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Figure 5
The temperature dependence of the radial scattering intensity profile along the [032 ]* direction. (a) The h0lr reciprocal space map, showing the radial direction along which the profile is taken (arrow) and the corresponding integration box (dashed lines); (b) the resulting intensity profile for the 300 K data; (c) a false-colour map showing the temperature dependence of the radial profile, the extracted peak positions being highlighted by the solid and dashed lines; (d) the extracted peak intensities. The nominal temperature of the phase transition is shown by the vertical dashed line at 585 K; the average temperature of thermal depoling (known from previous work) is shown by the vertical dashed line at 455 K. The intensity of the matrix peak can only be followed until 570 K.

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APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
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