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Figure 9
Reconstructed three-dimensional reciprocal lattice of silicalite-1 with (a) incorrectly specified tilt axis orientation (42.5°) and (b) correct tilt axis orientation (48.5°). Notice that the reflection rows are bent when the tilt axis orientation is wrong, as shown in (a). This can be used to refine the tilt axis orientation.

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APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
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