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Figure 5
[\phi] profiles of Bragg reflection recorded with the PILATUS 1M detector. (a) A typical reflection profile without error. (b), (c) Random counting errors can be detected and corrected if two conditions are fulfilled: many sample points have been acquired for the profile and the counting error is either unreasonably high or low. (d) The outlier at [\phi] = 5.62° was not detected by the semiautomatic algorithm.

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CRYSTALLOGRAPHY
ISSN: 1600-5767
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