
B2—B1—B8—B10 | −100.39 (13) | C17—B17—B19—B13 | 38.89 (11) |
C2—B2—B8—B7 | −1.11 (16) | B18—B17—B19—B13 | 137.60 (13) |
B5—B2—B8—B7 | −100.07 (13) | B12—B17—B19—B13 | 100.17 (13) |
B3—B2—B8—B7 | −62.47 (15) | C17—B17—B19—B15 | 1.24 (16) |
B1—B2—B8—B7 | 38.04 (12) | B18—B17—B19—B15 | 99.96 (14) |
C2—B2—B8—B1 | −39.15 (11) | B12—B17—B19—B15 | 62.53 (15) |
B5—B2—B8—B1 | −138.10 (13) | B13—B17—B19—B15 | −37.64 (12) |
B3—B2—B8—B1 | −100.51 (13) | C17—B17—B19—B20 | −61.80 (14) |
C2—B2—B8—B5 | 98.95 (12) | B18—B17—B19—B20 | 36.91 (12) |
B3—B2—B8—B5 | 37.60 (12) | B12—B17—B19—B20 | −0.52 (16) |
B1—B2—B8—B5 | 138.10 (13) | B13—B17—B19—B20 | −100.69 (13) |
C2—B2—B8—B10 | 62.01 (15) | C17—B17—B19—B18 | −98.72 (12) |
B5—B2—B8—B10 | −36.95 (12) | B12—B17—B19—B18 | −37.43 (11) |
B3—B2—B8—B10 | 0.65 (16) | B13—B17—B19—B18 | −137.60 (13) |
B1—B2—B8—B10 | 101.16 (13) | B12—B18—B19—B13 | −0.45 (17) |
B3—B5—B8—B7 | 63.39 (15) | B17—B18—B19—B13 | −38.11 (12) |
B2—B5—B8—B7 | 101.19 (13) | B20—B18—B19—B13 | 100.27 (14) |
B10—B5—B8—B7 | −37.16 (11) | B16—B18—B19—B13 | 62.68 (16) |
B6—B5—B8—B7 | 0.61 (16) | B12—B18—B19—B15 | −63.35 (16) |
B3—B5—B8—B1 | −0.08 (17) | B17—B18—B19—B15 | −101.01 (13) |
B2—B5—B8—B1 | 37.71 (12) | B20—B18—B19—B15 | 37.37 (12) |
B10—B5—B8—B1 | −100.63 (13) | B16—B18—B19—B15 | −0.22 (16) |
B6—B5—B8—B1 | −62.86 (15) | B12—B18—B19—B17 | 37.65 (12) |
B3—B5—B8—B2 | −37.80 (12) | B20—B18—B19—B17 | 138.37 (13) |
B10—B5—B8—B2 | −138.35 (12) | B16—B18—B19—B17 | 100.79 (13) |
B6—B5—B8—B2 | −100.57 (13) | B12—B18—B19—B20 | −100.72 (13) |
B3—B5—B8—B10 | 100.55 (13) | B17—B18—B19—B20 | −138.37 (13) |
B2—B5—B8—B10 | 138.35 (12) | B16—B18—B19—B20 | −37.59 (12) |
B6—B5—B8—B10 | 37.77 (11) | C18—B15—B20—B18 | −62.51 (16) |
C2—C3—B9—B7 | 101.99 (12) | B13—B15—B20—B18 | 0.20 (17) |
B1—C3—B9—B7 | 37.03 (12) | B14—B15—B20—B18 | −100.74 (14) |
B4—C3—B9—B7 | 140.93 (13) | B19—B15—B20—B18 | 37.67 (12) |
SN—C3—B9—B7 | −120.57 (12) | C18—B15—B20—B16 | 0.98 (16) |
C2—C3—B9—B4 | −38.94 (11) | B13—B15—B20—B16 | 63.70 (16) |
B7—C3—B9—B4 | −140.93 (13) | B14—B15—B20—B16 | −37.25 (12) |
B1—C3—B9—B4 | −103.90 (13) | B19—B15—B20—B16 | 101.17 (14) |
SN—C3—B9—B4 | 98.50 (12) | C18—B15—B20—B14 | 38.23 (11) |
C2—C3—B9—B10 | 63.23 (14) | B13—B15—B20—B14 | 100.94 (14) |
B7—C3—B9—B10 | −38.76 (12) | B19—B15—B20—B14 | 138.41 (13) |
B1—C3—B9—B10 | −1.73 (16) | C18—B15—B20—B19 | −100.18 (13) |
B4—C3—B9—B10 | 102.17 (13) | B13—B15—B20—B19 | −37.47 (12) |
SN—C3—B9—B10 | −159.33 (10) | B14—B15—B20—B19 | −138.41 (13) |
C2—C3—B9—B6 | 0.04 (15) | B12—B18—B20—B15 | 63.50 (16) |
B7—C3—B9—B6 | −101.95 (13) | B17—B18—B20—B15 | −0.22 (17) |
B1—C3—B9—B6 | −64.92 (15) | B16—B18—B20—B15 | 100.63 (14) |
B4—C3—B9—B6 | 38.98 (11) | B19—B18—B20—B15 | −37.39 (12) |
SN—C3—B9—B6 | 137.48 (11) | B12—B18—B20—B16 | −37.13 (11) |
B8—B7—B9—C3 | −98.25 (13) | B17—B18—B20—B16 | −100.85 (13) |
B10—B7—B9—C3 | −136.11 (13) | B19—B18—B20—B16 | −138.02 (13) |
B1—B7—B9—C3 | −34.62 (11) | B12—B18—B20—B14 | 0.67 (16) |
C3—B7—B9—B4 | 34.97 (11) | B17—B18—B20—B14 | −63.04 (16) |
B8—B7—B9—B4 | −63.28 (15) | B16—B18—B20—B14 | 37.81 (12) |
B10—B7—B9—B4 | −101.14 (13) | B19—B18—B20—B14 | −100.22 (13) |
B1—B7—B9—B4 | 0.35 (16) | B12—B18—B20—B19 | 100.89 (13) |
C3—B7—B9—B10 | 136.11 (13) | B17—B18—B20—B19 | 37.18 (12) |
B8—B7—B9—B10 | 37.86 (12) | B16—B18—B20—B19 | 138.02 (13) |
B1—B7—B9—B10 | 101.49 (13) | B12—B16—B20—B15 | −63.57 (15) |
C3—B7—B9—B6 | 98.82 (13) | B11—B16—B20—B15 | 0.20 (17) |
B8—B7—B9—B6 | 0.56 (16) | B18—B16—B20—B15 | −100.65 (14) |
B10—B7—B9—B6 | −37.30 (12) | B14—B16—B20—B15 | 37.02 (12) |
B1—B7—B9—B6 | 64.19 (15) | B12—B16—B20—B18 | 37.08 (11) |
C2—B4—B9—C3 | 37.02 (10) | B11—B16—B20—B18 | 100.86 (13) |
B6—B4—B9—C3 | 136.05 (12) | B14—B16—B20—B18 | 137.67 (13) |
B3—B4—B9—C3 | 98.43 (12) | B12—B16—B20—B14 | −100.59 (13) |
C2—B4—B9—B7 | 2.31 (16) | B11—B16—B20—B14 | −36.81 (12) |
C3—B4—B9—B7 | −34.71 (11) | B18—B16—B20—B14 | −137.67 (13) |
B6—B4—B9—B7 | 101.35 (13) | B12—B16—B20—B19 | −0.59 (16) |
B3—B4—B9—B7 | 63.72 (15) | B11—B16—B20—B19 | 63.18 (15) |
C2—B4—B9—B10 | −61.41 (15) | B18—B16—B20—B19 | −37.67 (12) |
C3—B4—B9—B10 | −98.43 (13) | B14—B16—B20—B19 | 99.99 (13) |
B6—B4—B9—B10 | 37.62 (12) | C18—B14—B20—B15 | −38.51 (11) |
B3—B4—B9—B10 | 0.00 (16) | B11—B14—B20—B15 | −101.36 (13) |
C2—B4—B9—B6 | −99.04 (13) | B16—B14—B20—B15 | −138.26 (13) |
C3—B4—B9—B6 | −136.05 (12) | C18—B14—B20—B18 | 61.88 (15) |
B3—B4—B9—B6 | −37.62 (11) | B15—B14—B20—B18 | 100.39 (14) |
B3—B6—B9—C3 | −0.58 (16) | B11—B14—B20—B18 | −0.96 (16) |
B4—B6—B9—C3 | −38.73 (11) | B16—B14—B20—B18 | −37.87 (12) |
B10—B6—B9—C3 | 99.46 (13) | C18—B14—B20—B16 | 99.75 (13) |
B5—B6—B9—C3 | 62.07 (14) | B15—B14—B20—B16 | 138.26 (13) |
B3—B6—B9—B7 | −62.83 (15) | B11—B14—B20—B16 | 36.91 (11) |
B4—B6—B9—B7 | −100.97 (13) | C18—B14—B20—B19 | −1.64 (16) |
B10—B6—B9—B7 | 37.21 (12) | B15—B14—B20—B19 | 36.86 (12) |
B5—B6—B9—B7 | −0.17 (16) | B11—B14—B20—B19 | −64.49 (15) |
B3—B6—B9—B4 | 38.15 (11) | B16—B14—B20—B19 | −101.40 (13) |
B10—B6—B9—B4 | 138.19 (13) | B13—B19—B20—B15 | 37.04 (12) |
B5—B6—B9—B4 | 100.80 (13) | B17—B19—B20—B15 | 100.90 (13) |
B3—B6—B9—B10 | −100.04 (13) | B18—B19—B20—B15 | 137.87 (13) |
B4—B6—B9—B10 | −138.19 (13) | B13—B19—B20—B18 | −100.83 (13) |
B5—B6—B9—B10 | −37.39 (11) | B15—B19—B20—B18 | −137.87 (13) |
C3—B7—B10—B5 | 62.20 (15) | B17—B19—B20—B18 | −36.97 (12) |
B9—B7—B10—B5 | 100.78 (13) | B13—B19—B20—B16 | −63.17 (15) |
B8—B7—B10—B5 | −37.40 (12) | B15—B19—B20—B16 | −100.21 (13) |
B1—B7—B10—B5 | −0.04 (16) | B17—B19—B20—B16 | 0.69 (16) |
C3—B7—B10—B9 | −38.58 (11) | B18—B19—B20—B16 | 37.65 (12) |
B8—B7—B10—B9 | −138.18 (13) | B13—B19—B20—B14 | 0.21 (16) |
B1—B7—B10—B9 | −100.81 (13) | B15—B19—B20—B14 | −36.83 (12) |
C3—B7—B10—B6 | −1.72 (16) | B17—B19—B20—B14 | 64.07 (15) |
B9—B7—B10—B6 | 36.87 (12) | B18—B19—B20—B14 | 101.04 (13) |
B8—B7—B10—B6 | −101.32 (13) | N2—C1—N1—C4 | −9.7 (2) |
B1—B7—B10—B6 | −63.95 (15) | C2—C1—N1—C4 | 167.54 (12) |
C3—B7—B10—B8 | 99.60 (13) | N2—C1—N1—SN | 163.67 (13) |
B9—B7—B10—B8 | 138.18 (13) | C2—C1—N1—SN | −19.08 (17) |
B1—B7—B10—B8 | 37.37 (11) | C9—C4—N1—C1 | 166.86 (13) |
B3—B5—B10—B7 | −63.69 (15) | C5—C4—N1—C1 | −71.01 (17) |
B2—B5—B10—B7 | −0.01 (16) | C9—C4—N1—SN | −6.32 (16) |
B8—B5—B10—B7 | 37.18 (11) | C5—C4—N1—SN | 115.81 (11) |
B6—B5—B10—B7 | −100.61 (13) | N1—C1—N2—C10 | −27.5 (3) |
B3—B5—B10—B9 | −0.92 (17) | C2—C1—N2—C10 | 155.19 (15) |
B2—B5—B10—B9 | 62.77 (15) | C11—C10—N2—C1 | −57.9 (2) |
B8—B5—B10—B9 | 99.96 (13) | C15—C10—N2—C1 | 179.89 (15) |
B6—B5—B10—B9 | −37.83 (12) | N4—C16—N3—C19 | 19.6 (3) |
B3—B5—B10—B6 | 36.92 (12) | C17—C16—N3—C19 | −155.61 (13) |
B2—B5—B10—B6 | 100.60 (13) | N4—C16—N3—SN | −165.20 (13) |
B8—B5—B10—B6 | 137.79 (12) | C17—C16—N3—SN | 19.58 (17) |
B3—B5—B10—B8 | −100.87 (13) | C24—C19—N3—C16 | 178.86 (14) |
B2—B5—B10—B8 | −37.19 (11) | C20—C19—N3—C16 | 59.61 (19) |
B6—B5—B10—B8 | −137.79 (12) | C24—C19—N3—SN | 3.65 (16) |
C3—B9—B10—B7 | 38.25 (11) | C20—C19—N3—SN | −115.60 (12) |
B4—B9—B10—B7 | 101.04 (13) | N3—C16—N4—C25 | 20.5 (3) |
B6—B9—B10—B7 | 138.61 (13) | C17—C16—N4—C25 | −164.17 (14) |
C3—B9—B10—B5 | −62.22 (15) | C26—C25—N4—C16 | −177.34 (15) |
B7—B9—B10—B5 | −100.47 (14) | C30—C25—N4—C16 | 60.5 (2) |
[SnCl(C9H24B10N2)(C9H25B10N2)] | Z = 2 |
Mr = 691.95 | F(000) = 704 |
Triclinic, P1 | Dx = 1.291 Mg m−3 |
a = 11.3063 (4) Å | Mo Kα radiation, λ = 0.71073 Å |
b = 13.4631 (4) Å | Cell parameters from 20939 reflections |
c = 13.7953 (4) Å | θ = 2.0–29.2° |
α = 97.078 (2)° | µ = 0.81 mm−1 |
β = 106.572 (2)° | T = 153 K |
γ = 113.377 (2)° | Plate, colorless |
V = 1779.52 (10) Å3 | 0.34 × 0.23 × 0.04 mm |
Stoe IPDS 2T diffractometer | 6943 independent reflections |
Radiation source: fine-focus sealed tube | 5878 reflections with I > 2σ(I) |
