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Figure 7
Synthesis of 4: a) HNO3 65%, 373 K, 8 h, 80%; b) Pd/C 10%, H2 3 bar, EtOH, RT, 24 h, 100%; c) Oxalic acid, HCl 4 N, 373 K, 16 h, 77%; d) POCl3, dichloroethane, 363 K, 16 h, 80%. |
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access
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Figure 7
Synthesis of 4: a) HNO3 65%, 373 K, 8 h, 80%; b) Pd/C 10%, H2 3 bar, EtOH, RT, 24 h, 100%; c) Oxalic acid, HCl 4 N, 373 K, 16 h, 77%; d) POCl3, dichloroethane, 363 K, 16 h, 80%. |