Figure 1
The design dimensions of the electrocrystallization cell. Top left: the base and working electrode assembly. The electrode is constructed from amorphous carbon rod coated in glass leaving the extreme tip exposed. Top right: a cross section of the base showing the electrical contact between the gallium and the working electrode. Bottom left: the upper part of the cell, which contains the electrolyte and the reference and counter electrodes. Bottom right: upper and lower components of the cell showing relative dimensions. |