Detector resolution: 6.67 pixels mm-1 | Rint = 0.055 |
area detector scans | θmax = 26.0°, θmin = 2.0° |
Absorption correction: numerical X-Area and X-Red (Stoe & Cie, 2002) | h = −13→13 |
Tmin = 0.832, Tmax = 0.964 | k = −16→16 |
15500 measured reflections | l = −17→15 |
Refinement on F2 | Secondary atom site location: difference Fourier map |
Least-squares matrix: full | Hydrogen site location: mixed |
R[F2 > 2σ(F2)] = 0.039 | H atoms treated by a mixture of independent and constrained refinement |
wR(F2) = 0.092 | w = 1/[σ2(Fo2) + (0.0535P)2] where P = (Fo2 + 2Fc2)/3 |
S = 1.02 | (Δ/σ)max = 0.001 |
6943 reflections | Δρmax = 0.84 e Å−3 |
469 parameters | Δρmin = −1.17 e Å−3 |
21 restraints | Extinction correction: SHELXL-2016/4 (Sheldrick 2015), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
Primary atom site location: heavy-atom method | Extinction coefficient: 0.0050 (6) |
Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. |
x | y | z | Uiso*/Ueq | ||
C1 | 0.4718 (3) | 0.2167 (3) | 0.4620 (2) | 0.0238 (6) | |
C2 | 0.3778 (3) | 0.2181 (3) | 0.5359 (2) | 0.0242 (6) | |
C3 | 0.6284 (3) | 0.2915 (3) | 0.5162 (3) | 0.0248 (6) | |
C4 | 0.8084 (4) | 0.4440 (3) | 0.6712 (3) | 0.0310 (7) | |
H22 | 0.812609 | 0.477758 | 0.741619 | 0.037* | |
C5 | 0.9204 (4) | 0.4057 (3) | 0.6924 (3) | 0.0355 (8) | |
H24 | 1.005836 | 0.464911 | 0.746877 | 0.053* | |
H23 | 0.937553 | 0.390043 | 0.627811 | 0.053* | |
H25 | 0.890266 | 0.337335 | 0.716220 | 0.053* | |
C6 | 0.8373 (4) | 0.5375 (3) | 0.6164 (4) | 0.0419 (9) | |
H28 | 0.924229 | 0.603104 | 0.661454 | 0.063* | |
H26 | 0.761306 | 0.558143 | 0.602364 | 0.063* | |
H27 | 0.844900 | 0.511477 | 0.549905 | 0.063* | |
C7 | 0.7023 (4) | 0.2535 (3) | 0.3694 (3) | 0.0323 (7) | |
H29 | 0.603301 | 0.198658 | 0.328106 | 0.039* | |
C8 | 0.7936 (5) | 0.1945 (4) | 0.3786 (4) | 0.0486 (10) | |
H30 | 0.785224 | 0.160707 | 0.308352 | 0.073* | |
H32 | 0.764233 | 0.135636 | 0.414269 | 0.073* | |
H31 | 0.890297 | 0.249131 | 0.419247 | 0.073* | |
C9 | 0.7485 (5) | 0.3492 (4) | 0.3194 (3) | 0.0459 (10) | |
H34 | 0.748453 | 0.320463 | 0.250622 | 0.069* | |
H35 | 0.842142 | 0.406309 | 0.364613 | 0.069* | |
H33 | 0.684654 | 0.382679 | 0.310810 | 0.069* | |
C10 | 0.5044 (3) | 0.2298 (3) | 0.8852 (3) | 0.0256 (7) | |
C11 | 0.6076 (3) | 0.2712 (3) | 0.8189 (2) | 0.0247 (6) | |
C12 | 0.3731 (4) | 0.2420 (3) | 0.8419 (3) | 0.0273 (7) | |
C13 | 0.2568 (4) | 0.3295 (3) | 0.7313 (3) | 0.0291 (7) | |
H36 | 0.274735 | 0.365353 | 0.674250 | 0.035* | |
C14 | 0.2794 (4) | 0.4235 (3) | 0.8202 (3) | 0.0392 (9) | |
H39 | 0.219748 | 0.458103 | 0.793065 | 0.059* | |
H37 | 0.376574 | 0.480443 | 0.847693 | 0.059* | |
H38 | 0.256447 | 0.392041 | 0.876511 | 0.059* | |
C15 | 0.1072 (4) | 0.2377 (3) | 0.6831 (3) | 0.0339 (8) | |
H41 | 0.050831 | 0.263178 | 0.634482 | 0.051* | |
H40 | 0.070925 | 0.221167 | 0.738863 | 0.051* | |
H42 | 0.103814 | 0.169596 | 0.644833 | 0.051* | |
C16 | 0.2594 (4) | 0.1551 (3) | 0.9691 (3) | 0.0370 (8) | |
H43 | 0.348126 | 0.154768 | 1.009300 | 0.044* | |
C17 | 0.2248 (7) | 0.2243 (6) | 1.0410 (4) | 0.0724 (16) | |
H45 | 0.210605 | 0.189638 | 1.097852 | 0.109* | |
H46 | 0.140135 | 0.227397 | 1.000966 | 0.109* | |
H44 | 0.301368 | 0.300545 | 1.070826 | 0.109* | |
C18 | 0.1461 (5) | 0.0360 (4) | 0.9228 (4) | 0.0625 (13) | |
H47 | 0.131227 | 0.001299 | 0.979444 | 0.094* | |
H49 | 0.173087 | −0.006882 | 0.878351 | 0.094* | |
H48 | 0.060313 | 0.036040 | 0.880327 | 0.094* | |
B1 | 0.3731 (4) | 0.2867 (3) | 0.4397 (3) | 0.0265 (7) | |
H2 | 0.429 (4) | 0.3794 (16) | 0.467 (3) | 0.032* | |
B2 | 0.4020 (4) | 0.1018 (3) | 0.5079 (3) | 0.0260 (7) | |
H3 | 0.474 (3) | 0.091 (3) | 0.577 (2) | 0.031* | |
B3 | 0.2402 (4) | 0.0921 (3) | 0.5063 (3) | 0.0285 (8) | |
H4 | 0.209 (4) | 0.064 (3) | 0.571 (2) | 0.034* | |
B4 | 0.3972 (4) | 0.0860 (3) | 0.3771 (3) | 0.0272 (8) | |
H5 | 0.469 (3) | 0.058 (3) | 0.357 (3) | 0.033* | |
B5 | 0.3790 (4) | 0.2005 (3) | 0.3340 (3) | 0.0280 (8) | |
H6 | 0.436 (4) | 0.248 (3) | 0.286 (3) | 0.034* | |
B6 | 0.2221 (4) | 0.2067 (3) | 0.4637 (3) | 0.0283 (8) | |
H7 | 0.174 (4) | 0.252 (3) | 0.499 (3) | 0.034* | |
B7 | 0.2181 (4) | 0.1916 (3) | 0.3333 (3) | 0.0316 (8) | |
H8 | 0.159 (4) | 0.224 (3) | 0.278 (3) | 0.038* | |
B8 | 0.2472 (4) | 0.0058 (3) | 0.4028 (3) | 0.0307 (8) | |
H9 | 0.212 (4) | −0.0855 (17) | 0.398 (3) | 0.037* | |
B9 | 0.1356 (4) | 0.0704 (3) | 0.3748 (3) | 0.0315 (8) | |
H10 | 0.021 (2) | 0.021 (3) | 0.346 (3) | 0.038* | |
B10 | 0.2337 (4) | 0.0672 (3) | 0.2956 (3) | 0.0309 (8) | |
H11 | 0.187 (4) | 0.016 (3) | 0.2130 (18) | 0.037* | |
B11 | 0.5200 (4) | 0.1300 (3) | 0.8068 (3) | 0.0275 (8) | |
H12 | 0.435 (3) | 0.077 (3) | 0.732 (2) | 0.033* | |
B12 | 0.5164 (4) | 0.1222 (3) | 0.9336 (3) | 0.0310 (8) | |
H13 | 0.422 (3) | 0.056 (3) | 0.940 (3) | 0.037* | |
B13 | 0.6962 (4) | 0.1939 (3) | 0.8184 (3) | 0.0306 (8) | |
H14 | 0.720 (4) | 0.179 (3) | 0.747 (2) | 0.037* | |
B14 | 0.6413 (5) | 0.0989 (3) | 0.8933 (3) | 0.0334 (9) | |
H15 | 0.632 (4) | 0.012 (2) | 0.879 (3) | 0.040* | |
B15 | 0.5982 (4) | 0.2619 (3) | 1.0164 (3) | 0.0291 (8) | |
H16 | 0.555 (4) | 0.282 (3) | 1.074 (3) | 0.035* | |
B16 | 0.7777 (4) | 0.3327 (3) | 0.9014 (3) | 0.0312 (8) | |
H17 | 0.851 (4) | 0.403 (3) | 0.880 (3) | 0.037* | |
B17 | 0.6538 (4) | 0.3567 (3) | 0.9409 (3) | 0.0285 (8) | |
H18 | 0.640 (4) | 0.434 (2) | 0.943 (3) | 0.034* | |
B18 | 0.8002 (4) | 0.2237 (4) | 0.9522 (3) | 0.0352 (9) | |
H19 | 0.904 (3) | 0.226 (3) | 0.975 (3) | 0.042* | |
B19 | 0.6896 (5) | 0.1808 (4) | 1.0235 (3) | 0.0345 (9) | |
H20 | 0.711 (4) | 0.149 (3) | 1.094 (2) | 0.041* | |
B20 | 0.7732 (4) | 0.3252 (4) | 1.0270 (3) | 0.0331 (8) | |
H21 | 0.856 (3) | 0.390 (3) | 1.100 (2) | 0.040* | |
CL | 0.56514 (10) | 0.51455 (6) | 0.72974 (8) | 0.0363 (2) | |
N1 | 0.6659 (3) | 0.3514 (2) | 0.6170 (2) | 0.0258 (6) | |
N2 | 0.7189 (3) | 0.3026 (2) | 0.4756 (2) | 0.0305 (6) | |
N3 | 0.3641 (3) | 0.2901 (2) | 0.7655 (2) | 0.0252 (6) | |
N4 | 0.2758 (4) | 0.2065 (3) | 0.8829 (3) | 0.0413 (8) | |
H1 | 0.200 (3) | 0.209 (4) | 0.847 (3) | 0.050* | |
SN | 0.52251 (2) | 0.32768 (2) | 0.68914 (2) | 0.02208 (9) |
U11 | U22 | U33 | U12 | U13 | U23 | |
C1 | 0.0300 (16) | 0.0240 (14) | 0.0200 (15) | 0.0146 (13) | 0.0090 (13) | 0.0065 (12) |
C2 | 0.0287 (16) | 0.0261 (15) | 0.0222 (15) | 0.0158 (13) | 0.0100 (13) | 0.0078 (12) |
C3 | 0.0279 (16) | 0.0237 (15) | 0.0259 (16) | 0.0135 (13) | 0.0104 (13) | 0.0093 (12) |
C4 | 0.0270 (17) | 0.0264 (16) | 0.0330 (18) | 0.0103 (14) | 0.0077 (14) | 0.0002 (13) |
C5 | 0.0307 (18) | 0.0399 (19) | 0.036 (2) | 0.0185 (16) | 0.0101 (16) | 0.0064 (15) |
C6 | 0.041 (2) | 0.0261 (17) | 0.062 (3) | 0.0133 (16) | 0.026 (2) | 0.0138 (17) |
C7 | 0.0315 (18) | 0.0377 (18) | 0.0273 (17) | 0.0144 (15) | 0.0135 (14) | 0.0060 (14) |
C8 | 0.059 (3) | 0.061 (3) | 0.042 (2) | 0.038 (2) | 0.027 (2) | 0.0101 (19) |
C9 | 0.049 (2) | 0.054 (2) | 0.032 (2) | 0.018 (2) | 0.0170 (18) | 0.0153 (17) |
C10 | 0.0306 (17) | 0.0251 (15) | 0.0218 (15) | 0.0150 (13) | 0.0071 (13) | 0.0066 (12) |
C11 | 0.0290 (16) | 0.0256 (15) | 0.0203 (15) | 0.0151 (13) | 0.0073 (13) | 0.0036 (12) |
C12 | 0.0316 (17) | 0.0265 (15) | 0.0283 (17) | 0.0161 (14) | 0.0125 (14) | 0.0080 (13) |
C13 | 0.0324 (18) | 0.0298 (16) | 0.0335 (18) | 0.0205 (14) | 0.0134 (15) | 0.0102 (14) |
C14 | 0.047 (2) | 0.0360 (19) | 0.044 (2) | 0.0267 (17) | 0.0197 (18) | 0.0067 (16) |
C15 | 0.0299 (18) | 0.0364 (18) | 0.039 (2) | 0.0182 (15) | 0.0130 (16) | 0.0119 (15) |
C16 | 0.037 (2) | 0.051 (2) | 0.0326 (19) | 0.0227 (17) | 0.0181 (16) | 0.0203 (16) |
C17 | 0.095 (4) | 0.116 (5) | 0.047 (3) | 0.073 (4) | 0.041 (3) | 0.029 (3) |
C18 | 0.043 (3) | 0.064 (3) | 0.068 (3) | 0.015 (2) | 0.010 (2) | 0.034 (3) |
