Figure 5
profiles of Bragg reflection recorded with the PILATUS 1M detector. (a) A typical reflection profile without error. (b), (c) Random counting errors can be detected and corrected if two conditions are fulfilled: many sample points have been acquired for the profile and the counting error is either unreasonably high or low. (d) The outlier at = 5.62° was not detected by the semiautomatic algorithm. |