Structure refinement of (NH4)3Al2(PO4)3 prepared by ionothermal synthesis in phospho­nium based ionic liquids – a redetermination

Nicholas, C.P.; Mowat, J.P.S.; Broach, R.W.

doi:10.1107/S2056989019015330

Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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Figure 5
XRD pattern (λ = 0.373811 Å) of (NH₄)₃Al₂(PO₄)₃ synthesized ionothermally in ethyl tributylphosphonium diethylphosphate and Rietveld residuals following structure refinement. Part A shows the fit to the overall pattern, and inset B shows the fit to high-angle regions.

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 75| Part 12| December 2019| Pages 1897-1901

https://doi.org/10.1107/S2056989019015330

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