Figure 5
Real-time monitoring of a solid-state transformation. (a) A subset of diffractograms around a temperature-induced crystallization process. Only those diffractograms where the reaction took place are shown [from frame 75 (blue) to frame 105 (red)]. (b) The evolution of the peak position and its FWHM over the entire measurements indicate at which frame, i.e. temperature, the transformation occurred. |