(IUCr) Synthesis, crystal structure and characterizations of di-<span class="symbol">μ</span>-cyanido-1:2<span class="symbol">κ</span><span class="sup"><sup>2</sup></span><span class="it"><i>N</i></span>:<span class="it"><i>C</i></span>;2:3<span class="symbol">κ</span><span class="sup"><sup>2</sup></span><span class="it"><i>C</i></span>:<span class="it"><i>N</i></span>-bis(4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane)-1<span class="symbol">κ</span><span class="sup"><sup>8</sup></span><span class="it"><i>N</i></span><span class="sup"><sup>1</sup></span>,<span class="it"><i>N</i></span><span class="sup"><sup>10</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>4</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>7</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>13</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>16</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>21</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>24</sup></span>;3<span class="symbol">κ</span><span class="sup"><sup>8</sup></span><span class="it"><i>N</i></span><span class="sup"><sup>1</sup></span>,<span class="it"><i>N</i></span><span class="sup"><sup>10</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>4</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>7</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>13</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>16</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>21</sup></span>,<span class="it"><i>O</i></span><span class="sup"><sup>24</sup></span>-[5,10,15,20-tetrakis(4-chlorophenyl)porphyrinato-2<span class="symbol">κ</span><span class="sup"><sup>4</sup></span><span class="it"><i>N</i></span>]-2-iron(II)-1,3-dipotassium(I) tetrahydrofuran disolvate with an unknown solvent

Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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[Figure 4]

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Figure 4
Diagram showing the distances between carbon atoms of [K(222)]⁺ and the centroids of pyrrole rings, which are involved in weak C—H⋯π interactions.

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 75| Part 12| December 2019| Pages 1914-1918

https://doi.org/10.1107/S2056989019014841

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