Figure 2
Photograph of the in situ cell mounted on the Bruker SMART APEX CCD diffractometer. The cell is supported by a short XYZ goniometer head to position the exposed-tip working electrode in the X-ray beam. It is pictured with a long non-aqueous reference electrode and a silver counter electrode. All wires leading from the three electrodes are insulated by heat-shrink tubing to prevent the circuit being shorted. The low-temperature device nozzle seen in the photograph provides a convenient mount for electric leads. |