Real-time synchrotron powder X-ray diffraction study of the antisite defect formation during sub- and supercritical synthesis of LiFePO4 and LiFe1−xMnxPO4 nanoparticles

Jensen, K.; Christensen, M.; Tyrsted, C.; Brummerstedt Iversen, B.

doi:10.1107/S0021889811006522

Journal of Applied Crystallography Journal of Applied
Crystallography

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Figure 6
Cation disorder plotted as a function of changes in the unit-cell a parameter for (a) LiFePO₄ precursor A and (b) LiFe_0.75Mn_0.25PO₄. Squares represent data at 443 K, circles at 543 K, triangles at 618 K and crosses at 653 K.

JOURNAL OF
APPLIED
CRYSTALLOGRAPHY

ISSN: 1600-5767

Volume 44| Part 2| March 2011| Pages 287-294

doi:10.1107/S0021889811006522

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