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Figure 3
A selected region of the TOF neutron powder diffraction patterns at 400 K and at 4.2 K, showing the Rietveld fits to the observed patterns, including observed, calculated and difference curves, and reflection markers. Note that only the lower d-spacing range is shown in order to emphasize the presence of the superstructure reflections at 4.2 K. Thus the maximum intensity scale is only roughly 25% of what it would be if the patterns were shown to full scale.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 35| Part 2| March 2002| Pages 233-242
doi:10.1107/S0021889802001280
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