B1 | 0.0302 (19) | 0.0272 (17) | 0.0268 (19) | 0.0174 (15) | 0.0097 (15) | 0.0099 (14) |
B2 | 0.0302 (18) | 0.0210 (16) | 0.0265 (18) | 0.0113 (14) | 0.0108 (15) | 0.0055 (13) |
B3 | 0.0295 (19) | 0.0253 (17) | 0.031 (2) | 0.0120 (15) | 0.0120 (16) | 0.0093 (14) |
B4 | 0.0309 (19) | 0.0240 (17) | 0.0256 (18) | 0.0135 (15) | 0.0083 (15) | 0.0044 (14) |
B5 | 0.034 (2) | 0.0276 (17) | 0.0227 (18) | 0.0157 (15) | 0.0083 (15) | 0.0065 (14) |
B6 | 0.0275 (18) | 0.0299 (18) | 0.0281 (19) | 0.0154 (15) | 0.0078 (15) | 0.0073 (15) |
B7 | 0.032 (2) | 0.0331 (19) | 0.0274 (19) | 0.0152 (16) | 0.0071 (16) | 0.0089 (15) |
B8 | 0.032 (2) | 0.0250 (17) | 0.033 (2) | 0.0123 (15) | 0.0127 (17) | 0.0035 (15) |
B9 | 0.0281 (19) | 0.0283 (18) | 0.029 (2) | 0.0094 (15) | 0.0056 (16) | 0.0023 (15) |
B10 | 0.033 (2) | 0.0297 (18) | 0.0243 (19) | 0.0130 (16) | 0.0061 (16) | 0.0020 (14) |
B11 | 0.034 (2) | 0.0257 (17) | 0.0257 (18) | 0.0166 (15) | 0.0111 (16) | 0.0074 (14) |
B12 | 0.039 (2) | 0.0276 (18) | 0.030 (2) | 0.0177 (17) | 0.0119 (17) | 0.0125 (15) |
B13 | 0.032 (2) | 0.0329 (19) | 0.033 (2) | 0.0206 (17) | 0.0126 (17) | 0.0091 (16) |
B14 | 0.043 (2) | 0.0325 (19) | 0.031 (2) | 0.0238 (18) | 0.0110 (18) | 0.0104 (16) |
B15 | 0.041 (2) | 0.0298 (18) | 0.0212 (17) | 0.0188 (16) | 0.0127 (16) | 0.0074 (14) |
B16 | 0.0299 (19) | 0.0345 (19) | 0.0267 (19) | 0.0170 (17) | 0.0049 (16) | 0.0043 (15) |
B17 | 0.0319 (19) | 0.0255 (17) | 0.0223 (18) | 0.0115 (15) | 0.0063 (15) | 0.0012 (14) |
B18 | 0.034 (2) | 0.047 (2) | 0.030 (2) | 0.0251 (19) | 0.0084 (17) | 0.0131 (17) |
B19 | 0.038 (2) | 0.040 (2) | 0.028 (2) | 0.0238 (18) | 0.0068 (17) | 0.0108 (16) |
B20 | 0.033 (2) | 0.039 (2) | 0.0230 (19) | 0.0160 (17) | 0.0056 (16) | 0.0059 (15) |
CL | 0.0470 (5) | 0.0213 (4) | 0.0479 (5) | 0.0175 (4) | 0.0242 (4) | 0.0096 (3) |
N1 | 0.0268 (14) | 0.0237 (13) | 0.0247 (14) | 0.0102 (11) | 0.0089 (11) | 0.0047 (10) |
N2 | 0.0318 (15) | 0.0360 (15) | 0.0253 (14) | 0.0156 (13) | 0.0126 (12) | 0.0076 (11) |
N3 | 0.0295 (14) | 0.0257 (13) | 0.0276 (14) | 0.0173 (11) | 0.0125 (12) | 0.0099 (11) |
N4 | 0.0421 (18) | 0.064 (2) | 0.0430 (19) | 0.0352 (17) | 0.0263 (16) | 0.0331 (16) |
SN | 0.02621 (12) | 0.01939 (11) | 0.02173 (12) | 0.01194 (8) | 0.00828 (8) | 0.00486 (7) |
C1—C3 | 1.533 (4) | B1—B6 | 1.771 (6) |
C1—C2 | 1.673 (4) | B1—B7 | 1.776 (6) |
C1—B4 | 1.712 (4) | B1—B5 | 1.783 (5) |
C1—B5 | 1.713 (5) | B1—H2 | 1.106 (18) |
C1—B1 | 1.714 (5) | B2—B8 | 1.770 (5) |
C1—B2 | 1.724 (5) | B2—B4 | 1.774 (5) |
C2—B3 | 1.685 (5) | B2—B3 | 1.775 (5) |
C2—B6 | 1.692 (5) | B2—H3 | 1.129 (18) |
C2—B1 | 1.708 (5) | B3—B8 | 1.767 (5) |
C2—B2 | 1.710 (4) | B3—B9 | 1.774 (6) |
C2—SN | 2.160 (3) | B3—B6 | 1.781 (5) |
C3—N2 | 1.269 (5) | B3—H4 | 1.108 (19) |
C3—N1 | 1.372 (4) | B4—B10 | 1.765 (6) |
C4—N1 | 1.482 (4) | B4—B8 | 1.776 (6) |
C4—C5 | 1.517 (5) | B4—B5 | 1.783 (5) |
C4—C6 | 1.521 (5) | B4—H5 | 1.108 (18) |
C4—H22 | 1.0000 | B5—B10 | 1.770 (6) |
C5—H24 | 0.9800 | B5—B7 | 1.773 (6) |
C5—H23 | 0.9800 | B5—H6 | 1.129 (19) |
C5—H25 | 0.9800 | B6—B7 | 1.770 (6) |
C6—H28 | 0.9800 | B6—B9 | 1.779 (5) |
C6—H26 | 0.9800 | B6—H7 | 1.118 (18) |
C6—H27 | 0.9800 | B7—B10 | 1.784 (5) |
C7—N2 | 1.458 (4) | B7—B9 | 1.785 (6) |
C7—C9 | 1.515 (6) | B7—H8 | 1.118 (19) |
C7—C8 | 1.521 (5) | B8—B10 | 1.779 (6) |
C7—H29 | 1.0000 | B8—B9 | 1.781 (6) |
C8—H30 | 0.9800 | B8—H9 | 1.118 (18) |
C8—H32 | 0.9800 | B9—B10 | 1.773 (6) |
C8—H31 | 0.9800 | B9—H10 | 1.113 (19) |
C9—H34 | 0.9800 | B10—H11 | 1.106 (19) |
C9—H35 | 0.9800 | B11—B14 | 1.768 (6) |
C9—H33 | 0.9800 | B11—B13 | 1.777 (6) |
C10—C12 | 1.515 (5) | B11—B12 | 1.778 (6) |
C10—C11 | 1.651 (5) | B11—H12 | 1.098 (19) |
C10—B12 | 1.706 (5) | B12—B19 | 1.772 (6) |
C10—B15 | 1.714 (5) | B12—B14 | 1.777 (6) |
C10—B11 | 1.717 (5) | B12—B15 | 1.785 (5) |
C10—B17 | 1.735 (5) | B12—H13 | 1.121 (19) |
C11—B13 | 1.708 (5) | B13—B14 | 1.775 (6) |
C11—B16 | 1.714 (5) | B13—B16 | 1.775 (5) |
C11—B11 | 1.719 (5) | B13—B18 | 1.776 (6) |
C11—B17 | 1.726 (5) | B13—H14 | 1.108 (19) |
C11—SN | 2.154 (3) | B14—B18 | 1.774 (6) |
C12—N3 | 1.304 (4) | B14—B19 | 1.793 (6) |
C12—N4 | 1.328 (5) | B14—H15 | 1.116 (19) |
C13—N3 | 1.491 (4) | B15—B20 | 1.768 (6) |
C13—C15 | 1.526 (5) | B15—B19 | 1.770 (6) |
C13—C14 | 1.533 (5) | B15—B17 | 1.781 (6) |
C13—H36 | 1.0000 | B15—H16 | 1.114 (19) |
C14—H39 | 0.9800 | B16—B20 | 1.762 (6) |
C14—H37 | 0.9800 | B16—B17 | 1.767 (6) |
C14—H38 | 0.9800 | B16—B18 | 1.777 (6) |
C15—H41 | 0.9800 | B16—H17 | 1.120 (19) |
C15—H40 | 0.9800 | B17—B20 | 1.755 (6) |
C15—H42 | 0.9800 | B17—H18 | 1.107 (18) |
C16—N4 | 1.467 (5) | B18—B19 | 1.770 (6) |
C16—C18 | 1.508 (6) | B18—B20 | 1.785 (6) |
C16—C17 | 1.512 (6) | B18—H19 | 1.114 (19) |
C16—H43 | 1.0000 | B19—B20 | 1.780 (6) |
C17—H45 | 0.9800 | B19—H20 | 1.106 (19) |
C17—H46 | 0.9800 | B20—H21 | 1.116 (19) |
C17—H44 | 0.9800 | CL—SN | 2.3264 (8) |
C18—H47 | 0.9800 | N1—SN | 2.076 (3) |
C18—H49 | 0.9800 | N3—SN | 2.250 (3) |
C18—H48 | 0.9800 | N4—H1 | 0.876 (19) |
C3—C1—C2 | 115.5 (2) | B6—B7—B1 | 59.9 (2) |
C3—C1—B4 | 124.5 (3) | B5—B7—B1 | 60.3 (2) |
C2—C1—B4 | 109.4 (3) | B6—B7—B10 | 107.5 (3) |
C3—C1—B5 | 124.0 (3) | B5—B7—B10 | 59.7 (2) |
C2—C1—B5 | 109.8 (3) | B1—B7—B10 | 107.5 (3) |
B4—C1—B5 | 62.7 (2) | B6—B7—B9 | 60.1 (2) |
C3—C1—B1 | 115.4 (2) | B5—B7—B9 | 107.8 (3) |
C2—C1—B1 | 60.5 (2) | B1—B7—B9 | 107.8 (3) |
B4—C1—B1 | 114.1 (3) | B10—B7—B9 | 59.6 (2) |
B5—C1—B1 | 62.7 (2) | B6—B7—H8 | 120 (2) |
C3—C1—B2 | 116.2 (3) | B5—B7—H8 | 122 (2) |
C2—C1—B2 | 60.44 (19) | B1—B7—H8 | 120 (2) |
B4—C1—B2 | 62.2 (2) | B10—B7—H8 | 124 (2) |
B5—C1—B2 | 113.8 (3) | B9—B7—H8 | 123 (2) |
B1—C1—B2 | 113.1 (3) | B3—B8—B2 | 60.2 (2) |
C1—C2—B3 | 111.7 (2) | B3—B8—B4 | 108.1 (3) |
C1—C2—B6 | 111.4 (3) | B2—B8—B4 | 60.0 (2) |
B3—C2—B6 | 63.7 (2) | B3—B8—B10 | 107.6 (3) |
C1—C2—B1 | 60.9 (2) | B2—B8—B10 | 107.5 (3) |
B3—C2—B1 | 115.4 (3) | B4—B8—B10 | 59.5 (2) |
B6—C2—B1 | 62.8 (2) | B3—B8—B9 | 60.0 (2) |
C1—C2—B2 | 61.27 (19) | B2—B8—B9 | 108.1 (3) |
B3—C2—B2 | 63.0 (2) | B4—B8—B9 | 107.7 (3) |
B6—C2—B2 | 115.5 (3) | B10—B8—B9 | 59.7 (2) |
B1—C2—B2 | 114.1 (2) | B3—B8—H9 | 119 (2) |
C1—C2—SN | 106.55 (19) | B2—B8—H9 | 117 (2) |
B3—C2—SN | 128.3 (2) | B4—B8—H9 | 121 (2) |
B6—C2—SN | 129.7 (2) | B10—B8—H9 | 127 (2) |
B1—C2—SN | 113.1 (2) | B9—B8—H9 | 125 (2) |
B2—C2—SN | 111.1 (2) | B10—B9—B3 | 107.5 (3) |
N2—C3—N1 | 120.5 (3) | B10—B9—B6 | 107.6 (3) |
N2—C3—C1 | 126.3 (3) | B3—B9—B6 | 60.2 (2) |
N1—C3—C1 | 113.2 (3) | B10—B9—B8 | 60.1 (2) |
N1—C4—C5 | 114.1 (3) | B3—B9—B8 | 59.6 (2) |
N1—C4—C6 | 111.9 (3) | B6—B9—B8 | 107.9 (3) |
C5—C4—C6 | 112.2 (3) | B10—B9—B7 | 60.2 (2) |
N1—C4—H22 | 106.0 | B3—B9—B7 | 107.7 (3) |
C5—C4—H22 | 106.0 | B6—B9—B7 | 59.5 (2) |
C6—C4—H22 | 106.0 | B8—B9—B7 | 108.2 (3) |
C4—C5—H24 | 109.5 | B10—B9—H10 | 123 (2) |
C4—C5—H23 | 109.5 | B3—B9—H10 | 121 (2) |
H24—C5—H23 | 109.5 | B6—B9—H10 | 121 (2) |
C4—C5—H25 | 109.5 | B8—B9—H10 | 122 (2) |
H24—C5—H25 | 109.5 | B7—B9—H10 | 122 (2) |
H23—C5—H25 | 109.5 | B4—B10—B5 | 60.6 (2) |
C4—C6—H28 | 109.5 | B4—B10—B9 | 108.5 (3) |
C4—C6—H26 | 109.5 | B5—B10—B9 | 108.5 (3) |
H28—C6—H26 | 109.5 | B4—B10—B8 | 60.1 (2) |
C4—C6—H27 | 109.5 | B5—B10—B8 | 108.7 (3) |
H28—C6—H27 | 109.5 | B9—B10—B8 | 60.2 (2) |
H26—C6—H27 | 109.5 | B4—B10—B7 | 108.4 (3) |
N2—C7—C9 | 107.1 (3) | B5—B10—B7 | 59.9 (2) |
N2—C7—C8 | 107.4 (3) | B9—B10—B7 | 60.3 (2) |
C9—C7—C8 | 111.4 (3) | B8—B10—B7 | 108.4 (3) |
N2—C7—H29 | 110.3 | B4—B10—H11 | 120 (2) |
C9—C7—H29 | 110.3 | B5—B10—H11 | 120 (2) |
C8—C7—H29 | 110.3 | B9—B10—H11 | 123 (2) |
C7—C8—H30 | 109.5 | B8—B10—H11 | 122 (2) |
C7—C8—H32 | 109.5 | B7—B10—H11 | 122 (2) |
H30—C8—H32 | 109.5 | C10—B11—C11 | 57.45 (19) |
C7—C8—H31 | 109.5 | C10—B11—B14 | 104.9 (3) |
H30—C8—H31 | 109.5 | C11—B11—B14 | 104.9 (3) |
