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Figure 9
(a) Refined Fe—N bond lengths as a function of reference γHS. (b) Enlargement of (a) in the range 0.8 < γ HS < 1.0. (c) [dFe—N(γ) − dFe—N(γ = 1.0)]/σ[dFe—N(γ = 1.0)] as a function of reference γHS. (d) Enlargement of (c) in the range 0.85 < γHS < 1.0. Part (b) also shows dFe—N corresponding to the 32 K data set after extraction of the LS species (γHS ≃ 0.98) and to those of Marchivie et al. (2002BB47) (unknown mean γHS).

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 40| Part 6| November 2007| Pages 1076-1088
doi:10.1107/S0021889807040149
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