Figure 1
(a) ED data collection along zone axes (high-symmetry orientations of the crystal), (b) ED data collection in fixed tilt steps, (c) left: PEDT and RED data collection (simplified representation); both protocols attempt to fill the reciprocal space between the tilt steps, right: cRED data collection (simplified representation), (d) under ideal conditions, 360° continuous rotation on ED-1 allowing a complete sampling of reciprocal space. |