H32—C8—H31 | 109.5 | C10—B11—B13 | 104.6 (3) |
C7—C9—H34 | 109.5 | C11—B11—B13 | 58.4 (2) |
C7—C9—H35 | 109.5 | B14—B11—B13 | 60.1 (2) |
H34—C9—H35 | 109.5 | C10—B11—B12 | 58.4 (2) |
C7—C9—H33 | 109.5 | C11—B11—B12 | 104.7 (2) |
H34—C9—H33 | 109.5 | B14—B11—B12 | 60.2 (2) |
H35—C9—H33 | 109.5 | B13—B11—B12 | 107.9 (3) |
C12—C10—C11 | 112.9 (3) | C10—B11—H12 | 120 (2) |
C12—C10—B12 | 125.8 (3) | C11—B11—H12 | 118 (2) |
C11—C10—B12 | 111.1 (3) | B14—B11—H12 | 130 (2) |
C12—C10—B15 | 124.1 (3) | B13—B11—H12 | 122 (2) |
C11—C10—B15 | 111.0 (3) | B12—B11—H12 | 126 (2) |
B12—C10—B15 | 62.9 (2) | C10—B12—B19 | 104.8 (3) |
C12—C10—B11 | 116.1 (3) | C10—B12—B14 | 104.9 (3) |
C11—C10—B11 | 61.3 (2) | B19—B12—B14 | 60.7 (2) |
B12—C10—B11 | 62.6 (2) | C10—B12—B11 | 59.0 (2) |
B15—C10—B11 | 114.5 (3) | B19—B12—B11 | 108.2 (3) |
C12—C10—B17 | 113.9 (3) | B14—B12—B11 | 59.6 (2) |
C11—C10—B17 | 61.2 (2) | C10—B12—B15 | 58.7 (2) |
B12—C10—B17 | 114.1 (3) | B19—B12—B15 | 59.7 (2) |
B15—C10—B17 | 62.2 (2) | B14—B12—B15 | 108.3 (3) |
B11—C10—B17 | 114.0 (3) | B11—B12—B15 | 108.2 (3) |
C10—C11—B13 | 110.8 (3) | C10—B12—H13 | 119 (2) |
C10—C11—B16 | 110.6 (3) | B19—B12—H13 | 127 (2) |
B13—C11—B16 | 62.5 (2) | B14—B12—H13 | 126 (2) |
C10—C11—B11 | 61.2 (2) | B11—B12—H13 | 119 (2) |
B13—C11—B11 | 62.5 (2) | B15—B12—H13 | 120 (2) |
B16—C11—B11 | 113.9 (3) | C11—B13—B14 | 105.1 (3) |
C10—C11—B17 | 61.8 (2) | C11—B13—B16 | 58.9 (2) |
B13—C11—B17 | 113.8 (3) | B14—B13—B16 | 108.1 (3) |
B16—C11—B17 | 61.8 (2) | C11—B13—B18 | 105.1 (3) |
B11—C11—B17 | 114.4 (3) | B14—B13—B18 | 59.9 (2) |
C10—C11—SN | 112.3 (2) | B16—B13—B18 | 60.0 (2) |
B13—C11—SN | 126.0 (2) | C11—B13—B11 | 59.1 (2) |
B16—C11—SN | 125.7 (2) | B14—B13—B11 | 59.7 (2) |
B11—C11—SN | 115.2 (2) | B16—B13—B11 | 108.2 (3) |
B17—C11—SN | 114.3 (2) | B18—B13—B11 | 107.7 (3) |
N3—C12—N4 | 123.3 (3) | C11—B13—H14 | 116 (2) |
N3—C12—C10 | 116.4 (3) | B14—B13—H14 | 129 (2) |
N4—C12—C10 | 120.2 (3) | B16—B13—H14 | 119 (2) |
N3—C13—C15 | 115.6 (3) | B18—B13—H14 | 129 (2) |
N3—C13—C14 | 110.2 (3) | B11—B13—H14 | 118 (2) |
C15—C13—C14 | 112.9 (3) | B11—B14—B18 | 108.2 (3) |
N3—C13—H36 | 105.8 | B11—B14—B13 | 60.2 (2) |
C15—C13—H36 | 105.8 | B18—B14—B13 | 60.1 (2) |
C14—C13—H36 | 105.8 | B11—B14—B12 | 60.2 (2) |
C13—C14—H39 | 109.5 | B18—B14—B12 | 107.4 (3) |
C13—C14—H37 | 109.5 | B13—B14—B12 | 108.0 (3) |
H39—C14—H37 | 109.5 | B11—B14—B19 | 107.7 (3) |
C13—C14—H38 | 109.5 | B18—B14—B19 | 59.5 (2) |
H39—C14—H38 | 109.5 | B13—B14—B19 | 107.4 (3) |
H37—C14—H38 | 109.5 | B12—B14—B19 | 59.5 (2) |
C13—C15—H41 | 109.5 | B11—B14—H15 | 121 (2) |
C13—C15—H40 | 109.5 | B18—B14—H15 | 124 (2) |
H41—C15—H40 | 109.5 | B13—B14—H15 | 125 (2) |
C13—C15—H42 | 109.5 | B12—B14—H15 | 118 (2) |
H41—C15—H42 | 109.5 | B19—B14—H15 | 121 (2) |
H40—C15—H42 | 109.5 | C10—B15—B20 | 104.7 (3) |
N4—C16—C18 | 108.4 (4) | C10—B15—B19 | 104.5 (3) |
N4—C16—C17 | 108.5 (4) | B20—B15—B19 | 60.4 (2) |
C18—C16—C17 | 111.7 (4) | C10—B15—B17 | 59.5 (2) |
N4—C16—H43 | 109.4 | B20—B15—B17 | 59.3 (2) |
C18—C16—H43 | 109.4 | B19—B15—B17 | 107.9 (3) |
C17—C16—H43 | 109.4 | C10—B15—B12 | 58.3 (2) |
C16—C17—H45 | 109.5 | B20—B15—B12 | 108.0 (3) |
C16—C17—H46 | 109.5 | B19—B15—B12 | 59.8 (2) |
H45—C17—H46 | 109.5 | B17—B15—B12 | 108.2 (3) |
C16—C17—H44 | 109.5 | C10—B15—H16 | 119 (2) |
H45—C17—H44 | 109.5 | B20—B15—H16 | 127 (2) |
H46—C17—H44 | 109.5 | B19—B15—H16 | 127 (2) |
C16—C18—H47 | 109.5 | B17—B15—H16 | 120 (2) |
C16—C18—H49 | 109.5 | B12—B15—H16 | 119 (2) |
H47—C18—H49 | 109.5 | C11—B16—B20 | 105.1 (3) |
C16—C18—H48 | 109.5 | C11—B16—B17 | 59.4 (2) |
H47—C18—H48 | 109.5 | B20—B16—B17 | 59.6 (2) |
H49—C18—H48 | 109.5 | C11—B16—B13 | 58.6 (2) |
C2—B1—C1 | 58.53 (19) | B20—B16—B13 | 108.6 (3) |
C2—B1—B6 | 58.2 (2) | B17—B16—B13 | 108.6 (3) |
C1—B1—B6 | 105.8 (3) | C11—B16—B18 | 104.8 (3) |
C2—B1—B7 | 104.2 (3) | B20—B16—B18 | 60.6 (2) |
C1—B1—B7 | 105.1 (3) | B17—B16—B18 | 108.3 (3) |
B6—B1—B7 | 59.9 (2) | B13—B16—B18 | 60.0 (2) |
C2—B1—B5 | 105.1 (2) | C11—B16—H17 | 116 (2) |
C1—B1—B5 | 58.6 (2) | B20—B16—H17 | 128 (2) |
B6—B1—B5 | 107.8 (3) | B17—B16—H17 | 117 (2) |
B7—B1—B5 | 59.8 (2) | B13—B16—H17 | 119 (2) |
C2—B1—H2 | 115 (2) | B18—B16—H17 | 130 (2) |
C1—B1—H2 | 116 (2) | C11—B17—C10 | 56.99 (19) |
B6—B1—H2 | 123 (2) | C11—B17—B20 | 104.9 (3) |
B7—B1—H2 | 133 (2) | C10—B17—B20 | 104.4 (3) |
B5—B1—H2 | 126 (2) | C11—B17—B16 | 58.8 (2) |
C2—B2—C1 | 58.29 (19) | C10—B17—B16 | 104.4 (2) |
C2—B2—B8 | 104.1 (3) | B20—B17—B16 | 60.0 (2) |
C1—B2—B8 | 105.2 (3) | C11—B17—B15 | 104.5 (3) |
C2—B2—B4 | 104.9 (3) | C10—B17—B15 | 58.3 (2) |
C1—B2—B4 | 58.6 (2) | B20—B17—B15 | 60.0 (2) |
B8—B2—B4 | 60.2 (2) | B16—B17—B15 | 107.8 (3) |
C2—B2—B3 | 57.8 (2) | C11—B17—H18 | 117 (2) |
C1—B2—B3 | 105.2 (3) | C10—B17—H18 | 117 (2) |
B8—B2—B3 | 59.8 (2) | B20—B17—H18 | 132 (2) |
B4—B2—B3 | 107.8 (3) | B16—B17—H18 | 125 (2) |
C2—B2—H3 | 114.4 (19) | B15—B17—H18 | 124 (2) |
C1—B2—H3 | 117 (2) | B19—B18—B14 | 60.8 (2) |
B8—B2—H3 | 133.0 (19) | B19—B18—B13 | 108.4 (3) |
B4—B2—H3 | 128 (2) | B14—B18—B13 | 60.0 (2) |
B3—B2—H3 | 121 (2) | B19—B18—B16 | 107.7 (3) |
C2—B3—B8 | 105.3 (3) | B14—B18—B16 | 108.1 (3) |
C2—B3—B9 | 104.8 (3) | B13—B18—B16 | 60.0 (2) |
B8—B3—B9 | 60.4 (2) | B19—B18—B20 | 60.1 (2) |
C2—B3—B2 | 59.2 (2) | B14—B18—B20 | 108.6 (3) |
B8—B3—B2 | 59.9 (2) | B13—B18—B20 | 107.5 (3) |
B9—B3—B2 | 108.2 (3) | B16—B18—B20 | 59.3 (2) |
C2—B3—B6 | 58.4 (2) | B19—B18—H19 | 124 (2) |
B8—B3—B6 | 108.4 (3) | B14—B18—H19 | 124 (2) |
B9—B3—B6 | 60.1 (2) | B13—B18—H19 | 121 (2) |
B2—B3—B6 | 108.1 (3) | B16—B18—H19 | 119 (2) |
C2—B3—H4 | 118 (2) | B20—B18—H19 | 120 (2) |
B8—B3—H4 | 125 (2) | B18—B19—B15 | 108.3 (3) |
B9—B3—H4 | 130 (2) | B18—B19—B12 | 107.8 (3) |
B2—B3—H4 | 116 (2) | B15—B19—B12 | 60.5 (2) |
B6—B3—H4 | 122 (2) | B18—B19—B20 | 60.4 (2) |
C1—B4—B10 | 104.9 (2) | B15—B19—B20 | 59.7 (2) |
C1—B4—B2 | 59.26 (19) | B12—B19—B20 | 108.0 (3) |
B10—B4—B2 | 108.0 (3) | B18—B19—B14 | 59.7 (2) |
C1—B4—B8 | 105.4 (3) | B15—B19—B14 | 108.3 (3) |
B10—B4—B8 | 60.3 (2) | B12—B19—B14 | 59.8 (2) |
B2—B4—B8 | 59.8 (2) | B20—B19—B14 | 107.9 (3) |
C1—B4—B5 | 58.66 (19) | B18—B19—H20 | 126 (2) |
B10—B4—B5 | 59.8 (2) | B15—B19—H20 | 118 (2) |
B2—B4—B5 | 108.1 (2) | B12—B19—H20 | 119 (2) |
B8—B4—B5 | 108.2 (3) | B20—B19—H20 | 123 (2) |
C1—B4—H5 | 116 (2) | B14—B19—H20 | 123 (2) |
B10—B4—H5 | 129 (2) | B17—B20—B16 | 60.3 (2) |
B2—B4—H5 | 118 (2) | B17—B20—B15 | 60.7 (2) |
B8—B4—H5 | 128 (2) | B16—B20—B15 | 108.6 (3) |
B5—B4—H5 | 119 (2) | B17—B20—B19 | 108.6 (3) |
C1—B5—B10 | 104.7 (3) | B16—B20—B19 | 107.9 (3) |
C1—B5—B7 | 105.2 (3) | B15—B20—B19 | 59.9 (2) |
B10—B5—B7 | 60.5 (2) | B17—B20—B18 | 108.5 (3) |
C1—B5—B4 | 58.6 (2) | B16—B20—B18 | 60.1 (2) |
B10—B5—B4 | 59.6 (2) | B15—B20—B18 | 107.7 (3) |
B7—B5—B4 | 108.1 (3) | B19—B20—B18 | 59.5 (2) |
C1—B5—B1 | 58.7 (2) | B17—B20—H21 | 121 (2) |
B10—B5—B1 | 107.8 (3) | B16—B20—H21 | 122 (2) |
B7—B5—B1 | 59.9 (2) | B15—B20—H21 | 121 (2) |
B4—B5—B1 | 107.4 (3) | B19—B20—H21 | 122 (2) |
C1—B5—H6 | 119 (2) | B18—B20—H21 | 123 (2) |
B10—B5—H6 | 130 (2) | C3—N1—C4 | 119.1 (3) |
B7—B5—H6 | 123 (2) | C3—N1—SN | 121.5 (2) |
B4—B5—H6 | 125 (2) | C4—N1—SN | 119.0 (2) |
B1—B5—H6 | 115 (2) | C3—N2—C7 | 130.0 (3) |
C2—B6—B7 | 105.2 (3) | C12—N3—C13 | 121.9 (3) |
C2—B6—B1 | 59.0 (2) | C12—N3—SN | 120.1 (2) |
B7—B6—B1 | 60.2 (2) | C13—N3—SN | 117.8 (2) |
C2—B6—B9 | 104.3 (3) | C12—N4—C16 | 135.6 (3) |
B7—B6—B9 | 60.4 (2) | C12—N4—H1 | 113 (3) |
B1—B6—B9 | 108.3 (3) | C16—N4—H1 | 111 (3) |
C2—B6—B3 | 58.0 (2) | N1—SN—C11 | 100.52 (12) |
B7—B6—B3 | 108.1 (3) | N1—SN—C2 | 82.93 (11) |
B1—B6—B3 | 107.7 (3) | C11—SN—C2 | 124.32 (12) |
B9—B6—B3 | 59.8 (2) | N1—SN—N3 | 176.28 (10) |
C2—B6—H7 | 120 (2) | C11—SN—N3 | 77.66 (11) |
B7—B6—H7 | 125 (2) | C2—SN—N3 | 95.39 (11) |
