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Figure 5
(a) The [2\overline{2}0] topograph of the top end of the crystal grown in H2 shows the crystal to be free of dislocations and contains a few of the striking features with a black–white contrast indicating the presence of voids. (b) The [1\overline{3}\overline{1}] topograph of the same crystal (tail part), revealing a dislocation density of 2600 cm−2 and showing no sign of voids.

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APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
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