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Figure 6
Results of the FPSM analysis on search–match round-robin sample 4. Two PbO phases are present with the same structure, one with large and one with small crystallites to provide a better fitting. Not having the real sample, we do not know if the PbO does have something like a bimodal distribution of grain sizes that may explain the particular peak profile. Rwp: 0.302.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 52| Part 3| June 2019| Pages 587-598
https://doi.org/10.1107/S160057671900342X
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