B1—B6—H7 | 119 (2) | N1—SN—CL | 95.78 (8) |
B9—B6—H7 | 127 (2) | C11—SN—CL | 115.59 (8) |
B3—B6—H7 | 121 (2) | C2—SN—CL | 119.30 (9) |
B6—B7—B5 | 108.3 (3) | N3—SN—CL | 87.93 (7) |
C3—C1—C2—B3 | −146.1 (3) | B3—B8—B10—B9 | −37.6 (3) |
B4—C1—C2—B3 | 0.5 (3) | B2—B8—B10—B9 | −101.1 (3) |
B5—C1—C2—B3 | 67.6 (3) | B4—B8—B10—B9 | −138.6 (3) |
B1—C1—C2—B3 | 107.8 (3) | B3—B8—B10—B7 | −0.1 (4) |
B2—C1—C2—B3 | −39.1 (3) | B2—B8—B10—B7 | −63.6 (3) |
C3—C1—C2—B6 | 144.8 (3) | B4—B8—B10—B7 | −101.1 (3) |
B4—C1—C2—B6 | −68.6 (3) | B9—B8—B10—B7 | 37.5 (3) |
B5—C1—C2—B6 | −1.5 (3) | B6—B7—B10—B4 | −63.7 (4) |
B1—C1—C2—B6 | 38.7 (2) | B5—B7—B10—B4 | 37.7 (3) |
B2—C1—C2—B6 | −108.2 (3) | B1—B7—B10—B4 | −0.5 (4) |
C3—C1—C2—B1 | 106.1 (3) | B9—B7—B10—B4 | −101.2 (3) |
B4—C1—C2—B1 | −107.3 (3) | B6—B7—B10—B5 | −101.4 (3) |
B5—C1—C2—B1 | −40.2 (2) | B1—B7—B10—B5 | −38.2 (3) |
B2—C1—C2—B1 | −147.0 (3) | B9—B7—B10—B5 | −138.9 (3) |
C3—C1—C2—B2 | −107.0 (3) | B6—B7—B10—B9 | 37.6 (3) |
B4—C1—C2—B2 | 39.7 (2) | B5—B7—B10—B9 | 138.9 (3) |
B5—C1—C2—B2 | 106.8 (3) | B1—B7—B10—B9 | 100.7 (3) |
B1—C1—C2—B2 | 147.0 (3) | B6—B7—B10—B8 | 0.0 (4) |
C3—C1—C2—SN | −1.6 (3) | B5—B7—B10—B8 | 101.4 (3) |
B4—C1—C2—SN | 145.1 (2) | B1—B7—B10—B8 | 63.2 (4) |
B5—C1—C2—SN | −147.8 (2) | B9—B7—B10—B8 | −37.5 (3) |
B1—C1—C2—SN | −107.6 (2) | C12—C10—B11—C11 | 103.0 (3) |
B2—C1—C2—SN | 105.4 (2) | B12—C10—B11—C11 | −138.3 (3) |
C2—C1—C3—N2 | 179.5 (3) | B15—C10—B11—C11 | −101.4 (3) |
B4—C1—C3—N2 | 38.5 (5) | B17—C10—B11—C11 | −32.4 (3) |
B5—C1—C3—N2 | −39.6 (5) | C12—C10—B11—B14 | −158.6 (3) |
B1—C1—C3—N2 | −112.6 (4) | C11—C10—B11—B14 | 98.4 (3) |
B2—C1—C3—N2 | 111.4 (4) | B12—C10—B11—B14 | −39.8 (3) |
C2—C1—C3—N1 | −2.2 (4) | B15—C10—B11—B14 | −3.0 (4) |
B4—C1—C3—N1 | −143.2 (3) | B17—C10—B11—B14 | 66.0 (3) |
B5—C1—C3—N1 | 138.7 (3) | C12—C10—B11—B13 | 139.1 (3) |
B1—C1—C3—N1 | 65.7 (4) | C11—C10—B11—B13 | 36.1 (2) |
B2—C1—C3—N1 | −70.3 (3) | B12—C10—B11—B13 | −102.2 (3) |
C12—C10—C11—B13 | −147.7 (3) | B15—C10—B11—B13 | −65.4 (3) |
B12—C10—C11—B13 | 0.0 (3) | B17—C10—B11—B13 | 3.6 (4) |
B15—C10—C11—B13 | 68.0 (3) | C12—C10—B11—B12 | −118.7 (3) |
B11—C10—C11—B13 | −39.3 (3) | C11—C10—B11—B12 | 138.3 (3) |
B17—C10—C11—B13 | 106.7 (3) | B15—C10—B11—B12 | 36.8 (3) |
C12—C10—C11—B16 | 145.0 (3) | B17—C10—B11—B12 | 105.8 (3) |
B12—C10—C11—B16 | −67.4 (3) | B13—C11—B11—C10 | 138.1 (3) |
B15—C10—C11—B16 | 0.6 (3) | B16—C11—B11—C10 | 101.2 (3) |
B11—C10—C11—B16 | −106.7 (3) | B17—C11—B11—C10 | 32.7 (3) |
B17—C10—C11—B16 | 39.3 (3) | SN—C11—B11—C10 | −102.8 (2) |
C12—C10—C11—B11 | −108.3 (3) | C10—C11—B11—B14 | −98.4 (3) |
B12—C10—C11—B11 | 39.3 (3) | B13—C11—B11—B14 | 39.7 (3) |
B15—C10—C11—B11 | 107.3 (3) | B16—C11—B11—B14 | 2.9 (4) |
B17—C10—C11—B11 | 146.0 (3) | B17—C11—B11—B14 | −65.6 (3) |
C12—C10—C11—B17 | 105.7 (3) | SN—C11—B11—B14 | 158.9 (2) |
B12—C10—C11—B17 | −106.7 (3) | C10—C11—B11—B13 | −138.1 (3) |
B15—C10—C11—B17 | −38.7 (2) | B16—C11—B11—B13 | −36.8 (3) |
B11—C10—C11—B17 | −146.0 (3) | B17—C11—B11—B13 | −105.3 (3) |
C12—C10—C11—SN | −0.9 (3) | SN—C11—B11—B13 | 119.2 (3) |
B12—C10—C11—SN | 146.7 (2) | C10—C11—B11—B12 | −35.9 (2) |
B15—C10—C11—SN | −145.3 (2) | B13—C11—B11—B12 | 102.2 (3) |
B11—C10—C11—SN | 107.4 (2) | B16—C11—B11—B12 | 65.4 (3) |
B17—C10—C11—SN | −106.6 (2) | B17—C11—B11—B12 | −3.1 (4) |
C11—C10—C12—N3 | −5.0 (4) | SN—C11—B11—B12 | −138.6 (2) |
B12—C10—C12—N3 | −146.9 (3) | C12—C10—B12—B19 | −153.7 (3) |
B15—C10—C12—N3 | 133.9 (3) | C11—C10—B12—B19 | 63.8 (3) |
B11—C10—C12—N3 | −73.1 (4) | B15—C10—B12—B19 | −39.6 (3) |
B17—C10—C12—N3 | 62.4 (4) | B11—C10—B12—B19 | 102.6 (3) |
C11—C10—C12—N4 | 176.2 (3) | B17—C10—B12—B19 | −3.0 (4) |
B12—C10—C12—N4 | 34.3 (5) | C12—C10—B12—B14 | 143.3 (3) |
B15—C10—C12—N4 | −44.8 (5) | C11—C10—B12—B14 | 0.8 (3) |
B11—C10—C12—N4 | 108.1 (4) | B15—C10—B12—B14 | −102.6 (3) |
B17—C10—C12—N4 | −116.4 (4) | B11—C10—B12—B14 | 39.6 (3) |
B3—C2—B1—C1 | −101.8 (3) | B17—C10—B12—B14 | −66.1 (3) |
B6—C2—B1—C1 | −139.1 (3) | C12—C10—B12—B11 | 103.7 (3) |
B2—C2—B1—C1 | −31.6 (3) | C11—C10—B12—B11 | −38.8 (3) |
SN—C2—B1—C1 | 96.7 (2) | B15—C10—B12—B11 | −142.2 (3) |
C1—C2—B1—B6 | 139.1 (3) | B17—C10—B12—B11 | −105.7 (3) |
B3—C2—B1—B6 | 37.2 (3) | C12—C10—B12—B15 | −114.0 (4) |
B2—C2—B1—B6 | 107.5 (3) | C11—C10—B12—B15 | 103.5 (3) |
SN—C2—B1—B6 | −124.2 (2) | B11—C10—B12—B15 | 142.2 (3) |
C1—C2—B1—B7 | 99.1 (3) | B17—C10—B12—B15 | 36.6 (3) |
B3—C2—B1—B7 | −2.7 (3) | C11—B11—B12—C10 | 35.5 (2) |
B6—C2—B1—B7 | −39.9 (2) | B14—B11—B12—C10 | 134.5 (3) |
B2—C2—B1—B7 | 67.6 (3) | B13—B11—B12—C10 | 96.5 (3) |
SN—C2—B1—B7 | −164.1 (2) | C10—B11—B12—B19 | −96.6 (3) |
C1—C2—B1—B5 | 37.2 (2) | C11—B11—B12—B19 | −61.2 (3) |
B3—C2—B1—B5 | −64.7 (3) | B14—B11—B12—B19 | 37.8 (3) |
B6—C2—B1—B5 | −101.9 (3) | B13—B11—B12—B19 | −0.1 (3) |
B2—C2—B1—B5 | 5.6 (4) | C10—B11—B12—B14 | −134.5 (3) |
SN—C2—B1—B5 | 133.9 (2) | C11—B11—B12—B14 | −99.0 (3) |
C3—C1—B1—C2 | −106.3 (3) | B13—B11—B12—B14 | −37.9 (3) |
B4—C1—B1—C2 | 99.6 (3) | C10—B11—B12—B15 | −33.4 (3) |
B5—C1—B1—C2 | 136.9 (3) | C11—B11—B12—B15 | 2.0 (4) |
B2—C1—B1—C2 | 31.0 (2) | B14—B11—B12—B15 | 101.0 (3) |
C3—C1—B1—B6 | −141.6 (3) | B13—B11—B12—B15 | 63.1 (3) |
C2—C1—B1—B6 | −35.3 (2) | C10—C11—B13—B14 | −0.8 (3) |
B4—C1—B1—B6 | 64.2 (3) | B16—C11—B13—B14 | 102.3 (3) |
B5—C1—B1—B6 | 101.5 (3) | B11—C11—B13—B14 | −39.6 (3) |
B2—C1—B1—B6 | −4.3 (3) | B17—C11—B13—B14 | 66.6 (3) |
C3—C1—B1—B7 | 156.0 (3) | SN—C11—B13—B14 | −142.0 (3) |
C2—C1—B1—B7 | −97.7 (3) | C10—C11—B13—B16 | −103.1 (3) |
B4—C1—B1—B7 | 1.9 (4) | B11—C11—B13—B16 | −141.9 (3) |
B5—C1—B1—B7 | 39.2 (3) | B17—C11—B13—B16 | −35.7 (3) |
B2—C1—B1—B7 | −66.7 (3) | SN—C11—B13—B16 | 115.7 (3) |
C3—C1—B1—B5 | 116.8 (3) | C10—C11—B13—B18 | −63.1 (3) |
C2—C1—B1—B5 | −136.9 (3) | B16—C11—B13—B18 | 40.0 (3) |
B4—C1—B1—B5 | −37.3 (3) | B11—C11—B13—B18 | −101.9 (3) |
B2—C1—B1—B5 | −105.9 (3) | B17—C11—B13—B18 | 4.3 (4) |
B3—C2—B2—C1 | 138.9 (3) | SN—C11—B13—B18 | 155.7 (2) |
B6—C2—B2—C1 | 101.5 (3) | C10—C11—B13—B11 | 38.8 (2) |
B1—C2—B2—C1 | 31.5 (3) | B16—C11—B13—B11 | 141.9 (3) |
SN—C2—B2—C1 | −97.9 (2) | B17—C11—B13—B11 | 106.2 (3) |
C1—C2—B2—B8 | −99.3 (3) | SN—C11—B13—B11 | −102.4 (3) |
B3—C2—B2—B8 | 39.5 (3) | C10—B11—B13—C11 | −35.6 (2) |
B6—C2—B2—B8 | 2.2 (4) | B14—B11—B13—C11 | −134.6 (3) |
B1—C2—B2—B8 | −67.9 (3) | B12—B11—B13—C11 | −96.6 (3) |
SN—C2—B2—B8 | 162.8 (2) | C10—B11—B13—B14 | 99.0 (3) |
C1—C2—B2—B4 | −37.0 (2) | C11—B11—B13—B14 | 134.6 (3) |
B3—C2—B2—B4 | 101.9 (3) | B12—B11—B13—B14 | 38.0 (2) |
B6—C2—B2—B4 | 64.5 (3) | C10—B11—B13—B16 | −1.8 (4) |
B1—C2—B2—B4 | −5.5 (4) | C11—B11—B13—B16 | 33.8 (3) |
SN—C2—B2—B4 | −134.8 (2) | B14—B11—B13—B16 | −100.7 (3) |
C1—C2—B2—B3 | −138.9 (3) | B12—B11—B13—B16 | −62.8 (3) |
B6—C2—B2—B3 | −37.4 (3) | C10—B11—B13—B18 | 61.7 (3) |
B1—C2—B2—B3 | −107.4 (3) | C11—B11—B13—B18 | 97.3 (3) |
SN—C2—B2—B3 | 123.3 (2) | B14—B11—B13—B18 | −37.3 (3) |
C3—C1—B2—C2 | 105.9 (3) | B12—B11—B13—B18 | 0.7 (3) |
B4—C1—B2—C2 | −137.1 (3) | C10—B11—B14—B18 | −61.1 (4) |
B5—C1—B2—C2 | −100.2 (3) | C11—B11—B14—B18 | −1.4 (4) |
B1—C1—B2—C2 | −31.1 (2) | B13—B11—B14—B18 | 37.5 (3) |
C3—C1—B2—B8 | −156.7 (3) | B12—B11—B14—B18 | −100.1 (3) |
C2—C1—B2—B8 | 97.5 (3) | C10—B11—B14—B13 | −98.6 (3) |
B4—C1—B2—B8 | −39.6 (2) | C11—B11—B14—B13 | −38.9 (2) |
B5—C1—B2—B8 | −2.7 (3) | B12—B11—B14—B13 | −137.6 (3) |
B1—C1—B2—B8 | 66.4 (3) | C10—B11—B14—B12 | 39.0 (3) |
C3—C1—B2—B4 | −117.0 (3) | C11—B11—B14—B12 | 98.6 (3) |
C2—C1—B2—B4 | 137.1 (3) | B13—B11—B14—B12 | 137.6 (3) |
B5—C1—B2—B4 | 36.9 (3) | C10—B11—B14—B19 | 1.8 (4) |
B1—C1—B2—B4 | 106.0 (3) | C11—B11—B14—B19 | 61.4 (4) |
C3—C1—B2—B3 | 141.1 (3) | B13—B11—B14—B19 | 100.4 (3) |
C2—C1—B2—B3 | 35.2 (2) | B12—B11—B14—B19 | −37.2 (3) |
