Syntheses and crystal structures of [IrIII{C(CHCO2Et)(dppm)2-κ4P,C,C′,P′}ClH]Cl·2.75CH2Cl2 and its derivatives, [IrIII{C(CHCO2Et)(dppm)2-κ4P,C,C′,P′}(CH2CO2Et)Cl]Cl·CH3OH·0.5H2O, [IrIII{C(CHCO2Et)(dppm)2-κ4P,C,C′,P′}Cl2]Cl·CH3OH·2H2O and [IrIII{C(CHCO2Et)(dppm)2-κ4P,C,C′,P′}(CH2CO2Et)(CO)]Cl2·2CH2Cl2·1.5H2O

Schlapp-Hackl, I.; Falschlunger, C.; Zauner, K.; Schuh, W.; Kopacka, H.; Wurst, K.; Peringer, P.

doi:10.1107/S2056989018017024

Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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Figure 7
A view along the a axis of the crystal packing of compound 5. Only the H atoms involved in the most significant intermolecular interactions (Table 3

) are presented and the intramolecular interactions are omitted. One phenyl group and the solvent molecules show positional disorder.

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 75| Part 1| January 2019| Pages 12-20

https://doi.org/10.1107/S2056989018017024

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