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Figure 9
Reconstructed three-dimensional reciprocal lattice of silicalite-1 with (a) incorrectly specified tilt axis orientation (42.5°) and (b) correct tilt axis orientation (48.5°). Notice that the reflection rows are bent when the tilt axis orientation is wrong, as shown in (a). This can be used to refine the tilt axis orientation.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 46| Part 6| December 2013| Pages 1863-1873
https://doi.org/10.1107/S0021889813027714
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