B4—C1—B2—B3 | −101.9 (3) | C11—B13—B14—B11 | 39.3 (2) |
B5—C1—B2—B3 | −64.9 (3) | B16—B13—B14—B11 | 100.9 (3) |
B1—C1—B2—B3 | 4.2 (3) | B18—B13—B14—B11 | 138.2 (3) |
C1—C2—B3—B8 | −1.5 (3) | C11—B13—B14—B18 | −98.9 (3) |
B6—C2—B3—B8 | 102.5 (3) | B16—B13—B14—B18 | −37.2 (3) |
B1—C2—B3—B8 | 65.6 (3) | B11—B13—B14—B18 | −138.2 (3) |
B2—C2—B3—B8 | −39.8 (3) | C11—B13—B14—B12 | 1.3 (4) |
SN—C2—B3—B8 | −136.3 (3) | B16—B13—B14—B12 | 62.9 (4) |
C1—C2—B3—B9 | −64.2 (3) | B18—B13—B14—B12 | 100.2 (3) |
B6—C2—B3—B9 | 39.7 (3) | B11—B13—B14—B12 | −38.0 (3) |
B1—C2—B3—B9 | 2.8 (4) | C11—B13—B14—B19 | −61.5 (3) |
B2—C2—B3—B9 | −102.6 (3) | B16—B13—B14—B19 | 0.1 (4) |
SN—C2—B3—B9 | 160.9 (2) | B18—B13—B14—B19 | 37.4 (3) |
C1—C2—B3—B2 | 38.4 (2) | B11—B13—B14—B19 | −100.8 (3) |
B6—C2—B3—B2 | 142.3 (3) | C10—B12—B14—B11 | −39.3 (2) |
B1—C2—B3—B2 | 105.5 (3) | B19—B12—B14—B11 | −138.1 (3) |
SN—C2—B3—B2 | −96.5 (3) | B15—B12—B14—B11 | −100.8 (3) |
C1—C2—B3—B6 | −103.9 (3) | C10—B12—B14—B18 | 62.1 (3) |
B1—C2—B3—B6 | −36.9 (3) | B19—B12—B14—B18 | −36.7 (3) |
B2—C2—B3—B6 | −142.3 (3) | B11—B12—B14—B18 | 101.4 (3) |
SN—C2—B3—B6 | 121.2 (3) | B15—B12—B14—B18 | 0.6 (4) |
C1—B2—B3—C2 | −35.4 (2) | C10—B12—B14—B13 | −1.3 (4) |
B8—B2—B3—C2 | −134.4 (3) | B19—B12—B14—B13 | −100.1 (3) |
B4—B2—B3—C2 | −96.8 (3) | B11—B12—B14—B13 | 38.0 (3) |
C2—B2—B3—B8 | 134.4 (3) | B15—B12—B14—B13 | −62.8 (4) |
C1—B2—B3—B8 | 99.0 (3) | C10—B12—B14—B19 | 98.8 (3) |
B4—B2—B3—B8 | 37.7 (3) | B11—B12—B14—B19 | 138.1 (3) |
C2—B2—B3—B9 | 96.7 (3) | B15—B12—B14—B19 | 37.3 (3) |
C1—B2—B3—B9 | 61.3 (3) | C12—C10—B15—B20 | −141.1 (3) |
B8—B2—B3—B9 | −37.7 (3) | C11—C10—B15—B20 | −1.5 (3) |
B4—B2—B3—B9 | 0.0 (3) | B12—C10—B15—B20 | 102.3 (3) |
C2—B2—B3—B6 | 33.2 (2) | B11—C10—B15—B20 | 65.6 (3) |
C1—B2—B3—B6 | −2.3 (3) | B17—C10—B15—B20 | −39.8 (3) |
B8—B2—B3—B6 | −101.3 (3) | C12—C10—B15—B19 | 156.3 (3) |
B4—B2—B3—B6 | −63.6 (3) | C11—C10—B15—B19 | −64.1 (3) |
C3—C1—B4—B10 | −153.7 (3) | B12—C10—B15—B19 | 39.6 (3) |
C2—C1—B4—B10 | 63.4 (3) | B11—C10—B15—B19 | 2.9 (4) |
B5—C1—B4—B10 | −39.5 (3) | B17—C10—B15—B19 | −102.4 (3) |
B1—C1—B4—B10 | −2.2 (4) | C12—C10—B15—B17 | −101.3 (3) |
B2—C1—B4—B10 | 102.3 (3) | C11—C10—B15—B17 | 38.3 (2) |
C3—C1—B4—B2 | 104.1 (3) | B12—C10—B15—B17 | 142.0 (3) |
C2—C1—B4—B2 | −38.9 (2) | B11—C10—B15—B17 | 105.4 (3) |
B5—C1—B4—B2 | −141.8 (3) | C12—C10—B15—B12 | 116.6 (4) |
B1—C1—B4—B2 | −104.5 (3) | C11—C10—B15—B12 | −103.8 (3) |
C3—C1—B4—B8 | 143.6 (3) | B11—C10—B15—B12 | −36.7 (3) |
C2—C1—B4—B8 | 0.6 (3) | B17—C10—B15—B12 | −142.0 (3) |
B5—C1—B4—B8 | −102.2 (3) | B19—B12—B15—C10 | 134.4 (3) |
B1—C1—B4—B8 | −64.9 (3) | B14—B12—B15—C10 | 96.7 (3) |
B2—C1—B4—B8 | 39.5 (3) | B11—B12—B15—C10 | 33.5 (3) |
C3—C1—B4—B5 | −114.2 (3) | C10—B12—B15—B20 | −96.6 (3) |
C2—C1—B4—B5 | 102.9 (3) | B19—B12—B15—B20 | 37.9 (3) |
B1—C1—B4—B5 | 37.3 (3) | B14—B12—B15—B20 | 0.1 (4) |
B2—C1—B4—B5 | 141.8 (3) | B11—B12—B15—B20 | −63.0 (4) |
C2—B2—B4—C1 | 36.8 (2) | C10—B12—B15—B19 | −134.4 (3) |
B8—B2—B4—C1 | 134.8 (3) | B14—B12—B15—B19 | −37.7 (3) |
B3—B2—B4—C1 | 97.3 (3) | B11—B12—B15—B19 | −100.9 (3) |
C2—B2—B4—B10 | −60.2 (3) | C10—B12—B15—B17 | −33.9 (3) |
C1—B2—B4—B10 | −97.0 (3) | B19—B12—B15—B17 | 100.5 (3) |
B8—B2—B4—B10 | 37.7 (2) | B14—B12—B15—B17 | 62.8 (4) |
B3—B2—B4—B10 | 0.2 (3) | B11—B12—B15—B17 | −0.4 (4) |
C2—B2—B4—B8 | −97.9 (3) | C10—C11—B16—B20 | 0.6 (3) |
C1—B2—B4—B8 | −134.8 (3) | B13—C11—B16—B20 | −102.9 (3) |
B3—B2—B4—B8 | −37.5 (2) | B11—C11—B16—B20 | −66.1 (3) |
C2—B2—B4—B5 | 3.1 (3) | B17—C11—B16—B20 | 39.9 (3) |
C1—B2—B4—B5 | −33.8 (2) | SN—C11—B16—B20 | 140.9 (2) |
B8—B2—B4—B5 | 101.0 (3) | C10—C11—B16—B17 | −39.3 (3) |
B3—B2—B4—B5 | 63.5 (3) | B13—C11—B16—B17 | −142.7 (3) |
C3—C1—B5—B10 | 154.3 (3) | B11—C11—B16—B17 | −105.9 (3) |
C2—C1—B5—B10 | −62.9 (3) | SN—C11—B16—B17 | 101.0 (3) |
B4—C1—B5—B10 | 39.3 (2) | C10—C11—B16—B13 | 103.5 (3) |
B1—C1—B5—B10 | −102.2 (3) | B11—C11—B16—B13 | 36.8 (3) |
B2—C1—B5—B10 | 2.6 (3) | B17—C11—B16—B13 | 142.7 (3) |
C3—C1—B5—B7 | −142.9 (3) | SN—C11—B16—B13 | −116.2 (3) |
C2—C1—B5—B7 | −0.1 (3) | C10—C11—B16—B18 | 63.6 (3) |
B4—C1—B5—B7 | 102.2 (3) | B13—C11—B16—B18 | −39.9 (3) |
B1—C1—B5—B7 | −39.3 (2) | B11—C11—B16—B18 | −3.1 (4) |
B2—C1—B5—B7 | 65.5 (3) | B17—C11—B16—B18 | 102.8 (3) |
C3—C1—B5—B4 | 114.9 (3) | SN—C11—B16—B18 | −156.2 (2) |
C2—C1—B5—B4 | −102.3 (3) | B14—B13—B16—C11 | −97.1 (3) |
B1—C1—B5—B4 | −141.5 (3) | B18—B13—B16—C11 | −134.2 (3) |
B2—C1—B5—B4 | −36.7 (3) | B11—B13—B16—C11 | −33.9 (3) |
C3—C1—B5—B1 | −103.6 (3) | C11—B13—B16—B20 | 96.7 (3) |
C2—C1—B5—B1 | 39.2 (2) | B14—B13—B16—B20 | −0.4 (4) |
B4—C1—B5—B1 | 141.5 (3) | B18—B13—B16—B20 | −37.6 (3) |
B2—C1—B5—B1 | 104.8 (3) | B11—B13—B16—B20 | 62.8 (4) |
B10—B4—B5—C1 | 134.7 (3) | C11—B13—B16—B17 | 33.4 (3) |
B2—B4—B5—C1 | 34.0 (2) | B14—B13—B16—B17 | −63.7 (4) |
B8—B4—B5—C1 | 97.3 (3) | B18—B13—B16—B17 | −100.9 (3) |
C1—B4—B5—B10 | −134.7 (3) | B11—B13—B16—B17 | −0.5 (4) |
B2—B4—B5—B10 | −100.7 (3) | C11—B13—B16—B18 | 134.2 (3) |
B8—B4—B5—B10 | −37.4 (3) | B14—B13—B16—B18 | 37.2 (3) |
C1—B4—B5—B7 | −97.1 (3) | B11—B13—B16—B18 | 100.3 (3) |
B10—B4—B5—B7 | 37.5 (3) | B13—C11—B17—C10 | −101.8 (3) |
B2—B4—B5—B7 | −63.1 (3) | B16—C11—B17—C10 | −137.8 (3) |
B8—B4—B5—B7 | 0.2 (3) | B11—C11—B17—C10 | −32.5 (3) |
C1—B4—B5—B1 | −33.9 (2) | SN—C11—B17—C10 | 103.3 (2) |
B10—B4—B5—B1 | 100.8 (3) | C10—C11—B17—B20 | 97.7 (3) |
B2—B4—B5—B1 | 0.1 (4) | B13—C11—B17—B20 | −4.0 (4) |
B8—B4—B5—B1 | 63.4 (3) | B16—C11—B17—B20 | −40.0 (3) |
C2—B1—B5—C1 | −37.1 (2) | B11—C11—B17—B20 | 65.2 (4) |
B6—B1—B5—C1 | −98.0 (3) | SN—C11—B17—B20 | −158.9 (2) |
B7—B1—B5—C1 | −135.1 (3) | C10—C11—B17—B16 | 137.8 (3) |
C2—B1—B5—B10 | 59.6 (3) | B13—C11—B17—B16 | 36.0 (3) |
C1—B1—B5—B10 | 96.7 (3) | B11—C11—B17—B16 | 105.2 (3) |
B6—B1—B5—B10 | −1.3 (4) | SN—C11—B17—B16 | −118.9 (3) |
B7—B1—B5—B10 | −38.3 (3) | C10—C11—B17—B15 | 35.5 (2) |
C2—B1—B5—B7 | 97.9 (3) | B13—C11—B17—B15 | −66.3 (3) |
C1—B1—B5—B7 | 135.1 (3) | B16—C11—B17—B15 | −102.3 (3) |
B6—B1—B5—B7 | 37.1 (3) | B11—C11—B17—B15 | 2.9 (4) |
C2—B1—B5—B4 | −3.3 (3) | SN—C11—B17—B15 | 138.8 (2) |
C1—B1—B5—B4 | 33.9 (2) | C12—C10—B17—C11 | −104.0 (3) |
B6—B1—B5—B4 | −64.1 (3) | B12—C10—B17—C11 | 101.8 (3) |
B7—B1—B5—B4 | −101.2 (3) | B15—C10—B17—C11 | 138.7 (3) |
C1—C2—B6—B7 | 2.3 (3) | B11—C10—B17—C11 | 32.5 (3) |
B3—C2—B6—B7 | −102.1 (3) | C12—C10—B17—B20 | 157.4 (3) |
B1—C2—B6—B7 | 40.3 (2) | C11—C10—B17—B20 | −98.6 (3) |
B2—C2—B6—B7 | −65.0 (3) | B12—C10—B17—B20 | 3.2 (4) |
SN—C2—B6—B7 | 138.7 (3) | B15—C10—B17—B20 | 40.1 (3) |
C1—C2—B6—B1 | −38.0 (2) | B11—C10—B17—B20 | −66.1 (3) |
B3—C2—B6—B1 | −142.4 (3) | C12—C10—B17—B16 | −140.4 (3) |
B2—C2—B6—B1 | −105.3 (3) | C11—C10—B17—B16 | −36.4 (2) |
SN—C2—B6—B1 | 98.4 (3) | B12—C10—B17—B16 | 65.4 (3) |
C1—C2—B6—B9 | 65.0 (3) | B15—C10—B17—B16 | 102.3 (3) |
B3—C2—B6—B9 | −39.5 (3) | B11—C10—B17—B16 | −3.9 (4) |
B1—C2—B6—B9 | 103.0 (3) | C12—C10—B17—B15 | 117.3 (3) |
B2—C2—B6—B9 | −2.3 (4) | C11—C10—B17—B15 | −138.7 (3) |
SN—C2—B6—B9 | −158.7 (2) | B12—C10—B17—B15 | −36.9 (3) |
C1—C2—B6—B3 | 104.5 (3) | B11—C10—B17—B15 | −106.2 (3) |
B1—C2—B6—B3 | 142.4 (3) | B20—B16—B17—C11 | −134.2 (3) |
B2—C2—B6—B3 | 37.1 (3) | B13—B16—B17—C11 | −33.0 (3) |
SN—C2—B6—B3 | −119.2 (3) | B18—B16—B17—C11 | −96.7 (3) |
C1—B1—B6—C2 | 35.5 (2) | C11—B16—B17—C10 | 35.6 (2) |
B7—B1—B6—C2 | 134.0 (3) | B20—B16—B17—C10 | −98.6 (3) |
B5—B1—B6—C2 | 97.0 (3) | B13—B16—B17—C10 | 2.6 (4) |
C2—B1—B6—B7 | −134.0 (3) | B18—B16—B17—C10 | −61.1 (3) |
C1—B1—B6—B7 | −98.5 (3) | C11—B16—B17—B20 | 134.2 (3) |
B5—B1—B6—B7 | −37.0 (3) | B13—B16—B17—B20 | 101.1 (3) |
C2—B1—B6—B9 | −96.0 (3) | B18—B16—B17—B20 | 37.5 (3) |
C1—B1—B6—B9 | −60.5 (3) | C11—B16—B17—B15 | 96.5 (3) |
B7—B1—B6—B9 | 38.0 (3) | B20—B16—B17—B15 | −37.7 (3) |
