view article
Figure 5
Quartz–Pd on- and off-coincidence spectra acquired using the mudstone rock sample shown in Fig. 4[link](a) mounted in three different positions: a reference position, rotated by 30° about the axis passing through the analysed surface of the sample and perpendicular to the plane of the experiment, and shifted by 2 mm away from the X-ray source. The source excitation conditions were 8 kV and 0.45, 0.38 and 0.47 mA, respectively. The on- and off-coincidence spectra are shown as solid and dashed lines, respectively. The spectra have been scaled to have equal K Kα fluorescence peak intensities. Each data set was acquired over 3 h with the Rh foil mounted in the incident beam.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 49| Part 5| October 2016| Pages 1561-1571
https://doi.org/10.1107/S1600576716011936
Follow J. Appl. Cryst.
Sign up for e-alerts
E-alerts
Follow J. Appl. Cryst. on Twitter
Twitter
Follow us on facebook
Facebook
Sign up for RSS feeds
RSS