Correlative vibrational spectroscopy and 2D X-ray diffraction to probe the mineralization of bone in phosphate-deficient mice

King, H.E.; Tommasini, S.M.; Rodriguez-Navarro, A.B.; Mercado, B.Q.; Skinner, H.C.W.

doi:10.1107/S1600576719009361

Journal of Applied Crystallography Journal of Applied
Crystallography

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Figure 2
(a) A representative 2D-XRD pattern generated from an orientated pregnant WT mouse bone sample. Arcs displayed in the 002 ring show that the crystal c axes are aligned with the long axis of the bone. (b) A 2θ scan generated from an angular sector in the 2D-XRD pattern containing the intense 002 arc. The large peak beginning at 5° is related to the (poly)methyl methacrylate (PMMA) block that the bone was embedded in. No background removal has been conducted on either of the patterns. (c) A 002 γ scan showing the contribution of the oriented and non-oriented fractions of bone mineral.

JOURNAL OF
APPLIED
CRYSTALLOGRAPHY

ISSN: 1600-5767

Volume 52| Part 5| October 2019| Pages 960-971

https://doi.org/10.1107/S1600576719009361

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