B5—B1—B6—B9 | 1.0 (4) | B13—B16—B17—B15 | 63.4 (3) |
C2—B1—B6—B3 | −32.9 (2) | B18—B16—B17—B15 | −0.2 (4) |
C1—B1—B6—B3 | 2.6 (3) | C10—B15—B17—C11 | −34.9 (2) |
B7—B1—B6—B3 | 101.1 (3) | B20—B15—B17—C11 | 99.1 (3) |
B5—B1—B6—B3 | 64.1 (3) | B19—B15—B17—C11 | 61.8 (3) |
B8—B3—B6—C2 | −97.0 (3) | B12—B15—B17—C11 | −1.4 (4) |
B9—B3—B6—C2 | −134.5 (3) | B20—B15—B17—C10 | 134.0 (3) |
B2—B3—B6—C2 | −33.5 (2) | B19—B15—B17—C10 | 96.6 (3) |
C2—B3—B6—B7 | 96.9 (3) | B12—B15—B17—C10 | 33.4 (3) |
B8—B3—B6—B7 | −0.1 (4) | C10—B15—B17—B20 | −134.0 (3) |
B9—B3—B6—B7 | −37.6 (3) | B19—B15—B17—B20 | −37.3 (3) |
B2—B3—B6—B7 | 63.4 (3) | B12—B15—B17—B20 | −100.5 (3) |
C2—B3—B6—B1 | 33.3 (2) | C10—B15—B17—B16 | −96.2 (3) |
B8—B3—B6—B1 | −63.7 (3) | B20—B15—B17—B16 | 37.7 (3) |
B9—B3—B6—B1 | −101.2 (3) | B19—B15—B17—B16 | 0.4 (4) |
B2—B3—B6—B1 | −0.2 (3) | B12—B15—B17—B16 | −62.8 (3) |
C2—B3—B6—B9 | 134.5 (3) | B11—B14—B18—B19 | 100.2 (3) |
B8—B3—B6—B9 | 37.6 (3) | B13—B14—B18—B19 | 137.8 (3) |
B2—B3—B6—B9 | 101.0 (3) | B12—B14—B18—B19 | 36.7 (3) |
C2—B6—B7—B5 | −2.3 (3) | B11—B14—B18—B13 | −37.6 (3) |
B1—B6—B7—B5 | 37.4 (2) | B12—B14—B18—B13 | −101.1 (3) |
B9—B6—B7—B5 | −100.4 (3) | B19—B14—B18—B13 | −137.8 (3) |
B3—B6—B7—B5 | −63.0 (3) | B11—B14—B18—B16 | −0.4 (4) |
C2—B6—B7—B1 | −39.7 (2) | B13—B14—B18—B16 | 37.2 (3) |
B9—B6—B7—B1 | −137.8 (3) | B12—B14—B18—B16 | −63.9 (4) |
B3—B6—B7—B1 | −100.4 (3) | B19—B14—B18—B16 | −100.6 (3) |
C2—B6—B7—B10 | 60.7 (3) | B11—B14—B18—B20 | 62.4 (4) |
B1—B6—B7—B10 | 100.4 (3) | B13—B14—B18—B20 | 100.0 (3) |
B9—B6—B7—B10 | −37.3 (3) | B12—B14—B18—B20 | −1.1 (4) |
B3—B6—B7—B10 | 0.0 (4) | B19—B14—B18—B20 | −37.8 (3) |
C2—B6—B7—B9 | 98.0 (3) | C11—B13—B18—B19 | 60.8 (4) |
B1—B6—B7—B9 | 137.8 (3) | B14—B13—B18—B19 | −38.2 (3) |
B3—B6—B7—B9 | 37.4 (3) | B16—B13—B18—B19 | 100.2 (3) |
C1—B5—B7—B6 | 1.5 (3) | B11—B13—B18—B19 | −1.0 (4) |
B10—B5—B7—B6 | 100.0 (3) | C11—B13—B18—B14 | 99.0 (3) |
B4—B5—B7—B6 | 62.9 (3) | B16—B13—B18—B14 | 138.4 (3) |
B1—B5—B7—B6 | −37.2 (3) | B11—B13—B18—B14 | 37.2 (3) |
C1—B5—B7—B1 | 38.7 (2) | C11—B13—B18—B16 | −39.4 (3) |
B10—B5—B7—B1 | 137.2 (3) | B14—B13—B18—B16 | −138.4 (3) |
B4—B5—B7—B1 | 100.1 (3) | B11—B13—B18—B16 | −101.2 (3) |
C1—B5—B7—B10 | −98.5 (3) | C11—B13—B18—B20 | −2.7 (4) |
B4—B5—B7—B10 | −37.2 (3) | B14—B13—B18—B20 | −101.7 (3) |
B1—B5—B7—B10 | −137.2 (3) | B16—B13—B18—B20 | 36.7 (3) |
C1—B5—B7—B9 | −62.0 (3) | B11—B13—B18—B20 | −64.5 (4) |
B10—B5—B7—B9 | 36.5 (3) | C11—B16—B18—B19 | −62.2 (3) |
B4—B5—B7—B9 | −0.6 (3) | B20—B16—B18—B19 | 37.0 (3) |
B1—B5—B7—B9 | −100.7 (3) | B17—B16—B18—B19 | −0.1 (4) |
C2—B1—B7—B6 | 39.1 (2) | B13—B16—B18—B19 | −101.4 (3) |
C1—B1—B7—B6 | 99.8 (3) | C11—B16—B18—B14 | 2.0 (4) |
B5—B1—B7—B6 | 138.4 (3) | B20—B16—B18—B14 | 101.3 (3) |
C2—B1—B7—B5 | −99.3 (3) | B17—B16—B18—B14 | 64.2 (3) |
C1—B1—B7—B5 | −38.7 (2) | B13—B16—B18—B14 | −37.2 (3) |
B6—B1—B7—B5 | −138.4 (3) | C11—B16—B18—B13 | 39.2 (3) |
C2—B1—B7—B10 | −61.4 (3) | B20—B16—B18—B13 | 138.5 (3) |
C1—B1—B7—B10 | −0.8 (4) | B17—B16—B18—B13 | 101.4 (3) |
B6—B1—B7—B10 | −100.5 (3) | C11—B16—B18—B20 | −99.3 (3) |
B5—B1—B7—B10 | 37.9 (3) | B17—B16—B18—B20 | −37.1 (3) |
C2—B1—B7—B9 | 1.4 (3) | B13—B16—B18—B20 | −138.5 (3) |
C1—B1—B7—B9 | 62.1 (3) | B14—B18—B19—B15 | −100.9 (3) |
B6—B1—B7—B9 | −37.7 (3) | B13—B18—B19—B15 | −63.1 (4) |
B5—B1—B7—B9 | 100.7 (3) | B16—B18—B19—B15 | 0.3 (4) |
C2—B3—B8—B2 | 39.5 (2) | B20—B18—B19—B15 | 37.0 (3) |
B9—B3—B8—B2 | 138.1 (3) | B14—B18—B19—B12 | −36.9 (3) |
B6—B3—B8—B2 | 100.7 (3) | B13—B18—B19—B12 | 0.9 (4) |
C2—B3—B8—B4 | 1.8 (4) | B16—B18—B19—B12 | 64.3 (3) |
B9—B3—B8—B4 | 100.4 (3) | B20—B18—B19—B12 | 101.0 (3) |
B2—B3—B8—B4 | −37.7 (3) | B14—B18—B19—B20 | −137.9 (3) |
B6—B3—B8—B4 | 63.0 (3) | B13—B18—B19—B20 | −100.1 (3) |
C2—B3—B8—B10 | −61.1 (3) | B16—B18—B19—B20 | −36.7 (3) |
B9—B3—B8—B10 | 37.5 (3) | B13—B18—B19—B14 | 37.8 (3) |
B2—B3—B8—B10 | −100.6 (3) | B16—B18—B19—B14 | 101.2 (3) |
B6—B3—B8—B10 | 0.1 (4) | B20—B18—B19—B14 | 137.9 (3) |
C2—B3—B8—B9 | −98.6 (3) | C10—B15—B19—B18 | 61.7 (3) |
B2—B3—B8—B9 | −138.1 (3) | B20—B15—B19—B18 | −37.3 (3) |
B6—B3—B8—B9 | −37.4 (3) | B17—B15—B19—B18 | −0.5 (4) |
C2—B2—B8—B3 | −38.5 (2) | B12—B15—B19—B18 | 100.6 (3) |
C1—B2—B8—B3 | −99.0 (3) | C10—B15—B19—B12 | −38.9 (3) |
B4—B2—B8—B3 | −137.9 (3) | B20—B15—B19—B12 | −137.8 (3) |
C2—B2—B8—B4 | 99.3 (3) | B17—B15—B19—B12 | −101.0 (3) |
C1—B2—B8—B4 | 38.9 (2) | C10—B15—B19—B20 | 98.9 (3) |
B3—B2—B8—B4 | 137.9 (3) | B17—B15—B19—B20 | 36.8 (3) |
C2—B2—B8—B10 | 62.0 (3) | B12—B15—B19—B20 | 137.8 (3) |
C1—B2—B8—B10 | 1.6 (3) | C10—B15—B19—B14 | −1.6 (4) |
B4—B2—B8—B10 | −37.3 (2) | B20—B15—B19—B14 | −100.5 (3) |
B3—B2—B8—B10 | 100.6 (3) | B17—B15—B19—B14 | −63.7 (4) |
C2—B2—B8—B9 | −1.0 (4) | B12—B15—B19—B14 | 37.3 (3) |
C1—B2—B8—B9 | −61.5 (3) | C10—B12—B19—B18 | −62.2 (3) |
B4—B2—B8—B9 | −100.4 (3) | B14—B12—B19—B18 | 36.9 (3) |
B3—B2—B8—B9 | 37.5 (3) | B11—B12—B19—B18 | −0.5 (4) |
C1—B4—B8—B3 | −1.5 (4) | B15—B12—B19—B18 | −101.4 (3) |
B10—B4—B8—B3 | −100.2 (3) | C10—B12—B19—B15 | 39.2 (3) |
B2—B4—B8—B3 | 37.8 (3) | B14—B12—B19—B15 | 138.2 (3) |
B5—B4—B8—B3 | −63.0 (3) | B11—B12—B19—B15 | 100.9 (3) |
C1—B4—B8—B2 | −39.3 (2) | C10—B12—B19—B20 | 1.6 (4) |
B10—B4—B8—B2 | −137.9 (3) | B14—B12—B19—B20 | 100.7 (3) |
B5—B4—B8—B2 | −100.8 (3) | B11—B12—B19—B20 | 63.3 (3) |
C1—B4—B8—B10 | 98.7 (3) | B15—B12—B19—B20 | −37.6 (3) |
B2—B4—B8—B10 | 137.9 (3) | C10—B12—B19—B14 | −99.1 (3) |
B5—B4—B8—B10 | 37.2 (2) | B11—B12—B19—B14 | −37.4 (3) |
C1—B4—B8—B9 | 61.9 (3) | B15—B12—B19—B14 | −138.2 (3) |
B10—B4—B8—B9 | −36.8 (2) | B11—B14—B19—B18 | −101.1 (3) |
B2—B4—B8—B9 | 101.1 (3) | B13—B14—B19—B18 | −37.6 (3) |
B5—B4—B8—B9 | 0.4 (3) | B12—B14—B19—B18 | −138.6 (3) |
C2—B3—B9—B10 | 61.8 (3) | B11—B14—B19—B15 | −0.1 (4) |
B8—B3—B9—B10 | −37.7 (3) | B18—B14—B19—B15 | 101.0 (3) |
B2—B3—B9—B10 | −0.2 (3) | B13—B14—B19—B15 | 63.4 (4) |
B6—B3—B9—B10 | 100.6 (3) | B12—B14—B19—B15 | −37.6 (3) |
C2—B3—B9—B6 | −38.9 (2) | B11—B14—B19—B12 | 37.5 (3) |
B8—B3—B9—B6 | −138.3 (3) | B18—B14—B19—B12 | 138.6 (3) |
B2—B3—B9—B6 | −100.8 (3) | B13—B14—B19—B12 | 101.0 (3) |
C2—B3—B9—B8 | 99.4 (3) | B11—B14—B19—B20 | −63.3 (4) |
B2—B3—B9—B8 | 37.5 (2) | B18—B14—B19—B20 | 37.8 (3) |
B6—B3—B9—B8 | 138.3 (3) | B13—B14—B19—B20 | 0.2 (4) |
C2—B3—B9—B7 | −1.7 (3) | B12—B14—B19—B20 | −100.8 (3) |
B8—B3—B9—B7 | −101.1 (3) | C11—B17—B20—B16 | 39.4 (3) |
B2—B3—B9—B7 | −63.6 (3) | C10—B17—B20—B16 | 98.5 (3) |
B6—B3—B9—B7 | 37.2 (3) | B15—B17—B20—B16 | 137.7 (3) |
C2—B6—B9—B10 | −61.9 (3) | C11—B17—B20—B15 | −98.3 (3) |
B7—B6—B9—B10 | 37.6 (3) | C10—B17—B20—B15 | −39.2 (2) |
B1—B6—B9—B10 | −0.3 (4) | B16—B17—B20—B15 | −137.7 (3) |
B3—B6—B9—B10 | −100.5 (3) | C11—B17—B20—B19 | −61.1 (4) |
C2—B6—B9—B3 | 38.6 (3) | C10—B17—B20—B19 | −2.0 (4) |
B7—B6—B9—B3 | 138.1 (3) | B16—B17—B20—B19 | −100.5 (3) |
B1—B6—B9—B3 | 100.2 (3) | B15—B17—B20—B19 | 37.2 (3) |
C2—B6—B9—B8 | 1.5 (4) | C11—B17—B20—B18 | 2.0 (4) |
B7—B6—B9—B8 | 101.0 (3) | C10—B17—B20—B18 | 61.1 (4) |
B1—B6—B9—B8 | 63.1 (4) | B16—B17—B20—B18 | −37.3 (3) |
B3—B6—B9—B8 | −37.1 (3) | B15—B17—B20—B18 | 100.4 (3) |
C2—B6—B9—B7 | −99.5 (3) | C11—B16—B20—B17 | −39.8 (2) |
B1—B6—B9—B7 | −37.9 (3) | B13—B16—B20—B17 | −101.1 (3) |
B3—B6—B9—B7 | −138.1 (3) | B18—B16—B20—B17 | −138.4 (3) |
B3—B8—B9—B10 | 137.8 (3) | C11—B16—B20—B15 | −1.5 (4) |
B2—B8—B9—B10 | 100.2 (3) | B17—B16—B20—B15 | 38.2 (3) |
B4—B8—B9—B10 | 36.7 (3) | B13—B16—B20—B15 | −62.9 (4) |
B2—B8—B9—B3 | −37.6 (3) | B18—B16—B20—B15 | −100.2 (3) |
B4—B8—B9—B3 | −101.1 (3) | C11—B16—B20—B19 | 61.9 (3) |
B10—B8—B9—B3 | −137.8 (3) | B17—B16—B20—B19 | 101.6 (3) |
B3—B8—B9—B6 | 37.3 (3) | B13—B16—B20—B19 | 0.5 (4) |
B2—B8—B9—B6 | −0.3 (4) | B18—B16—B20—B19 | −36.8 (3) |
