Figure 3
The single-crystal X-ray structure of [DyAl6Na5(OAc)(Hshi)2(shi)7(DMF)8.5]2·6.335DMF, 2, including connections to neighboring sodium ions [symmetry codes: (i) x, y − 1, z; (ii) x, y + 1, z; (iii) x + 1, y, z; (iv) x − 1, y, z]. The displacement ellipsoids are at the 50% probability level. For clarity, labels have only been added to the metal ions and some of the carbon, nitrogen, and oxygen atoms. In addition, the solvent DMF molecules, the hydrogen atoms, and disorder have been omitted. See Fig. 2 for additional display details. |