B4—B8—B9—B6 | −63.7 (3) | C11—B16—B20—B18 | 98.7 (3) |
B10—B8—B9—B6 | −100.4 (3) | B17—B16—B20—B18 | 138.4 (3) |
B3—B8—B9—B7 | 100.3 (3) | B13—B16—B20—B18 | 37.3 (3) |
B2—B8—B9—B7 | 62.7 (3) | C10—B15—B20—B17 | 39.9 (2) |
B4—B8—B9—B7 | −0.8 (4) | B19—B15—B20—B17 | 138.4 (3) |
B10—B8—B9—B7 | −37.5 (3) | B12—B15—B20—B17 | 100.8 (3) |
B6—B7—B9—B10 | −137.9 (3) | C10—B15—B20—B16 | 1.8 (4) |
B5—B7—B9—B10 | −36.6 (3) | B19—B15—B20—B16 | 100.4 (3) |
B1—B7—B9—B10 | −100.2 (3) | B17—B15—B20—B16 | −38.1 (3) |
B6—B7—B9—B3 | −37.4 (3) | B12—B15—B20—B16 | 62.8 (3) |
B5—B7—B9—B3 | 63.9 (3) | C10—B15—B20—B19 | −98.5 (3) |
B1—B7—B9—B3 | 0.2 (4) | B17—B15—B20—B19 | −138.4 (3) |
B10—B7—B9—B3 | 100.4 (3) | B12—B15—B20—B19 | −37.6 (3) |
B5—B7—B9—B6 | 101.3 (3) | C10—B15—B20—B18 | −61.8 (3) |
B1—B7—B9—B6 | 37.6 (3) | B19—B15—B20—B18 | 36.8 (3) |
B10—B7—B9—B6 | 137.9 (3) | B17—B15—B20—B18 | −101.7 (3) |
B6—B7—B9—B8 | −100.5 (3) | B12—B15—B20—B18 | −0.8 (4) |
B5—B7—B9—B8 | 0.9 (4) | B18—B19—B20—B17 | 101.0 (3) |
B1—B7—B9—B8 | −62.8 (3) | B15—B19—B20—B17 | −37.6 (3) |
B10—B7—B9—B8 | 37.4 (3) | B12—B19—B20—B17 | 0.3 (4) |
C1—B4—B10—B5 | 38.9 (2) | B14—B19—B20—B17 | 63.5 (4) |
B2—B4—B10—B5 | 100.9 (3) | B18—B19—B20—B16 | 37.1 (3) |
B8—B4—B10—B5 | 138.4 (3) | B15—B19—B20—B16 | −101.5 (3) |
C1—B4—B10—B9 | −62.3 (3) | B12—B19—B20—B16 | −63.6 (4) |
B2—B4—B10—B9 | −0.3 (3) | B14—B19—B20—B16 | −0.4 (4) |
B8—B4—B10—B9 | 37.2 (3) | B18—B19—B20—B15 | 138.6 (3) |
B5—B4—B10—B9 | −101.2 (3) | B12—B19—B20—B15 | 37.9 (3) |
C1—B4—B10—B8 | −99.5 (3) | B14—B19—B20—B15 | 101.1 (3) |
B2—B4—B10—B8 | −37.5 (2) | B15—B19—B20—B18 | −138.6 (3) |
B5—B4—B10—B8 | −138.4 (3) | B12—B19—B20—B18 | −100.7 (3) |
C1—B4—B10—B7 | 1.6 (4) | B14—B19—B20—B18 | −37.5 (3) |
B2—B4—B10—B7 | 63.6 (3) | B19—B18—B20—B17 | −101.1 (3) |
B8—B4—B10—B7 | 101.1 (3) | B14—B18—B20—B17 | −63.0 (4) |
B5—B4—B10—B7 | −37.3 (3) | B13—B18—B20—B17 | 0.4 (4) |
C1—B5—B10—B4 | −38.9 (2) | B16—B18—B20—B17 | 37.4 (3) |
B7—B5—B10—B4 | −138.3 (3) | B19—B18—B20—B16 | −138.6 (3) |
B1—B5—B10—B4 | −100.2 (3) | B14—B18—B20—B16 | −100.4 (3) |
C1—B5—B10—B9 | 62.4 (3) | B13—B18—B20—B16 | −37.0 (3) |
B7—B5—B10—B9 | −37.0 (3) | B19—B18—B20—B15 | −36.9 (3) |
B4—B5—B10—B9 | 101.3 (3) | B14—B18—B20—B15 | 1.2 (4) |
B1—B5—B10—B9 | 1.1 (4) | B13—B18—B20—B15 | 64.7 (4) |
C1—B5—B10—B8 | −1.5 (3) | B16—B18—B20—B15 | 101.7 (3) |
B7—B5—B10—B8 | −100.9 (3) | B14—B18—B20—B19 | 38.1 (3) |
B4—B5—B10—B8 | 37.4 (3) | B13—B18—B20—B19 | 101.6 (3) |
B1—B5—B10—B8 | −62.8 (3) | B16—B18—B20—B19 | 138.6 (3) |
C1—B5—B10—B7 | 99.4 (3) | N2—C3—N1—C4 | 11.0 (5) |
B4—B5—B10—B7 | 138.3 (3) | C1—C3—N1—C4 | −167.5 (3) |
B1—B5—B10—B7 | 38.1 (3) | N2—C3—N1—SN | −176.0 (2) |
B3—B9—B10—B4 | 0.3 (3) | C1—C3—N1—SN | 5.6 (4) |
B6—B9—B10—B4 | 63.7 (3) | C5—C4—N1—C3 | −65.8 (4) |
B8—B9—B10—B4 | −37.2 (3) | C6—C4—N1—C3 | 62.9 (4) |
B7—B9—B10—B4 | 101.1 (3) | C5—C4—N1—SN | 121.0 (3) |
B3—B9—B10—B5 | −64.0 (3) | C6—C4—N1—SN | −110.3 (3) |
B6—B9—B10—B5 | −0.5 (4) | N1—C3—N2—C7 | −175.9 (3) |
B8—B9—B10—B5 | −101.4 (3) | C1—C3—N2—C7 | 2.3 (6) |
B7—B9—B10—B5 | 36.8 (3) | C9—C7—N2—C3 | 114.4 (4) |
B3—B9—B10—B8 | 37.5 (2) | C8—C7—N2—C3 | −125.9 (4) |
B6—B9—B10—B8 | 100.9 (3) | N4—C12—N3—C13 | 12.1 (5) |
B7—B9—B10—B8 | 138.2 (3) | C10—C12—N3—C13 | −166.7 (3) |
B3—B9—B10—B7 | −100.8 (3) | N4—C12—N3—SN | −172.5 (3) |
B6—B9—B10—B7 | −37.3 (3) | C10—C12—N3—SN | 8.8 (4) |
B8—B9—B10—B7 | −138.2 (3) | C15—C13—N3—C12 | −65.4 (4) |
B3—B8—B10—B4 | 101.0 (3) | C14—C13—N3—C12 | 64.0 (4) |
B2—B8—B10—B4 | 37.5 (2) | C15—C13—N3—SN | 119.0 (3) |
B9—B8—B10—B4 | 138.6 (3) | C14—C13—N3—SN | −111.5 (3) |
B3—B8—B10—B5 | 63.4 (3) | N3—C12—N4—C16 | −177.1 (4) |
B2—B8—B10—B5 | −0.1 (4) | C10—C12—N4—C16 | 1.6 (7) |
B4—B8—B10—B5 | −37.6 (3) | C18—C16—N4—C12 | −112.1 (5) |
B9—B8—B10—B5 | 101.0 (3) | C17—C16—N4—C12 | 126.5 (5) |
Acknowledgements
General financial support by the Otto-Von-Guericke-Universität Magdeburg is gratefully acknowledged.
References
Altomare, A., Burla, M. C., Camalli, M., Cascarano, G. L., Giacovazzo, C., Guagliardi, A., Moliterni, A. G. G., Polidori, G. & Spagna, R. (1999). J. Appl. Cryst. 32, 115–119. Web of Science CrossRef CAS IUCr Journals
Belmont, J. A., Soto, J., King, R. E. III, Donaldson, A. J., Hewes, J. D. & Hawthorne, M. F. (1989). J. Am. Chem. Soc. 111, 7475–7486. CrossRef CAS Web of Science
Brandenburg, K. (1999). DIAMOND. Crystal Impact GbR, Bonn, Germany.
Brown, A. D., Colquhoun, H. M., Daniels, A. J., MacBride, J. A. H., Stephenson, I. R. & Wade, K. (1992). J. Mater. Chem. 2, 793–804. CrossRef CAS Web of Science
Collins, S. (2011). Chem. Rev. 214, 91–141.
Devi, A. (2013). Coord. Chem. Rev. 257, 3332–3384. Web of Science CrossRef CAS
Dröse, P., Hrib, C. G. & Edelmann, F. T. (2010). J. Am. Chem. Soc. 132, 15540–15541. Web of Science PubMed
Edelmann, F. T. (2008). Adv. Organomet. Chem. 57, 183–352. Web of Science CrossRef CAS
Edelmann, F. T. (2013a). Adv. Organomet. Chem. 61, 55–374. Web of Science CrossRef CAS
Edelmann, F. T. (2013b). Z. Anorg. Allg. Chem. 639, 655–667. Web of Science CrossRef CAS
Felekidis, A., Goblet-Stachow, M., Liégeois, J. F., Pirotte, B., Delarge, J., Demonceau, A., Fontaine, M., Noels, A. F., Chizhevsky, I. T., Zinevich, T. V., Bregadze, V. I., Dolgushin, F. M., Yanovsky, A. I. & Struchkov, Y. T. (1997). J. Organomet. Chem. 536–537, 405–412. CSD CrossRef Web of Science
Groom, C. R., Bruno, I. J., Lightfoot, M. P. & Ward, S. C. (2016). Acta Cryst. B72, 171–179. Web of Science CSD CrossRef IUCr Journals
Harmgarth, N., Gräsing, D., Dröse, P., Hrib, C. G., Jones, P. G., Lorenz, V., Hilfert, L., Busse, S. & Edelmann, F. T. (2014). Dalton Trans. 43, 5001–5013. Web of Science CSD CrossRef CAS PubMed
Harmgarth, N., Liebing, P., Förster, A., Hilfert, L., Busse, S. & Edelmann, F. T. (2017). Eur. J. Inorg. Chem. DOI, 10, 1002ejic. 201700500.
Hillebrand, P., Hrib, C. G., Harmgarth, N., Jones, P. G., Lorenz, V., Kühling, M. & Edelmann, F. T. (2014). Inorg. Chem. Commun. 46, 127–129. Web of Science CSD CrossRef CAS
Junk, P. C. & Leary, S. G. (2000). Z. Anorg. Allg. Chem. 626, 2279–2283. CrossRef CAS
Li, Z., Barry, S. T. & Gordon, R. G. (2005). Inorg. Chem. 44, 1728–1735. Web of Science CSD CrossRef PubMed CAS
Lim, B. S., Rahtu, A., Park, J.-S. & Gordon, R. G. (2003). Inorg. Chem. 42, 7951–7958. Web of Science CSD CrossRef PubMed CAS
Murphy, D. M., Mingos, D. M. P., Haggitt, J. L., Powell, H. R., Westcott, S. A., Marder, T. B., Taylor, N. J. & Kanis, D. R. (1993). J. Mater. Chem. 3, 139–148. CSD CrossRef CAS Web of Science
Sheldrick, G. M. (2015). Acta Cryst. C71, 3–8. Web of Science CrossRef IUCr Journals
Stoe & Cie (2002). X-AREA and X-RED. Stoe & Cie, Darmstadt, Germany.
Teixidor, F., Flores, M. A., Viñas, C., Kivekäs, R. & Sillanpää, R. (1996). Angew. Chem. Int. Ed. Engl. 35, 2251–2253. CSD CrossRef CAS Web of Science
Valliant, J. F., Guenther, K. J., King, A. S., Morel, P., Schaffer, P., Sogbein, O. O. & Stephenson, K. (2002). Coord. Chem. Rev. 232, 173–230. Web of Science CrossRef CAS
Westrip, S. P. (2010). J. Appl. Cryst. 43, 920–925. Web of Science CrossRef CAS IUCr Journals
Xu, B., Yao, Z.-J. & Jin, G.-X. (2014). Russ. Chem. Bull. 63, 963–969. CSD CrossRef CAS
Yao, Z.-J. & Jin, G.-X. (2012). Organometallics, 31, 1767–1774. Web of Science CSD CrossRef CAS
Yao, Z.-J. & Jin, G.-X. (2013). Coord. Chem. Rev. 257, 2522–2535. Web of Science CrossRef CAS
Yao, Z.-J., Lin, Y.-J., Li, Z.-H. & Jin, G.-X. (2013). Chem. Eur. J. 19, 2611–2614. Web of Science CSD CrossRef CAS PubMed
Yao, Z.-J., Su, G. & Jin, G.-X. (2011). Chem. Eur. J. 17, 13298–13307. Web of Science CSD CrossRef CAS PubMed
Yao, Z.-J., Xu, B., Su, G. & Jin, G.-X. (2012). J. Organomet. Chem. 721–722, 31–35. Web of Science CSD CrossRef CAS
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